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Cycloaddition reactions between vinyl ethers 3 and -quinone methides 2, thermally generated from 2-hydroxybenzyl alcohols 1, have been studied. The structure and conformational preferences of the 4-substituted 2-ethoxy-(2,3)-dihydro-2-benzopyrans 4–9 obtained, which show new interesting features, are discussed together with competitive kinetic data. The cycloaddition process is concerted and involves -quinone methides in the -configuration. The OEt- transition state seems to be preferred with ethyl vinyl ether and -1-propenyl ethyl ether, whereas with -1-propenyl ethyl ether the stereoselectivity of the cycloaddition process depends on substituents on the methylene group of the starting alcohol 1. These results are discussed in terms of and preference of the propenyl ether methyl group. 相似文献
3.
Zhang Jiaqing Zhang Bosi Li Wenjie Ouyang Benhong Fan Minghao Wang Haoming 《Journal of Thermal Analysis and Calorimetry》2020,140(6):2749-2756
Journal of Thermal Analysis and Calorimetry - The burning process and typical fire parameters of power-cable silicon ointment were explored experimentally using a cone calorimeter, and the effects... 相似文献
4.
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Gianni Bosi Juan Carlos Candeal Esteban Induráin Esteban Oloriz Margarita Zudaire 《Order》2001,18(2):171-190
In the framework of the analysis of orderings whose associated indifference relation is not necessarily transitive, we study the structure of an interval order and its representability through a pair of real-valued functions. We obtain a list of characterizations of the existence of a representation, showing that the three main techniques that have been used in the literature to achieve numerical representations of interval orders are indeed equivalent. 相似文献
6.
A. Yildiz S. B. Lisesivdin S. Acar M. Kasap M. Bosi 《中国物理快报》2007,24(10):2930-2933
Resistivity and Hall effect measurements on n-type undoped Ga-rich InxGa1-xN (0.06 ≤ x ≤ 0.135) alloys grown by metal-organic vapour phase epitaxy (MOVPE) technique are carried out as a function of temperature (15-350 K). Within the experimental error, the electron concentration in Inx Ga1-x N alloys is independent of temperature while the resistivity decreases as the temperature increases. Therefore, Inx Ga1-xN (0.06 ≤ x ≤0.135) alloys are considered in the metallic phase near the Mort transition. It has been shown that the temperaturedependent metallic conductivity can be well explained by the Mort model that takes into account electron-electron interactions and weak localization effects. 相似文献
7.
K Kordatos T Da Ros S Bosi E Vázquez M Bergamin C Cusan F Pellarini V Tomberli B Baiti D Pantarotto V Georgakilas G Spalluto M Prato 《The Journal of organic chemistry》2001,66(14):4915-4920
We report the synthesis of three novel, versatile fullerene intermediates whose main feature is the presence of an amino end group. Simple condensation reactions of these intermediates under standard conditions produce new derivatives that are useful for applications in materials science and medicinal chemistry. 相似文献
8.
Summary A detailed experimental analysis of the inelastic crosssection along the [111]-direction in Co−Ni alloys is presented. Using
a simple model and studying the cross-section as a function of both composition and temperature, it is shown that interesting
information about the h.c.p.-f.c.c. transition can be gained in these alloys.
Riassunto Nel presente lavoro si describe un’analisi sperimentale dettagliata della sezione d’urto anelastica dei neutroni lungo la direzione [111] in leghe Co−Ni. Impiegando un modello relativamente semplice e studiando la sezione d’urto in funzione di temperatura e concentrazione, si mostra che si possono ottenere utili informazioni riguardanti la transizione h.c.p.-f.c.c.相似文献
9.
In this paper the continuous utility representation problem will be discussed in arbitrary concrete categories. In particular,
generalizations of the utility representation theorems of Eilenberg, Debreu and Estévez and Hervés will be presented that
also hold if the codomain of a utility function is an arbitrary totally ordered set and not just the real line. In addition,
we shall prove and apply a general result on the characterization of structures that have the property that every continuous
total preorder has a continuous utility representation. Finally, generalizations of the utility representation theorems of
Debreu and Eilenberg will be discussed that are valid if we consider arbitrary binary relations and allow a utility function
to have values in an arbitrary totally ordered set.
相似文献
10.
Anna Bosi 《Meccanica》2007,42(5):477-485
A wavelet-based methodology for detecting critical events in displacement and temperature histories, obtained by monitoring
in-situ thermoelastic structures, is proposed. It is based on the wavelet analysis of thermoelastic potentials furnishing
also the possibility to detect separately cases in which sudden jumps occur in the displacement history from those in which
they occur on temperature history. 相似文献