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1.
NIKITIN S.; PR?TZEL-WOLTERS D. 《IMA Journal of Mathematical Control and Information》1991,8(4):431-439
In 1983 Morse proved, for unknown scalar one-dimensional linearsystems, the nonexistence of rational or polynomial universalstabilizers (UAS). In 1983, Nussbaum gave an example of an analyticUAS. In our paper, it is shown that there exist time-invariantpolynomial UAS's with multidimensional gain adaptation. Thedesign procedure is developed for linear, minimum-phase systemsof relative degree one. Convergence of the closed-loop systemis proved. Some numerical simulations are provided. 相似文献
2.
J. T. Elliston S. E. Glover R. H. Filby 《Journal of Radioanalytical and Nuclear Chemistry》2005,263(2):301-306
Summary In the analysis of biological samples with sub ng/g uranium concentrations, pre-concentration has been shown to improve the detection limit for the determination of uranium. Recovery corrected kinetic phosphorescence analysis (KPA) combines pre-concentration and separation of uranium by anion-exchange from human tissues dissolved in 6M HCl, with the radiochemical yield determined by alpha-spectrometry, using 232U as a tracer. Total uranium is determined by KPA after correction for chemical recovery. Twenty-one randomly selected dissolved tissue samples from the United States Transuranium and Uranium Registries (USTUR) Case 0242 were chosen for comparative analyses. The set of samples included dissolved bone and soft tissues. Uranium concentrations for seven of the samples had not been previously reported. Direct KPA could not be used to determine uranium concentrations of five unreported tissues. Three of these tissues had uranium concentrations at or below the KPA LQ value of 0.028 ng/ml and two tissues had known matrix interferences. All seven of the unreported tissues were successfully analyzed by recovery corrected KPA; concentrations ranged from 9 to 1380 ng per tissue, including those that could not be analyzed by direct KPA due to matrix problems. Recovery corrected KPA gives results similar to direct KPA where matrix interferences and low detection limits are not encountered. A comparison of the direct method of KPA versus recovery corrected KPA shows marked improvement for the determination of uranium in samples that heretofore either uranium was not detected or the sample had to be drastically diluted to minimize matrix effects in order to measure uranium. 相似文献
3.
Xiao Chi Ma Bao Jing Zhang Sha Deng Shan Shan Huang Ke Xin Liu Jing Ming Jia 《中国化学快报》2009,20(3):317-319
A new ent-labdane diterpenoid lactone with a new natural product was isolated from Andrographis paniculata. Their structures were elucidated on the basis of spectral evidences including 2D NMR. 相似文献
4.
An alternative approach to synthesize pedamide,a key building block of pederin was described.Iodine-induced asymmetric heterocyclization was used as the key step to construct the skeleton,a tetrahydropyran ring with three chiral centers.Brown's asymmetric allylation and Lewis acid-mediated allylation were investigated to introduce chains and chiral alcohols.Sharpless dihydroxylation decorated the side chain.And high optically pure target was obtained by removing the epimers formed in these reactions on c... 相似文献
5.
A convenient route for the synthesis of 3,4-dihydrocoumarin derivates from salicylaldehyde derivates and 1,3-dicarbonyl compounds under solvent-free microwave irradiation conditions was described. In this way, a range of compounds was obtained in moderate to good yields in a short reaction time. 相似文献
6.
Self-injection length in La0.7Ca0.3MnO3-YBa2Cu3O7-δ ferromagnet-superconductor multilayer thin films
We have carried out extensive studies on the self-injection problem in barrierless heterojunctions between La0.7Ca0.3MnO3 (LCMO) and YBa2Cu3O7-δ (YBCO) thin films. The heterojunctions were formed in situ by sequentially growing LCMO and YBCO films on 〈100〉 LaAlO3 (LAO) substrate using a pulsed laser deposition (PLD) system. YBCO micro-bridges with 64 μm width were patterned both on
the LAO (control) and LCMO side of the substrate. Critical current, I
c, was measured at 77 K on both the control side as well as the LCMO side for different YBCO film thickness. It was observed
that while the control side showed a J
c of ∼ 2 × 106 A/cm2, the LCMO side showed about half the value for the same thickness (1800 ?). The difference in J
c indicates that a certain thickness of YBCO has become ‘effectively’ normal due to self-injection. From the measurement of
J
c at two different thicknesses (1800 ? and 1500 ?) of YBCO films both on the LAO as well as the LCMO side, the value of self-injection
length (at 77 K) was estimated to be ∼ 900 ?. To the authors’ best knowledge, this is the first time that self-injection length
has been quantified. A control experiment carried out with LaNiO3 deposited by PLD on YBCO did not show any evidence of self-injection. 相似文献
7.
8.
P.R. Elliston F. Habbal N. Saleh G.E. Watson K.W. Blazey H. Rohrer 《Journal of Physics and Chemistry of Solids》1975,36(9):877-881
Magnetic and optical measurements in the layer compound NaCrO2 are reported. This compound is antiferromagnetic with Tn = 46±2 K and θ = ?400±30 K. Broad antiferromagnetic resonances are observed which cannot be interpreted on any simple model. Optical absorption data are consistent with the appearance of antiferromagnetism. Non-intrinsic fluorescence has also been observed. 相似文献
9.
T. Mitchell P. Sandwall B. Rolfes M. Lobaugh J. Bowen J. Elliston S. E. Glover H. B. Spitz 《Journal of Radioanalytical and Nuclear Chemistry》2008,277(1):223-225
A study was initiated to investigate the chronological deposition of uranium in certain species of trees growing on the site
of a former uranium metal processing facility. The Feed Materials Production Center (FMPC) is located in Fernald, Ohio, and
for roughly 40 years operated as a large scale uranium processing center. Core samples from several species of trees growing
in different locations throughout the site were extracted using a 12.5 mm incremental wood boring drill bit. After extraction,
each core sample was cut and packaged into individual sections representing 4 annual growth rings and submitted for instrumental
neutron activation analysis (INAA). The reaction 235U(n,f)140Ba→140La+γ was evaluated using high resolution germanium gamma-spectroscopy to detect the 1.596 MeV photon emission from the fission
product 140La following a minimum of a 3 week decay. A total of 106 samples representing 7 individual trees of 3 unique species were
irradiated. In addition to the tree-core samples, 18 quality control (QC) samples and 18 standard reference material (SRM)
Fly Ash samples were irradiated with the core samples for determining neutron flux. The activity in any one sample in a batch
was determined by comparison with the amount of natural uranium in the QC standards. No significantly measurable amount of
uranium was detected in any of the tree core samples, although 3 tree core samples were in excess of the minimum detectable
amount (30 ng). 相似文献
10.
Highly effective direct synthesis of DMC from CH_3OH and CO_2 using novel Cu-Ni/C bimetallic composite catalysts 总被引:1,自引:0,他引:1
Novel Cu-Ni/C has been prepared and utilized as an efficient catalyst system in direct synthesis of DMC from CH3OH and CO2. 相似文献