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The 230Ra has been produced via 232Th-2p reaction induced by 60 MeV/u 18O ion irradia-tion of natural thorium. The radium was radiochemically separated from the mixture of thorium andreaction products. Thin Ra sources in which 230Ac was got through 230Ra β- → 230Ac were pre-pared for observing fission fragments from β-delayed fission of 230Ac. The sources were exposedto the mica fission track detectors and measured by the HPGe γ detector. The precursor 230Ac wasidentified by means of observed two fission events as well as γ spectra, and the β-delayed fissionprobability of 230Ac was obtained to be (1.19±0.85) × 10-8. 相似文献
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为了考察常温、无氧下浸渍Na2CO3改性、原料气相对湿度对活性炭吸附硫化氢的促进作用,用动态吸附法分别测试了不同湿度下原活性炭和浸渍活性炭对低浓度硫化氢的吸附,同时考察了温度对该吸附过程的影响。结果表明,吸附平衡数据均符合Freundlich吸附等温方程。与原活性炭相比,浸渍活性炭的孔容和比表面积略有降低,但对硫化氢的吸附能力却显著提高,说明硫化氢与浸渍剂在活性炭表面上发生了化学反应。相对湿度增加,活性炭和浸渍活性炭对H2S的吸附能力均显著增强。温度升高,平衡吸附量均略有下降。 相似文献
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1-苯基-3-甲基-4-苯甲酰基-5-吡唑啉酮和磷酸三丁脂协同萃取镭的研究 总被引:2,自引:0,他引:2
用1-苯基-3-甲基-4-苯甲酰基-5-吡唑啉酮(PMBP)为萃取剂,苯为稀释剂,从pH5的水相中萃取^224Ra,发现^224Ra的萃取效率非常低。若往PMBP中加入少量的磷酸三丁脂(TBP),则会极大地提高镭的萃取效率,这说明TBP对PMBP萃取镭有显著的协同萃取效应。完成了萃取时间和反萃时间对^224Ra萃取效率的影响以及^224Ra萃取效率与TBP量之间的依赖关系等条件实验。 相似文献
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The basic process of an exotic decay mode namely β-delayed fission is simply introduced. The progress status of the study in the world is essentialized. The observation of β-delayed fission of 228Ac is reported. The radium was radiochemically separated from natural thorium. Thin Ra sources in which 228Ac was got through 228Ra →β-228Ac were prepared for observing fission fragments from β-delayed fission of 228Ac. They exposed to the mica fission track detectors, and measured by an HPGe γ-ray detector. The β-delayed fission events of 228Ac were observed and its β-delayed fission probability was found to be (5±2)×10-12. 相似文献
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189W activities were produced via the 192Os(n, α) reaction using irradiation of isotopically enriched 192Os metallic powder of ~100 mg/cm2 with 14 MeV neutrons. The X-γ and γ-γ coincidence measurements were made so as to obtain γ rays from 189W decay and its coincidence relations. A new simple decay scheme of 189W including three γ rays of 210.2, 229.6 and 260.2 keV is proposed. Two new levels of 189Re at 470.4 and 489.8 keV are assigned. 相似文献
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浸渍法制备了Na2CO3浸渍活性炭(IACⅠ)和一种高效脱硫剂(IACⅡ)。通过测定低质量浓度H2S在固定床上的穿透曲线,比较了原活性炭(AC)、IACⅠ和IACⅡ的脱硫效果。考察了原料气相对湿度,H2S质量浓度对穿透过程的影响。建立了固定床反应器一维轴向扩散模型模拟脱硫穿透曲线,并进行了数值求解。通过模型计算与实验测量穿透曲线拟合,确定了有效扩散系数等参数。结果表明,IACⅡ的脱硫效果最佳,其有效扩散系数较IACⅠ有所提高。提高相对湿度有利于增大硫容,但有效扩散系数略有降低。随着H2S入口质量浓度升高,有效扩散系数增大,穿透变快,硫容略有降低。 相似文献
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1-苯基-3-甲基-4-苯甲酰基-5-吡唑啉酮(PMBP) 萃取钍流程的改进 总被引:2,自引:1,他引:1
在用PMBP(1—苯基—3—甲基—4—苯甲酰基—5—吡唑啉酮)从14MeV中子照射过的天然U靶溶液中萃取Th流程的基础上,将萃取介质改为HNO3溶液,并将单次萃取—反萃改为两次萃取—反萃;在反萃溶液中加入I^-载体和:NaNO2溶液,在Fe(OH)3沉淀溶液中加入Br^-载体。用改进后的流程从60MeV/u^18O离子轰击天然U的:HNO3溶液中分离Th,从制得的Th样品的γ射线谱可以看出,该流程能去除绝大部分产物元素,特别是能完全去除溴和碘。 相似文献
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由14 MeV中子照射天然铂靶,通过^198Pt(n,α)反应产生^195Os.用γ(X)-γ符合方法搜索了^195Os的衰变γ射线,结果,没有找到可以属于它衰变的γ射线. 相似文献