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1.
A room temperature ionic liquid, 1-pentyl-3-methylimidazolium bromide, [pmIm]Br efficiently catalyzes Michael addition of thiols and diethyl dithiophosphate to a variety of conjugated alkenes such as α,β-unsaturated carbonyl compounds, carboxylic esters, nitriles and chalcones without requiring any other organic solvent and catalyst. The ionic liquid can be recycled for subsequent reactions without any appreciable loss of efficiency. 相似文献
2.
E. V. McCloskey A. Dey R. M. Parr N. Aras A. Balogh J. Bostock A. Borell S. Krishnan G. Lobo L. L. Qin Y. Zhang S. Cvijetic V. Zaichick M. Lim-Abraham K. Bose S. Wynchank G. V. Iyengar 《Journal of Radioanalytical and Nuclear Chemistry》2004,259(2):341-345
In 1994, the International Atomic Energy Agency (IAEA) initiated a 5-year Co-ordinated Research Project (CRP) to determine
geographical and racial differences in peak bone mineral density (BMD) in men and women aged 15-49 years. The study demonstrates
that there are distinct global differences in BMD at the hip and spine in both men and women approximating to one population
standard deviation between populations with the highest and lowest BMD. These differences persist following adjustments for
age, sex and body size. Such information is valuable in understanding the reasons for global differences in fracture rate
and predicting future trends in fracture incidence.
This revised version was published online in August 2006 with corrections to the Cover Date. 相似文献
3.
This paper deals with the small-angle neutron scattering (SANS) investigation on solution-quenched PH13-8 Mo stainless steel.
From the nature of the variation of the functionality of the profiles for varying specimen thickness and also from the transmission
electron microscopy (TEM), it has been established that the small-angle scattering signal predominantly originates from the
block-like metallic carbide precipitates in the specimen. The contribution due to double Bragg reflection is not significant
in the present case. The single scattering profile has been extracted from the experimental profiles corresponding to different
values of specimen thickness. In order to avoid complexity and non-uniqueness of the multi-parameter minimization for randomly
oriented polydisperse block-like precipitate model, the data have been analyzed assuming randomly oriented polydisperse cylindrical
particle model with a locked aspect ratio. 相似文献
4.
5.
Summary The enzymes a-amylase, invertase and glucoamylase were immobilized on acid activated montmorillonite using two techniques,
viz. adsorption and covalent binding, and their activities were tested in a batch and packed-bed reactor and were compared. The
packed-bed reactor showed an improved performance for all immobilized enzymes, which was attributed to lowering of diffusional
restrictions to mass transfer. Lower activity in case of batch reactor for immobilized invertase was due to a combined effect
of loss of native conformation of enzyme on account of immobilization and mass transfer resistances due to improper diffusion
of substrate to the active site of enzyme. For immobilized glucoamylase, the packed-bed reactor demonstrated exceptionally
high activity that was very close to the free enzyme. Covalently bound glucoamylase showed higher activity than the free enzyme. 相似文献
6.
A four-noded rectangular element with seven degrees of freedom at each node is developed for buckling analysis of laminated plate structures having any number of layers with a constant thickness of individual layers. The displacement model is so chosen that it can explain adequately the parabolic distribution of transverse shear stresses and the non-linearity of in-plane displacements across the thickness. A geometrical stiffness matrix is developed using in-plane stresses. A wide range of plates from thick to thin are examined under uniaxial loading conditions. The results are compared with the existing analytical and numerical solutions. The present formulations confirm its applicability for buckling analysis of a wide range of plates. 相似文献
7.
8.
Within the framework of the covariant simultaneous approach of quantum field theory, a complex system of two identical scalar particles with third- and fourth-order self-action is examined. Explicit forms of the retarded component of the Green's two-time function and of the energy-dependent interaction operator of the system are obtained in the lowest orders of perturbation theory. Three-dimensional quasi-potential equations for the relativistic wave function of a bound state are derived. Based on the results obtained, a complex system of two Higgs bosons is examined. 相似文献
9.
Schwinger variational principle has been used to calculate triple differential cross-sections for ionization of hydrogen atoms
by positrons at intermediate and high energies for Ehrhardt type asymmetric geometry. The results agree in general with the
calculations of Brauneret al [8] and with the second Born calculation. 相似文献
10.
J. Pal C. C. Dey S. Bose B. K. Sinha M. B. Chatterjee D. P. Mahapatra 《Zeitschrift für Physik A Hadrons and Nuclei》1987,356(3):281-286
The analogue of the 0+ ground state in 118Sn has been observed in the compound nucleus 118Sb through 117Sn(p,n γ) 117Sb reaction. The neutron decays of this analogue resonance have been studied from the deexciting γ-rays of the residual nucleus 117Sb. From off resonance excitation functions, spin assignments have been made to states in 117Sb, on the basis of Hauser-Feshbach formalism. The resonance parameters of the isobaric analogue resonance have been determined, including the total, proton and neutron decay widths. 相似文献