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YAN Xiaomin ZHAO Lin SHAO Jianhui TAN Xin SONG Zhengxiao School of Chemical Engineering Technology Tianjin University Tianjin China Slichem Liquid Material Co. Ltd. Shijiazhuang China 《Chinese Journal of Reactive Polymers》2004,(Z1)
1. INTRODUCTION Methionine, namely 2-amido-4-thiomethyl butyric acid with a structure of CH3SCH2CH2CHCOOH, is one of the essential amino acids and has two natural enantionmers, D and L-methionine. The mixture of L- and D-isomers can be used as analeptics or nutritive additives to maintain the equilibrium of amino acids of feed [1,2]. L-methionine can release active methyl and accelerate the synthesis of choline, which further speeds up the conversion of the lipid accumulated in liv… 相似文献
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ZHANG Yifeng GUO Hong ZHANG Guangming YAN Xiuyun YIN Shougen ZHANG Zhengpu Institute of Taitai Pharmaceutical Co. Ltd Shengzhen China State Key Lab. of Functional Polymeric Materials for Adsorption Separation Institute of Polyme 《Chinese Journal of Reactive Polymers》2002,(1)
1. INTRODUCTION Fig.1 The Chemical Structure of Milupeinan As a new type of antibiotics Milupeinan, not only possesses antibacterial activities against a wide range of Gram-positive and Gram-negative bacteria, but also higgh stability under th… 相似文献
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ZhiQuanZHAO LiZengPENG YuLinLI 《中国化学快报》2005,16(3):290-292
The phenomenon of migration of the silyl groups from α-oxygen to β-oxygen in sodium aldol reaction was observed for the first time in this paper. 相似文献
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高温煤焦油的超临界萃取分馏研究 总被引:5,自引:0,他引:5
采用正戊烷溶剂,在超临界状态下,于220℃和5MPa~15MPa循序升压条件下,将高温煤焦油萃取分馏为10个液相窄馏分和1个固相沥青产物;切割深度达78.36%,萃余沥青收率为21.64%,明显低于常规蒸馏沥青收率。研究发现,所用高温煤焦油的初馏分萃取收率最高,随着萃取压力的增加,较低压力段一次萃取液相馏分的收率迅速减少;压力达到10 MPa,液相馏分总收率趋于峰值。元素分析和色质联用分析数据表明,随着萃取压力的增加,一次萃取获得窄馏分的碳氢原子比逐渐增加,平均环数和相对分子质量均逐渐增大,萃取馏分逐渐变重。 相似文献
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一种微型FAIMS传感器芯片的研制 总被引:1,自引:0,他引:1
基于微机电系统(MEMS)技术,研制了一种微型高场非对称波形离子迁移谱(FAIMS)传感器芯片.芯片尺寸为18.8mm×12.4mm×1.2mm,由离子化区、迁移区、离子检测区组成.采用真空紫外灯离子源在大气压环境下对样品进行离子化,经过离子化区中聚焦电极的电场作用,实现离子在进入迁移区之前的聚焦,提高离子信号的强度.通过在上下玻璃上溅射Au/Cr(300nm/30nm)金属,并与厚度为200μm、采用感应耦合等离子体(ICP)工艺刻蚀的硅片键合,形成迁移区的矩形通道,尺寸为10mm×5mm×0.2mm.离子检测区为三排直径200μm、间距100μm交错排列的圆柱阵列式微法拉第筒,能同时检测正负离子.采用频率为2MHz,最大电压为364V,占空比为30%的高场非对称方波电压进行FAIMS芯片实验.以丙酮和甲苯为实验样品,载气流速80L·h-1,补偿电压从-10V到3V以0.1V的步长进行扫描,得到了丙酮和甲苯的FAIMS谱图,验证了FAIMS芯片的性能.丙酮和甲苯的FAIMS-MS实验进一步表明FAIMS系统实现了离子分离和过滤功能. 相似文献
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绝对编码光栅的相位细分及其在位移测量中的应用 总被引:2,自引:1,他引:1
提出通过光栅条纹相位的精密测量,获取光栅高精度位移信息的方法。具体方法是对光栅图像采用多码道设计,用CCD二维图像传感器获取测量段光栅图像多码道信息。对最低码道图形的周期函数序列进行傅里叶变换、基频滤波和逆傅里叶变换获得光栅截断相位分布,其余码道信息提供相位展开的级次,以此获得测量段光栅的绝对相位分布。用光刻的手段制作了实用的绝对编码光栅,基元码道的尺寸是:27.36μm用于明条纹,27.36μm用于暗条纹,最小基元码道空间周期为54.72μm,光栅长度为14008.32μm。在步长近似3μm的位移测试中,与比对的标准仪器记录值比较,标准偏差为0.2057μm,精度在亚微米量级。重复性实验表明,位置测试的稳定性为0.09μm(标准差),得到600倍以上细分的分辨力。 相似文献
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Xue Jing Yanga Ya Ling Yang Wei Zhenb Mou Sheng Liua Jun Hong Chaia a Faculty of Life Science Technology Kunming University of Science Technology Kunming China b Kunming Fruit Business Economics Co.Ltd. Kunming China 《中国化学快报》2009,20(4)
An modified laminar crystal sodium silicate(A1-SKS-6) was synthesized by spray drying and high temperature crystallization using sodium silicate as silicon source,Al atom as inorganic source and hexadecyltrimethy ammonium bromide(CTMAB) as the structure template.The hydrothermal stability of product was at least 1 h.The synthesized material was characterized by XRD and SEM.The results indicated that shape and intensity of XRD diffraction peak at 2θtook changes,but raw materialδphase crystal form kept unc... 相似文献
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Ten coumarin derivatives containing(E)-methyl 2-(methoxyimino)-2-phenylacetate were synthesized and bioassayed.The compounds were identified by IR,~1H NMR and elemental analyses.The test results indicated that compound 5j(R~1 is methyl and R~2 is n-C_6H_(13)) was the optimal structure in this paper with good fungicidal activity against CDM(85%) at 6.25 mg/L concentration. 相似文献