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Some new complexes between thecis-4,4′-dinitrodibenzo-18-crown-6 and rare earth chlorides LnCl3 (Ln=Nd, Gd, Yb) were synthesized in acetonitrile. Ligandcis-4,4′-dinitrodibenzo-18-crown-6 and its complexes were identified by infrared spectroscopy, X-ray diffraction and thermal
analysis (TG and DTA). Acis-trans isomerisation of the complexed ligand is observed about 148°C when heating the rare earth complex.
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Summary Pyridine-2,6-dialdehyde is used as a reagent in a very simple and fast method for differentiating between theo- andp-isomers of aminophenol.
Zusammenfassung Pyridin-2,6-aldehyd wurde für die einfache und schnelle Unterscheidung zwischen den o- und p-Isomeren des Aminophenols verwendet.
Résumé On décrit une méthode simple et rapide dans laquelle Pyridine 2–6 aldehyde est employé pour distinguer entre les isomères de l'aminophénol.相似文献
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Etify A. Bakhite Abdu E. Abdel-Rahman Omima. S. Mohamed Eman A. Thabet 《Phosphorus, sulfur, and silicon and the related elements》2013,188(10):1983-2006
(4-Aryl-3-cyano-6-(2-thienyl)pyridin-2-ylthio)acethydrazides (5a–c), 3-amino-4-aryl-6-(2-thienyl)thieno[2,3-b]pyridine-2-carbohydrazides (6a–c) and 3-amino-4-phenyl-6-(2-thienyl)thieno[2,3-b]pyridine-2-carboxylic acid (30) were prepared and employed as key intermediates in the synthesis of the title compounds. 相似文献
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Thabet Abdeljawad 《Numerical Functional Analysis & Optimization》2013,34(5):477-495
In this article, a completion theorem for cone metric spaces and a completion theorem for cone normed spaces are proved. The completion spaces are constructed by means of an equivalence relation defined via an ordered cone norm on the Banach space E whose cone is strongly minihedral and ordered closed. This order norm has to satisfy the generalized absolute value property. In particular, if E is a Dedekind complete Banach lattice, then, together with its absolute value norm, satisfy the desired properties. 相似文献
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We discuss the representability almost everywhere (a.e.) in C of an irreducible algebraic function as the Cauchy transform of a signed measure supported on a finite number of compact semi-analytic curves and a finite number of isolated points. This brings us to the study of trajectories of the particular family of quadratic differentials A(z ? a)(z ? b)×(z ? c)?2 dz2. More precisely, we give a necessary and sufficient condition on the complex numbers a and b for these quadratic differentials to have finite critical trajectories. We also discuss all possible configurations of critical graphs. 相似文献
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Thabet Abdeljawad Fadila Madjidi 《The European physical journal. Special topics》2017,226(16-18):3355-3368
Fractional difference operators with discrete-Mittag-Leffler kernels of order α > 1 are defined and their corresponding fractional sum operators are confirmed. We prove existence and uniqueness theorems for the discrete fractional initial value problems in the frame of discrete Caputo (ABC) and Riemann (ABR) operators by using Banach contraction theorem. Then, we prove Lyapunov type inequality for a Riemann type fractional difference boundary value problem of order 2 < α < 5∕2 within discrete Mittag-Leffler kernels, where the limiting case α → 2+ results in the ordinary difference Lyapunov inequality. Examples are given to clarify the applicability of our results and an application about the discrete fractional Sturm-Liouville eigenvalue problem is analyzed. 相似文献