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Magnetostratigraphic studies of 112 cores specimens (249 samples) in a Precambrian-Cambrian section at Meishucun, Jinning County, Yunnan Province reveal the following: (ⅰ) Around the Sinian-Cambrian boundary in the Meishucun section existed a mixed polarity zone in which the Meishucun fauna went through an evolution of appearance—flourish—extinction. (ⅱ) The Meishucun section had a paleolatitude of no more than 20° during the Sinian-Cambrian, The phosphate deposits in this region and in the Zhongyicun Member were formed in the low-latitude environments. 相似文献
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建立了高效液相色谱-串联质谱同时测定猪肉中29种咪唑类药物及其代谢物残留的检测方法。样品采用乙酸乙酯提取,浓缩复溶后加入乙腈饱和正己烷净化除脂,以0.3%(体积分数)甲酸水溶液和乙腈为流动相,反相C_(18)色谱柱梯度洗脱分离,采用电喷雾正离子(ESI+)源多反应监测(MRM)模式进行检测。29种化合物在0.05~20.0μg/L范围内线性关系良好,相关系数r~20.99。在1.0~5.0μg/kg添加范围内,平均回收率为65.4%~103%,相对标准偏差(RSD)为1.3%~6.8%。方法检出限为0.02~0.3μg/kg,定量限为0.1~1μg/kg。该方法简便、快速、灵敏,适用于猪肉中咪唑类及其代谢物残留的检测。 相似文献
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