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The electroredox behavior of novel modified electrodes coated with complexes of different polyviologens was investigated using cyclic voltammetry. The influences of compositions of electrolyte complex on the reversibility of the modified electrode and the electrochromic properties were studied also. It was found that all the ratios of integrated charges of cathodic to anodic scan (Qc/QA) are close to 1, which indicates that these modified electrodes have good reversible behavior. Repeated stepping over the first wave for 500 scans, the PSS-PX(p)V modified electrode showed excellent stability. The first reduction potential (E1), decrease of current height (Dec%), response time (tre tox) of various polyviologen modified electrodes were reported. In addition, the effect of the coverage of polyviologen on the electrode surface was also examined. The rate of electron transfer in this heterogeneous system is diffusion-controlled, consistent with the Conttrell equation. 相似文献
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Jun Ying LIU Yi Yang DONG Tian Song WANG Hu Wei LIU Al Jin HUANG yi Liang SUNI Zeng Pei SUN 《中国化学快报》1999,10(1):39-42
IntroductionChaedcyclodextrlnswerefirstIntroducedby几rabelforchlralseparationofamlnoacids,andthechargedCDcommonlyusednowdaysarecarboxymethyl-p-CD(CM-p-CD),p-CD-phosphate,Y-CD-phosphate,sulfobutylether-p-cyclodextrln(SBE-p-CD)etc.... 相似文献
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ZHONG Guangwu ZHANG Jiquan SONG Xianming LU Jie ZHENG Yinjia ZHANG Guangyang WANG Quanming TANG Nianyi DENG Zhongchao DING Xuantong LIU Yong WANG Enyao 《核聚变与等离子体物理》2003,23(3):161-169
1 IntroductionConfinementandheatingofplasmasareele mentarytopicsinfusionresearch .Tocharacterizethefusionplasmasinauxiliaryheatingexperimentsaswellasinohmicheatingexperiments,measure mentofionenergyinplasmasbecomesnecessary .Neutralparticleanalyzersaresuchdevicesthatareaimedatdirectanalysisofneutralparticlesemittedfromfusionplasmasandareusedinmanyfusionresearchlaboratories[1~ 4] .Detailsofparticledi agnosticprincipleforfusionplasmacanbefoundinReference [5].Emissionofneutralparticlesisintrin… 相似文献
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石墨炉原子吸收法测定组织及超滤液中的铂类药物 总被引:2,自引:0,他引:2
顺铂是目前临床上最常用也是最有前途的抗癌药物之一,特别是应用在睾丸癌和乳腺癌上。肿瘤组织及肾组织分别是顺铂抗癌作用及毒性作用的靶组织;血浆超滤液中铂则代表了血液中(氵申)蛋白结合的活性铂。为了提高药物治疗疗效和控制药物毒性反应,有必要了解顺铂在体内的处置及合并用药后顺铂在体内处置的变化,因此需要建立生物组织及超滤液中铂浓度的测定方法。 相似文献
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细胞内Ca^2+测定的新进展 总被引:5,自引:1,他引:5
Ca~(2+)对细胞的代谢与功能有重要的调节作用,它的作用几乎涉及到细胞的所有生理生化过程,如细胞的胞吐、胞饮、神经递质释放、DNA合成、细胞分裂,乃至细胞死亡等。研 相似文献
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采用超声沉淀法从In(NO3)3制备出了In(OH)3纳米晶体, 发现其在254 nm紫外光照射下对苯催化活性和活性稳定性比P25-TiO2高得多. 相似文献