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1.
Summary The essential oils of Estonian spruce and pine needles have been analysed by a combination of steam distillation/extraction, GC and GC-MS. According to their monoterpene composition Estonian pines belong to a high carene chemotype with monoterpenes representing up to 85% of total oil. Estonian spruce needle oil contains up to 70% of oxygenated terpenes and more limonene and 1,8-cineole than the same spruce species [Picea abies (L.) Karst.] from other localities.A total of 60 components were identified. Coefficients of variation describe the range of component contents in individual trees within the population. 相似文献
2.
A. Karnik S. Kailas A. Chatterjee P. Singh A. Navin D. C. Biswas D. M. Nadkarni A. Shrivastava S. S. Kapoor 《Zeitschrift für Physik A Hadrons and Nuclei》1995,351(2):195-198
The fission fragment angular distributions for the system12C +232Th have been measured in the energy range 0.97<>c.m./VB<1.22. the=" measured=" anisotropies=" have=" been=" compared=" with=" the=" predictions=" of=" the=" standard=" saddle=" point=" statistical=" model,=" using=" the=" second=" moment=" of=" the=" compound=" nucleus=" spin=" distribution=">1.22.>l2 deduced from a Wong model fit to the fission excitation function. While the measured anisotropies agree with the standard saddle point statistical model for Ec.m./VB>1.05, they are abnormally large at lower energies. This is also true for the existing measurements of16O and19F +232Th systems. Since for this system pre-equilibrium fission contributions are not expected, this anomaly indicates strong channel coupling effects leading to an increase in l2 at sub-barrier energies.The authors thank Drs. R.K. Choudhury and A. Saxena for useful discussions, Dr. R.J. Singh for making the thorium target and the Pellectron operation staff for excellent operation of the machine. 相似文献
3.
Kristin Lippur Cindy Elmers Tiiu Kailas Aleksander-Mati Müürisepp Tõnis Pehk 《合成通讯》2013,43(2):266-281
A general method for the synthesis of 5,5′-disubstituted bimorpholines is proposed. According to the method, methyl-substituted and benzyl-substituted compounds were synthesized, starting from tartaric ester acetal. Target compounds were obtained in good yield and high enantiomeric purity. 相似文献
4.
Kailas K. Sanap Rama S. Kulkarni Shriniwas D. Samant 《Journal of heterocyclic chemistry》2013,50(3):713-719
The thermal [4 + 2] cycloaddition reaction of 7‐substituted 4‐styrylcoumarins with N‐phenylmaleimide and tetracyanoethylene in nitrobenzene under reflux conditions rapidly gives 3,4‐annulated coumarins as the Diels–Alder adducts. The position of the surviving double bond was determined on the basis of NMR and supported by energies of the possible structures. The effects of the 7‐substituent and the solvent on the reaction were studied. 相似文献
5.
Tripathi V Navin A Mahata K Ramachandran K Chatterjee A Kailas S 《Physical review letters》2002,88(17):172701
Results for the cross section and average angular momentum for complete fusion at energies around the Coulomb barrier are presented for 7Li with 165Ho. Comparison of the cross sections with a one-dimensional barrier penetration model, using a potential consistent with the measured elastic scattering, showed a reduction above the barrier and an enhancement below it. An increase in the measured average angular momentum, , above the barrier and its consistency with that obtained from the fusion excitation function for weakly bound nuclei, is reported. These results together with a reanalysis of existing data conclusively demonstrate that the effect of breakup on fusion is coherent, like coupling to any nonelastic channel. 相似文献
6.
Ever since it was proposed more than three decades ago, the nuclear optical model has been very successful in interpreting
a large body of nucleon-induced nuclear reaction data in terms of a complex nucleon-nucleus potential. Rapid progress both
in the experimental measurements and the theoretical developments in the last two decades has led to a better understanding
of this nucleon-nucleus optical potential. From the parameter-fitting phenomenological stage, the optical model has come a
long way and it is now possible to calculate the nucleon-nucleus optical potential in a reasonable way starting from the fundamental
nucleon-nucleon interaction. Excellent reviews on various aspects of the optical model exist in the literature for proton
energies above 10 MeV. The present article is an attempt to review comprehensively the status of the proton-nucleus optical
potential at low proton energies, below the Coulomb-barrier, for target nuclei with mass numbers lying between 40 and 130.
The sets of phenomenological optical potential derived mostly from (p, n) reaction data are reviewed and their applicabilities discussed. The neutron-nucleus optical model is referred to wherever
it is relevant. Microscopic calculations for one case is carried out and compared with the corresponding phenomenological
values. 相似文献
7.
Light charged particles emitted in heavy-ion induced reactions, their spectra and angular distributions measured over a range
of energies, carry the signature of the underlying reaction mechanisms. Analysis of data of light charged particles, both
inclusive and exclusive measured in coincidence with gamma rays, fission products, evaporation residues have yielded interesting
results which bring out the influence of nuclear structure, nuclear mean field and dynamics on the emission of these particles. 相似文献
8.
L. Kailas 《Applied Surface Science》2006,252(19):6648-6651
Thin films of polystyrene (PS)/poly (methyl methacrylate) (PMMA) blends with different end groups were investigated using ToF-SIMS and AFM. PS with -OH and -NH2 end groups were blended in toluene solvent with pure PMMA homopolymer, and PMMA having anhydride end group. The ToF-SIMS spectra of PS-OH/PMMA resembled that of pure PS-PMMA blends showing an increase of PMMA intensity after annealing. On the contrary, the PS-NH2 blended with PMMA showed an increase in PS intensity on the surface after annealing. The ToF-SIMS spectra were similar to that of a pure PS-PMMA di-block copolymer. These results indicate copolymer formation at the surface. The PS-NH2 with PMMA-anhydride blend spectra showed very slight changes in spectra before and after annealing and the AFM images revealed spinodal bi-continuous structures on the surface before and after annealing. The copolymer formation is found to occur in the as-cast film itself and not after thermal treatment. 相似文献
9.
S Kailas A Navin A Chatterjee P Singh A Saxena D M Nadkarni D C Biswas R K Choudhury S S Kapoor 《Pramana》1993,41(4):339-344
The measurements of fission fragment angular distributions for the system19F+232Th have been extended to the sub-barrier energies of 89.3, 91.5 and 93.6 MeV. The measured anisotropies, within errors are
nearly the same over this energy region. However, the deviation of the experimental values of anisotropies from that of standard
statistical model predictions increases as the bombarding energy is lowered. 相似文献
10.