排序方式: 共有26条查询结果,搜索用时 0 毫秒
1.
2.
Ghazali NF Patterson DA Livingston AG 《Chemical communications (Cambridge, England)》2004,(8):962-963
Organic solvent nanofiltration (OSN) was used to investigate the mechanism of chiral selectivity in diastereomeric salt formation of alpha-phenylethylamine with D-tartaric acid and di-p-toluoyl-D-tartaric acid as resolving agents; results indicate that for these systems chiral selectivity occurs only upon crystallisation and chiral interactions in solution were negligible. 相似文献
3.
Abdul Rohman Mohd AlIkhsan B. Ghazali Anjar Windarsih Irnawati Sugeng Riyanto Farahwahida Mohd Yusof Shuhaimi Mustafa 《Molecules (Basel, Switzerland)》2020,25(22)
Currently, the authentication analysis of edible fats and oils is an emerging issue not only by producers but also by food industries, regulators, and consumers. The adulteration of high quality and expensive edible fats and oils as well as food products containing fats and oils with lower ones are typically motivated by economic reasons. Some analytical methods have been used for authentication analysis of food products, but some of them are complex in sampling preparation and involving sophisticated instruments. Therefore, simple and reliable methods are proposed and developed for these authentication purposes. This review highlighted the comprehensive reports on the application of infrared spectroscopy combined with chemometrics for authentication of fats and oils. New findings of this review included (1) FTIR spectroscopy combined with chemometrics, which has been used to authenticate fats and oils; (2) due to as fingerprint analytical tools, FTIR spectra have emerged as the most reported analytical techniques applied for authentication analysis of fats and oils; (3) the use of chemometrics as analytical data treatment is a must to extract the information from FTIR spectra to be understandable data. Next, the combination of FTIR spectroscopy with chemometrics must be proposed, developed, and standardized for authentication and assuring the quality of fats and oils. 相似文献
4.
Shaeel Ahmed Al-Thabaiti Abdullah Yousif Obaid Ziya Ahmad Khan Tanweer Ahmad Arniza Ghazali Kabir-ud-Din 《Colloid Journal》2012,74(1):125-131
The energetics of clouding in anionic surfactant (SDBS) and tetrabutylammonium bromide system in the presence of additives,
such as ureas, amino acids and sugars is reported. The change of standard Gibbs energy of solubilization (ΔG
s
o) for all of the additives was found to be negative. The values of change of standard enthalpy (ΔH
s
o) and that of standard entropy (TΔS
s
o) values were found to depend on the type and chemistry of the additive. The results were explained on the basis including
chemistry of additives, their effect on water structure, and solubilization of additives either in the micellar or in aqueous
phases. 相似文献
5.
6.
Circular neighbor-balanced designs using cyclic shifts 总被引:3,自引:0,他引:3
In agriculture experiments, the response on a given plot may be affected by the treatments on neighboring plots as well as by the treatments applied to that plot. In this paper we consider such type of situations and construct circular neighbor-balanced designs (CNBDs) by the method of cyclic shifts or sets of shifts. An important feature of this method is that the properties of a design can be easily obtained from the sets of shifts instead of constructing the actual blocks of the design. That is, the off-... 相似文献
7.
E Okuyama M Homma Y Satoh H Fujimoto M Ishibashi M Yamazaki M Satake A B Ghazali 《Chemical & pharmaceutical bulletin》1999,47(10):1473-1476
From the extract of a Malaysian herbal medicine, Lemuni Hitam (Diospyros sp.), which exhibited monoamine oxidase (MAO) inhibition, three new naphthoquinone and/or naphthalene dimers (lemuninols A-C, 1-3) were isolated together with 4,6-dihydroxy-5-methoxy-2-methyl-naphthalene (8) and six known monomers (4-7, 9 and 10). The structures were determined by spectroscopic methods including 2D-NMR techniques. Among them, lemuninol A showed 45% inhibition of MAO (mouse liver) at 5.0 x 10(-6) g/ml, and lemuninols B and C and a naphthoquinone (9) indicated weak activity. Some related quinones were also tested for their MAO inhibitory activities. 相似文献
8.
9.
A reliable method for the measurement of different plasminogen activators is of great interest for both manufacturing and
clinical medicine. A one-step assay based on a thickness shear mode acoustic sensor has been developed for this purpose. Two
separate mixtures of substrates (fibrinogen and plasminogen) and enzymes (thrombin and the plasminogen activator) were mixed,
and placed on the acoustic sensor surface. During the assay, the resonant frequency of a quartz crystal oscillating in the
thickness shear mode was measured and used to find a characteristic clot dissolution time, from the sample addition to the
time at the maximum dissolution rate. Calibrations of the acoustic assay were done for tissue-type plasminogen activator (t-PA)
as well as for the other plasminogen activators: urokinase (u-PA); streptokinase (SK) and staphylokinase (SAK). All gave relative
standard deviations of about 12%. Since the same method was used for all of the activators, their activities were compared,
resolving the differences between their unit definitions. Linear relationships were found between urokinase and streptokinase
which activate plasminogen directly and between t-PA and staphylokinase which require fibrin as a cofactor. The relationship
between the groups was found to curve, indicating the difference between the two mechanisms. The acoustic method, therefore,
may be used as a rapid and cost-effective reference method for the standardization and comparison of different plasminogen
activators. 相似文献
10.
Stichopus hermanni and Stichopus vastus are sea cucumber species from the Stichopodidae family within the coastal waters of Malaysia. The integument of these invertebrates is hypothesised to contain abundant glycosaminoglycans (GAGs). GAGs are divided into non-sulphated and sulphated GAGs. Sulphated GAGs have various chemico-biological functions that are beneficial to humans. This study quantitatively analysed N-, O-sulphated and total sulphated GAG content from three different anatomical regions (integument, internal organs and coelomic fluid) of S. hermanni and S. vastus. The integument revealed the highest content of total, O- and N-sulphated GAGs, followed by the internal organs and the coelomic fluid for both species of sea cucumbers. The percentage division of O- and N-sulphated GAGs suggested that anatomical parts of both species showed higher levels of O-sulphated GAGs compared to N-sulphated GAGs. In conclusion, these findings indicate that the integument body wall of S. hermanni and S. vastus is a rich source of sulphated GAGs. 相似文献