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1.
The reaction of 2-(2 pyridytcarbonyl)benzoic acid with thionyl chloride affords an unexpected product of the intramolecular acylation of the pyridine nitrogen atom, namely, 6,11-dioxo-6,11-dihydrobenzo[blquinotizinium chloride. At the same time, 2-(2-quinotylcarbonyl)benzoic acid forms the expected cyclic acid chloride, namely, 3-(2-gitinotyl)-3-chlorophthalide in this reaction. Both compounds acylate ammonia and primary amines, including those with bulky alkyl groups (tert-butyl, 1-adamantyl, and 1,1,3,3-tetramethylbutyl) with the formation of 2-R-3-hydroxy-3-(2pyridyl- or 2-quinolyl)isoindolines. The protonation of the pyridine nitrogen atom of N-(1,1,3,3-tetramethylbutyl)-2-(2pyridylcarbonyl)benzamide, obtained in the open amide form, is accompanied by the closing of the isoindotinone ring; the deprotonation is accompanied by ring opening.Riga Technical University, Riga LV-1048. Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 4, pp. 499–504, April, 1994. Original article submitted March 17, 1994. 相似文献
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Ya. A. Éyubov 《International Applied Mechanics》1991,27(1):48-55
Azerbaidzhan Institute of Construction Engineering, Baku. Translated from Prikladnaya Mekhanika, Vol. 27, No. 1, pp. 55–64, January, 1991. 相似文献
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A. A. Afanas'ev V. M. Katarkevich A. N. Rubinov T. Sh. Éfendiev 《Journal of Applied Spectroscopy》2002,69(5):782-787
Spatial redistribution of microparticles in a suspension on exposure to the interference laser field depending on the parameters of the particles and the field characteristics has been analyzed theoretically. Results of experimental investigations are presented that illustrate the capture of an ensemble of polymeric small spheres and also of the lymphocytes of human blood and other microparticles in a liquid in the interference radiation bands of the He–Ne laser. 相似文献
7.
F. F. Éfendiev 《Mathematical Notes》1992,51(2):204-207
Translated from Matematicheskie Zametki, Vol. 51, No. 2, pp. 139–143, February, 1992. 相似文献
8.
Institut des Hautes Études Scientifiques 《Publications Mathématiques de L'IHéS》2004,100(1):271-282
Sans résumé 相似文献
9.
A multiparameter boundary-value problem of fresh infiltration water seepage in a drained fringe above quiescent saline water is solved in the direct statement and studied in detail. 相似文献
10.
Yu. G. Abov D. S. Denisov N. O. Elyutin S. K. Matveev Yu. I. Smirnov A. O. Éidlin F. S. Dzheparov D. V. L’vov 《Journal of Experimental and Theoretical Physics》1998,87(6):1195-1200
The asymptotic behavior of the spectra for large values of the scattering vector for the case of elastic multiple small-angle
neutron scattering (SANS) is investigated theoretically and experimentally. An expansion of the spectrum in terms of the reciprocal
of the magnitude of the momentum transfer is obtained taking account of the influence of the instrumental line. It is shown
that, to within some factor, the leading term of the expansion is identical to the differential single-scattering cross section
averaged over a statistical ensemble of particles; several subsequent terms in the expansion are calculated and the range
of applicability of the resulting expressions is determined. The asymptotic behavior of the multiple SANS spectrum is measured,
using a two-crystal neutron spectrometer, for samples of an HTSC ceramic, the alloy Fe-Ni, and Al powder. The agreement between
the experimental results and the theoretical predictions is analyzed.
Zh. éksp. Teor. Fiz. 114, 2194–2203 (December 1998) 相似文献