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The aggregation of dansyl chloride (DNS-Cl) in acetone has been studied in detail by steady-state fluorescence techniques.It has been demonstrated that DNS-Cl is stable in acetone during purification and aggregation study processes.The aggregates are not solvolyzed in acetone,and do not take part n any chemical reactions either.It has been found that DNS-Cl tends to aggregate even when its concentration is much lower than its solubility in acetone.The aggregation is reversible,and both the aggregation and the deaggregation are very slow processes.Introduction of SDS has a positive effect upon the formation and stabilization of the aggregates. 相似文献
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SHEN Yehua WANG Haibo BAI Quan & GENG Xindu Institute of Modern Separation Science Shaanxi Key Laboratory of Modern Separation Science Northwest University Xi''''an China 《中国科学B辑(英文版)》2005,(Z1)
The renaturation of the denaturedα-chymotrypsin (α-Chy) with 1.7 mol·L-1 gua-nidine hydrochloride (GuHCI) by three kinds of stationary phase of high performance hydropho-bic interaction chromatography (STHIC) with a comparable hydrophobicity but different ligand structures was investigated. The obtained result indicates that the ligand structures of the three STHIC contribute to the renaturation efficiency ofα-Chy in the order of the end ligands PEG-600< phenyl group < tetrahydrofurfuryl alcohol (THFA). 相似文献
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Hong She Wang Wei Xing Zhao 《中国化学快报》2011,22(8):911-914
An efficient magnesium bistrifluoromethanesulfonimide[Mg(NTf_2)_2]catalyzed hydroalkylation of aromatic olefins with 1,3- diketones under solvent-free conditions has been developed.The reactions proceed smoothly to give the desired products in good yields in short reaction times. 相似文献
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The components of the rock, the pigments, the gold foils and the adhesive of One Thousand Hand Buddha in Dazu stone sculptures, Chongqing, China, have been analyzed by X-ray diffraction (XRD), X-ray fluorescence (XRF), infrared spectroscopy (IR), energy dispersive X-ray analysis (EDX) and fiber optics reflectance spectroscopy (FORS). Furthermore, the weathering and degeneration of One Thousand Hand Buddha have been discussed and the protective methods have been provided. In this work some useful information to study on conservation of stone relics is given. 相似文献
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<正>Two new eudesmane derivatives were isolated from the leaves and flowers of Verbesina virginica,along with the known 6-O-β-E -p-coumaroyl-4α-hydroxyeudesmane(1).Their structures were determined as 6-O-β-Z-p-coumaroyl-4α-hydroxyeudesmane(2) and 6-O-α-E-p-coumaroyl-1β-4α-dihydroxyeudesmane(3) by spectroscopic methods. 相似文献
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本文通过定义新的谱集,给出了算子满足a-Browder定理和a-Weyl定理的充要条件,运用了文章中新定义的谱集,研究了解析hyponormal算子的a-Weyl定理. 相似文献
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非交换Lipschitz-φ算子代数 总被引:4,自引:0,他引:4
本文引入由紧距离空间(K,d)到给定Banach代数A中的Lipschitz-φ算子构成的非交换Banach代数L~φ(K,A)与l~φ(K,A),证明了它们都是由K到A的全体连续算子构成的非交换Banach代数C(K,A)的子代数,并且关于范数||f||φ=L_φ(f)+||f||∞是Banach代数,研究了不同 Lipschitz尺度函数φ对应的大(小)Lipschitz代数之间的关系。特别当φ(t)=t~α时,引入了极限代数lim_(α→0+)l~α(K,A),lim_(α→+∞)l~α(K,A),lim_(α→0+)L~α(K,A)与lim_(α→+∞)L~α(K,A)以及距离空间的Lipschitz连通性,得到了lim_(α→+∞)l~α(K,A)=A的充要条件,也给出了lim_(α→0+)L~α(K,A)=C(K,A)的条件。 相似文献
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