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排序方式: 共有1497条查询结果,搜索用时 31 毫秒
1.
2.
Sufficient conditions which guarantee that certain linear integro-differential equation cannot have a positive solution are
established. 相似文献
3.
I. Bretos J. Ricote R.J. Jiménez-Riobóo L. Pardo M.L. Calzada 《Applied Physics A: Materials Science & Processing》2007,89(4):967-973
A novel method to investigate the early formation stages of polycrystalline (Pb1-xCax)TiO3 (PCT) perovskite films by means of traditional Brillouin and micro-Brillouin spectroscopy (BS, mBS) is described in the present
work. The films were prepared by chemical solution deposition (CSD) onto oxidized (100)Si substrates and treated at temperatures
between 350–650 °C by rapid thermal processing (RTP). The elastic instability observed by Brillouin spectroscopy at the nano-structured
state of the PCT films was used here to determine their crystallization temperatures. Coexistence of different nanocrystalline
phases (e.g., pyrochlore, perovskite) in the films could also be detected by this technique. The reliability of these results
is demonstrated by complementary information obtained by X-ray diffraction (XRD) and scanning force microscopy (SFM). The
effects of the annealing temperature and of the Ca2+ content on the crystallization process of these films are also discussed.
PACS 78.35.+c; 77.84.-s; 61.82.Rx 相似文献
4.
5.
The bunching system of the ATLAS positive ion injector (PII) has been improved by relocating the harmonic buncher to a point
significantly closer to the second stage sine-wave buncher and the injector LINAC. The longitudinal optics design has also
been modified and now employs a virtual waist from the harmonic buncher feeding the second stage sine-wave buncher. This geometry
improves the handling of space charge for high-current beams, significantly increases the capture fraction into the primary
rf bucket and reduces the capture fraction of the unwanted parasitic rf bucket. Total capture and transport through the PII
has been demonstrated as high as 80% of the injected dc beam while the population of the parasitic, unwanted rf bucket is
typically less than 3% of the total transported beam. To remove this small residual parasitic component a new traveling-wave
transmission-line chopper has been developed reducing both transverse and longitudinal emittance growth from the chopping
process. This work was supported by the U.S. Department of Energy under contract W-31-109-ENG-38. 相似文献
6.
M. Alves Da Silva M. Helena Gil A. P. Piedade J. S. Redinha A. M. Oliveira Brett J. M. Caridade Costa 《Journal of polymer science. Part A, Polymer chemistry》1991,29(2):269-274
The immobilization of catalase on grafted membranes of poly(ethylene)-g-co-acrylic acid and poly(tetrafluoroethylene)-g-co-acrylic acid and their application in hydrogen peroxide electrochemical sensors is described. The introduction of carboxylic acid groups onto a hydrophobic support provides a good environment for subsequent enzyme immobilization. This single membrane, hydrogen peroxide sensor showed significant improvement with respect to the double membrane versions. The response is very rapid, the linear range being from 10 μM up to 6 mM, with a detection limit of 4.7 μM, and a lifetime of more than 4 months. 相似文献
7.
Inequalities of Nikolski
(Trudy Mat. Inst. Steklova 38 (1951), 2.3, p. 255) in L2πp, p 1, and of Oswald (Izv. Vyssh. Uchebn. Zaved. Mat. 7 (1976), (3.4), p. 71; Theorem 1, p. 69), 0 < p < 1, are extended to the case of Orlicz spaces L2π. 相似文献
8.
JiŘí Kvapil Josef Kvapil Bohumil Perner Michal Košelja Helena Jelínková 《Czechoslovak Journal of Physics》1990,40(11):1283-1287
The methods of growing YAG:Nd crystals with a flat interface and YAP:Nd crystals with a sharp conical interface are described. The form of the interface was controlled by the He and H2O content in the reducing atmosphere composed mainly of Ar and H2 as well as by axial temperature gradient above the melt level. The crystals of 120–180 mm in length were machined to the high-quality slabs. 相似文献
9.
Georgi E. Chernev Bisserka I. Samuneva Petar R. Djambaski Isabel M. M. Salvado Helena V. Fernandes 《Central European Journal of Chemistry》2006,4(1):81-91
In this work we present experimental results about the formation, properties and structure of sol — gel silica based biocomposite
containing Calcium alginate as an organic compound. Two different types of silicon precursors have been used in the synthesis:
tetramethylortosilicate (TMOS) and ethyltrimethoxysilane (ETMS). The samples have been prepared at room temperature. The hybrids
have been synthesized by replacing different quantitis of the inorganic precursor with alginate. The structure of the obtained
hybrid materials has been studied by XRD, IR Spectroscopy, EDS, BET and AFM. The results proved that all samples are amorphous
possessing a surface area from 70 to 290 m2/g. It has also been established by FT IR spectra that the hybrids containing TMOS display Van der Walls and Hydrogen bonding
or electrostatic interactions between the organic and inorganic components. Strong chemical bonds between the inorganic and
organic components in the samples with ETMS are present. A self-organized nanostructure has been observed by AFM. In the obtained
hybrids the nanobuilding blocks average in size at about 8–14 nm for the particles. 相似文献
10.
A. de la Hoz C. Pardo J. Elguero M. L. Jimeno 《Monatshefte für Chemie / Chemical Monthly》1992,123(1-2):99-104
Summary The reaction of tetracyanoethylene oxide on one hand and toluene, chlorobenzene, fluorobenzene, anisole, and nitrobenzene, on the other, has been studied. Toluene and the halogenobenzenes yield mixtures of monoadducts, anisole yieldp-methoxyphenylmalononitrile and its dimer and nitrobenzene does not react. These results are discussed with the help of a qualitative orbital model.1H-NMR analysis of some monoadducts has been carried out.
Der Benzolring als Dipolarophil: Reaktionen monosubstituierter Benzole mit Tetracyanoethylenoxid
Zusammenfassung Es wurden die Reaktionen von Tetracyanoethylenoxid mit Toluol, Chlorbenzol, Fluorbenzol, Anisol und Nitrobenzol untersucht. Toluol und die Halogenbenzole ergaben Mischungen von Monoaddukten, Anisol ergabp-Methoxyphenylmalononitril und sein Dimer, Nitrobenzol zeigte keine Reaktion. Diese Resultate werden mit Hilfe eines qualitativen Orbitalmodells diskutiert. Die Analyse einiger Monoaddukte erfolgte mittels1H-NMR-Analyse.相似文献