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固相配位化学反应研究——ⅩⅩⅩⅤ 热分解合成Co-N2配合物及其加氢性质研究 总被引:1,自引:0,他引:1
This paper reports the thermodecomposition of K3[Co(CN)5N3]·2H2O both in helium and hydrogen atmosphere with gas chromatography. The product in helium at 250℃ have been studied by IR, Raman, ESR and XRD. The dinitrogen complexes of K3Co(CN)5N2 and K6[Co2(CN)10N2] have been identified, and those dinitrogen complexes could be hydrogenized under hydrogen atmosphere to obtain ammonia. 相似文献
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