排序方式: 共有32条查询结果,搜索用时 31 毫秒
1.
Archiv der Mathematik - We study the mean of the values of the zeta-function on a generalized arithmetic progression on the critical line. 相似文献
2.
Bamdad R. Yahaghi 《Proceedings of the American Mathematical Society》2004,132(4):1059-1066
In this paper we prove the existence of dense-range or one-to-one compact operators on a separable Banach space leaving a given finite chain of subspaces invariant. We use this result to prove that a semigroup of bounded operators is reducible if and only if there exists an appropriate one-to-one compact operator such that the collection of compact operators is reducible.
3.
Ali M. Soltani Seyed H. Tabatabaeian Payam Hanafizadeh Jahanyar Bamdad Soofi 《Journal of nanoparticle research》2011,13(12):7303-7312
Dozens of countries are executing national nanotechnology plans. No rigorous evaluation scheme for these plans exists, although
stakeholders—especially policy makers, top-level agencies and councils, as well as the society at large—are eager to learn
the outcome of these policies. In this article, we recommend an evaluation scheme for national nanotechnology policies that
would be used to review the whole or any component part of a national nanotechnology plan. In this scheme, a component at
any level of aggregation is evaluated. The component may be part of the plan’s overarching policy goal, which for most countries
is to create wealth and improve the quality of life of their nation with nanotechnology. Alternatively, the component may
be a programme or an activity related to a programme. The evaluation could be executed at different times in the policy’s
life cycle, i.e., before the policy is formulated, during its execution or after its completion. The three criteria for policy
evaluation are appropriateness, efficiency and effectiveness. The evaluator should select the appropriate qualitative or quantitative
methods to evaluate the various components of national nanotechnology plans. 相似文献
4.
In this work the catalytic role of unsupported gold nanoparticles on the luminol–hydrazine reaction is investigated. Gold nanoparticles catalyze the reaction of hydrazine and dissolved oxygen to generate hydrogen peroxide and also catalyze the oxidation of luminol by the produced hydrogen peroxide. The result is an intense chemiluminescence (CL) due to the excited 3-aminophthalate anion. In the absence of gold nanoparticles no detectable CL was observed by the reaction of luminol and hydrazine unless an external oxidant is present in the system. The size effect of gold nanoparticles on the CL intensity was investigated. The most intensive CL signals were obtained with 15-nm gold nanoparticles. UV–vis spectra and transmission electron microscopy studies were used to investigate the CL mechanism. The luminol and hydroxide ion concentration, gold nanoparticles size and flow rate were optimized. The proposed method was successfully applied to the determination of hydrazine in boiler feed water samples. Between 0.1 and 30 μM of hydrazine could be determined with a detection limit of 30 nM. 相似文献
5.
Research on Chemical Intermediates - Sodium ascorbate (SA) was used as a safe catalyst for the synthesis of 5-aminopyrazole-4-carbonitriles from the one-pot three-component cyclocondensation (3-CC)... 相似文献
6.
Elnaz Marzi Khosrowshahi Habib Razmi Rahim Mohammad-Rezaei Mahdiyeh Hassanpour Khaneghah 《Journal of the Iranian Chemical Society》2018,15(11):2475-2482
In this study, a simple, sensitive and low-cost iodate electrochemical sensor based on graphenized pencil lead electrode (GPLE) modified with Ag nanoparticles (AgNPs) was presented. The GPLE was simply prepared via electrochemical exfoliation of pencil lead electrode (PLE) by applying an optimized potential in acidic media. Afterward, silver nanoparticles were electrochemically deposited on the surface of GPLE using chronoamperometry technique. The fabricated electrode was carefully characterized by X-ray powder diffraction (XRD) and scanning electron microscopy (SEM) techniques. Electrochemical behavior and also the electrocatalytic performance of the modified electrode toward the reduction of iodate were studied in details using cyclic voltammetry (CV) and differential pulse voltammetry (DPV) techniques. The fabricated sensor responds efficiently to iodate over the concentration range of 0.05 to 75 mM with a detection limit of 0.017 mM and sensitivity of 0.26 µA µM?1 cm?2. Remarkably enhanced electrocatalytic performance of the modified electrode was ascribed to the synergistic effect of graphene-like nanostructures with high surface to volume ratio, excellent conductivity and also the excessive electrocatalytic behavior of silver nanoparticles. The modified electrode was successfully employed for the determination of iodate in table and sea salt samples. 相似文献
7.
Maryam Ezoddin Khosrou Abdi Somaye Behnamipour Mahdiyeh H. S. Javadi 《Journal of separation science》2022,45(10):1757-1765
A free dispersive method, air-assisted in situ deep eutectic solvent decomposition followed by the solidification of floating organic droplets liquid-liquid microextraction was indicated in this study. This technique was utilized to simultaneously ascertain some azole antifungal drugs prior to high-performance liquid chromatography. In this research, a quasi-hydrophobic deep eutectic solvent was formed from tetrabutylammonium bromide and 1-dodecanol as an organic solvent at a 1:2 molar ratio. The synthesized deep decomposition in the sample solution caused in situ dispersion of extraction solvent and analytes. Air-assisted enhanced a dispersion condition in the sample solution. 1-Dodecanol as a green option was replaced with typical extraction solvents providing the advantages of a suitable freezing point near room temperature and low density. The effect of important analytical parameters on the extraction recovery of analytes was assessed. Under these optimal conditions, the limits of detection and the limits of quantitation determined were in the range of 0.5–2.8 and 1.5–9 μg/L, for water, urine and plasma samples, respectively. The intra-day and inter-day relative standard deviations (n = 5) were calculated to be 2.9–4.6 and 4.2–8.9%, respectively. The results represented the effectiveness of the developed method for the extraction and determination of analytes in biological samples. 相似文献
8.
Masoud Salavati-Niasari Mina Gholami-Daghian Mahdiyeh Esmaeili-Zare Fatemeh Sadat Sangsefidi 《Journal of Cluster Science》2013,24(4):1093-1101
A novel and simple one-step solid state reaction in the presence of a suitable surfactant, sodium dodecyl sulfate (SDS), and a novel precursor, [bis(acetylacetonato)zinc(II)]; [Zn(acac)2]; has been developed to synthesize uniform zinc oxide microflakes with an average thickness of 0.3–2.4 μm. In the absence of SDS the product samples contained microrods. The formation of zinc oxide microflakes depends on the molar ratio of Zn(II)/SDS and the experimental procedure. The products were characterized by X-ray diffraction, photoluminescence spectroscopy, FT-IR spectroscopy, surface area, scanning electron microscopy and transmission electron microscopy to depict the phase and morphology. The synthesized ZnO microflakes have a hexagonal zincite structure. 相似文献
9.
Mahdiyeh Naderzadeh Mohammad Reza Monazzam Parvin Nassiri Samaneh Momen Bellah Fard 《Applied Acoustics》2011,72(6):393-398
The scope of this paper is to study the performance of noise barriers treated with different diffusers with/without a perforated sheet. We investigated the barrier insertion loss using a 2D boundary element method (BEM). To obtain a better depth sequence, a Random Sequence Diffuser (RSD) was designed. The results clearly showed that employing a "RSD" instead of the most popular Schroeder diffusers (Quadratic Residue Diffuser and Primitive Root Diffuser) increased the acoustic performance. We also found that the diffuser performance improved by treating the diffuser with perforated sheets either on the top surface or inside the wells. The addition of these perforated sheets inside the "RSD" (barrier model "RPI2") improved the performance by 3.59 dB (A). 相似文献
10.
Majid M. Heravi Tayebeh Hosseinnejad Zeinab Faghihi Morteza Shiri Mahdiyeh Vazinfard 《Journal of the Iranian Chemical Society》2017,14(4):823-832
An efficient, high yielding and environmentally benign strategy to the synthesis of new 2-amino-3-cyano-4-H-chromene derivatives, via one-pot three-component reaction involving malononitrile, various α- or β-naphthol and appropriate aromatic aldehydes including 2-chloroquinoline-3-carbaldehydes in the presence of morpholine in water, was achieved. During the development of the synthesis five new chromene derivatives were fruitfully synthesized. It was found that employing this approach, aromatic aldehydes bearing electron-withdrawing groups give higher yields of the corresponding products in shorter reaction times. This observation was in agreement with topological analysis of calculated electron density functions using density functional theory and quantum theory of atoms in molecules approaches. 相似文献