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A carbon paste electrode modified with electropolymerized fills of isonicotinic acid was developed.The modified electrode shows excellent electrocatalytic activity toward the oxidation of both dopamine(DA)and epinephrine(EP).Separation of the reduction peak potentials for dopamine and epinephrine was about 357 mV in pH 5.3 phosphate buffer solution(PBS)and the character was used for the detection DA and EP simultaneously.The peak currents increase linearly with DA and EP concentration over the range of 8.0×10-5 to 7.0×10-4 mol/L and 5.0×10-6 to 1.0×10-4 mol/L with detection limits of 2 × 10-5 and 1×10-6 mol/L,respectively.The interference studies showed that the modified electrode exhibits excellent selectivity in the presence of large excess of ascorbic acid(AA). 相似文献
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超高感彩卷乳剂微晶体电镜研究 总被引:1,自引:0,他引:1
应用物理和化学相结合的方法,将超高感彩卷分层剥离,离心沉降,水洗除胶,电镜观测各层乳剂的微晶体结构。揭示了超高感彩卷各乳剂层的结构情况,披露了超高感彩剂制造技术。 相似文献
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WU GuoXiong State Key Laboratory of Ocean Engineering College of Naval Architecture Ocean Civil Engineering Shanghai Jiao Tong University Shanghai China 《中国科学:物理学 力学 天文学(英文版)》2011,(1)
The sloshing of inviscid liquid of stratified density in a rectangular tank is analyzed.As the flow is no longer irrotional,the governing equation is found to be quite different from the Laplace equation used for the liquid of constant density.In particular it contains terms of mixed temporal and spatial derivatives.The problem is solved based on the variable separation method and Laplace transform for the constant Vaisala-Brunt frequency.It is found that the stratification of density may have small effects... 相似文献
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柔性曲梁多体系统的研究现状和展望 总被引:1,自引:0,他引:1
本文对近几年来柔性多体系统建模理论的研究进展进行了评述, 详细阐述了曲梁结构多体系统动力学研究的理论背景和工程意义. 结合连续介质力学和多体系统动力学理论, 介绍了平面曲梁、空间曲梁应变位移场的描述以及几何非线性问题研究现状. 通过国内外文献及已有的研究, 综述了现有曲梁的离散化方法, 以及这些方法对于定曲率、变曲率曲梁的适用性. 然后, 总结了曲梁刚柔耦合动力学建模和数值计算中的难点问题, 介绍了平面曲梁、空间曲梁实验研究的现状. 最后, 综合全文, 提出了目前研究存在的难点问题, 以及计划解决这些难点问题的方法. 相似文献
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<正>A convenient and effective Paal-Knorr condensations of 2,5-hexanedione with most amines have been carried out at room temperature under solvent-free condition.Macroporous strongly acidic styrol resin(D001) as a novel,efficient,cost-effective,and reusable solid acid catalyst for the synthesis of pyrroles under the same conditions.The pyrroles were obtained in high yields in short reaction times. 相似文献
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Chuan Fu College of Architecture North China University of Technology Beijing China 《Acta Mechanica Sinica》2011,27(5):817-822
The sealed,tuned liquid column gas damper (TLCGD) with gas-spring effect extends the frequency range of application and efficiently increases the modal structural damping.Active tuned liquid column gas damper (ATLCGD) is developed for the vibration control of plane asymmetric buildings subjected to earthquake excitation,improving the performance of the passive control scheme.The active behaviour is obtained by adjusting the pressure at the end of the liquid column using a pressurised reservoir.The classical linear quadratic regulator (LQR) design is presented as a straightforward approach to optimal control.Numerical simulations indicate a significant vibration reduction of plane asymmetric buildings by active control within the strong motion of the dynamic response. 相似文献
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Yue XiukuiDept. of Math. Phys. Shandong Institute of Architecture Engineering Shandong China. 《高校应用数学学报(英文版)》2004,19(3):252-256
§1 IntroductionSuppose thatf is analytic in the open unit disc D in the complex plane.We defineMp(r,f) =12π∫2π0 | f(reiθ) | pdθ1 / p,0
相似文献
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CHEN RuiLin ZENG QingYuan HUANG YunQing XIANG Jun WEN Ying GUO XiaoGang YIN ChangJun DONG Hui & ZHAO Gang Hunan Key Laboratory for Computation Simulation in Science Engineering Xiangtan University Xiangtan China School of Civil Engineering & Mechanics School of Civil Architecture Central South University Changsha AMEC Toronto MAG Canada 《中国科学:物理学 力学 天文学(英文版)》2010,(4)
Based on the analysis theory of random energy of train derailment, an analysis theory of random energy of train derailment in wind is suggested. Two methods are proposed -the time domain method and the frequency domain method of analysis theory of random energy of train derailment in wind. The curves of σ pw -v under various wind speeds are obtained through the computation. The original curve of σ p -v is expanded, which turns the analysis theory of random energy of train derailment into the all-weather theory. Train derailment condition has been established under wind action. The first and second criterions of train derailment have been proposed in light of wind action. The analysis of train derailment cases at home or abroad is made, in- cluding the first analysis of Xinjiang train derailment case encountered 13-level of gale, which explained the inevitability of train derailment. The analysis theory of random energy of train derailment in wind shows its validity and accuracy. The input energy σ pw of the transverse vibration of train-track(bridge)-wind system is linked to train speed. With the establishment of the analysis theory of random energy of train derailment in wind, It is likely to initiate an all-weather speed limit map for a train or any high-speed train. 相似文献
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