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The spatial structures of magnetic Co nanowire array embedded in anodic aluminium membranes were investigated by grazing incidence small angle X-ray scattering (GISAXS) and conventional small angle X-ray scattering (SAXS) techniques. Compared with SEM observation, the GISAXS and SAXS measurements can get more overall structural information in a large-area scale. In this study, the two-dimensional GISAXS pattern was well reconstructed by using the IsGISAXS program. The results demonstrate that the hexagonal lattice formed by the Co nanowires is distorted (a ≈ 105 nm, b ≈ 95 nm). These Co nanowires are isolated into many structure domains with different orientations with a size of about 2 μm. The SAXS results have also confirmed that the nanopore structures in the AAM can be retained after depositing Co nanowires although the Co nanowires can not completely but only just fill up the nanopores. These results are helpful for understanding the global structure of the Co nanowire array. 相似文献
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以苯酐、顺酐、二丙二醇、丙二醇为主要原料,通过一步合成法得到不饱和聚酯,并以凝胶渗透色谱法(GPC)测量产品分子量和分子量分布。经探索发现本实验在醇过量10.9%、酸值为23.78~29.18 mg KOH/g、椎板粘度控制在10.25~15.50 Pa.s、反应时间32±2 h、反应温度204.5±0.5℃的条件下,可获得分子量分布较窄(分子量分布为1.17~1.18)的不饱和聚酯(分子量为4 000~4 500),为获得窄分子量分布的不饱和聚酯产品的合成条件的选择提供实践依据。 相似文献
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探讨了矩阵电位滴定法在不经分离的情况下测量钙镁含量的测量原理、方法和误差影响因素,并用该法对丙酮酸生产过程中,中间产品的钙镁离子含量进行测量,RSD(%)=2.01(Ca),RSD(%)=0.31(Mg)。 相似文献
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氧化铜(CuO)/氧化石墨烯(GO)复合材料中CuO的纳米结构起着至关重要的作用。本文通过在83℃下改变反应时间来控制CuO/GO复合材料中CuO纳米结构的形貌。采用红外吸收光谱、透射电子显微镜、X射线光电子能谱和小角X射线散射方法对样品进行了表征。反应时间0~560min,产生了3种不同纳米结构的CuO/GO复合材料。SAXS数据表明,在整个反应过程中较小粒径的CuO纳米粒子逐渐发生部分溶解。CuO/GO纳米颗粒形成过程是由CuO较高的过饱和度与CuO生长/溶解来驱动的。本实验工作将为制备不同形貌CuO/GO纳米复合材料提供一个可行的制备方法。 相似文献
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应用小角X射线散射技术研究了Cu60Zr30Ti10非晶合金从300到813 K之间微结构的演化情况.发现在淬火状态下Cu60Zr30Ti10非晶合金中存在直径30 nm左右的富Cu区.非晶的结构弛豫包括573 K之前的低温结构弛豫和573 K到玻璃转变温度的高温结构弛豫,弛豫的结果是产生含有有序原子团簇的富Cu区,这些有序原子团簇的富Cu区是随后晶化过程中晶核产生的基础.Porod曲线分析表明,晶化生成的纳米体心立方CuZr相和基体之间有明锐的界面. 相似文献
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Inorganic nanohybrid polyimide (PI) is widely applied in electrical and electronic devices for its outstanding insulating properties. Samples IOOCR and IOONH are made in Dupont. Among them, IOONH is a kind of pure PI films; however, IOOCR is a kind of inorganic nanohybrid PI films with excellent corona-resistance. The nanostructure of PI films is investigated with small-angle x-ray scattering technique and transmission electron microscopy (TEM). The normalized volume fractions of the scatterers in the specimens are obtained with a tangent-by-tangent data analysis for the small-angle x-ray scattering data. The multi-hierarchical scatterers of IOONH can be divided into two dominant components, i.e., the sharp component and the wide component. The sharp component is corresponding to the contribution of PI molecular chains, and the wide component includes the aggregates formed by PI molecular chains and the film has nested dual-fractal characteristics, nevertheless the IOOCR film possesses three types of scale scattering made up of inorganic nanoparticles, molecular chains and aggregates. The present films have multi-fractal structures. The distribution and structure of scattering body of two kinds of PI films are analyzed. The results of SAXS agree well with those of TEM methods. 相似文献