沉淀聚合制备粒径可控的温度响应型蛋白纳米胶囊

以牛血清蛋白(BSA)为模型蛋白,N-异丙基丙烯酰胺(NIPAM)为单体,N,N'-亚甲基双丙烯酰胺(BIS)为交联剂,采用原位沉淀聚合法制备了单分散的温度响应型蛋白纳米胶囊(nBSA).通过调整单体与蛋白的比例制备了粒径大小不同的含有单个蛋白分子的BSA纳米胶囊.采用基质辅助激光解吸电离飞行时间质谱仪(MALDI-TOF MS)、透射电镜(TEM)和动态光散射仪(DLS)等对BSA蛋白的修饰度,nBSA的形貌和结构,以及温度响应性能进行了表征,并用HeLa细胞对nBSA的体外安全性进行了初步评价.结果表明,在一定范围内,随着单体和蛋白比例的升高,蛋白纳米胶囊的粒径也逐渐增大,且在7.4～17 nm之间可控,而nBSA的响应温度则逐渐减小在33～41℃之间可控;制备的nBSA单分散性较好;nBSA具有温度响应性能,当环境温度高于其响应温度时,nBSA的粒径可显著增大16～33倍,且这种变化随温度呈现可逆性,并通过对nBSA细胞毒性的初步考察,评价将其用于生物领域的潜力.     

电动平移式喷灌机行走同步控制与仿真

 为避免大型平移式喷灌机传统试验中反复试验、改进造成的浪费及受季节、人力、物力等的制约,研究了大型平移式喷灌机行走控制系统在虚拟环境中的仿真和控制方法。对大型平移式喷灌机进行测绘,用Pro/Engineer建立三维仿真模型,用Multigen Creator软件建立三维虚拟农田场景。利用地面车辆力学理论,建立大型喷灌机的塔架车受力数学模型。在Visual C++ 6.0环境下,结合Multigen Vega软件,将三维喷灌机模型加载到虚拟场景中,对大型平移式喷灌机驱动系统和行走系统进行协同仿真。根据仿真实验结果,对大型喷灌机实体样机行走控制参数进行优化,并进行田间行走控制试验。仿真结果及田间试验表明,该系统能真实反映大型喷灌机在驱动电机作用下的行走状态。田间试验中,大型喷灌机能进行同步行走,相邻各跨之间的最大夹角误差为0.04°。     

The structural and magnetic properties of barium ferrite powders prepared by the solben gel method

In this paper, M-type hexagonal barium ferrite powders are synthesized using the sol-gel method. A dried precursor heated in air is analyzed in the temperature range from 50 to 1200 ℃ using thermo-gravimetric analysis and differential scanning calorimetry. The effects of the additives and the cacinating temperature on the magnetic properties are investigated, and the results show that single-phase barium ferrite powders can be formed. After heat-treating at 950 ℃ for 4h with 3 wt% additive, the coercivity and saturation magnetization are found to be 440 Oe and 57.9 emu/g, respectively.     

基于3S技术的银川平原湿地类型调查研究

以银川平原2004年丰水期中巴卫星影像为主要研究资料,建立银川平原湿地分类系统,并建立中巴影像的解译标志,利用遥感和地理信息系统技术相结合对银川平原湿地资源现状进行类型分布和面积调查。     

双氢青蒿素醚化法制备蒿甲醚的工艺优化

采用正交试验法和HPLC分析技术,对蒿甲醚的制备工艺进行优选,以蒿甲醚收率和含量为考察指标,对影响双氢青蒿素醚化的因素进行研究,其醚化的最佳条件为A2B3C4D1,即甲醇与二氯甲烷的体积比为1∶2;双氢青蒿素与三氟乙酸的量之比为10∶1;反应温度为40℃;反应时间为1.5h。该工艺稳定可行。     

大学生英语自主学习能力调查与分析

本文以问卷和访谈的形式，通过描述性统计和定量、定性分析，对300名非英语专业学生英语自主学习能力进行了调查研究。结果表明，大学生英语自主学习能力普遍较低。研究结果对大学英语教学改革有一定的启示。     

Development and application of ferrite materials for low temperature co-fired ceramic technology

Development and application of ferrite materials for low temperature co-fired ceramic(LTCC)technology are discussed,specifically addressing several typical ferrite materials such as M-type barium ferrite,NiCuZn ferrite,YIG ferrite,and lithium ferrite.In order to permit co-firing with a silver internal electrode in LTCC process,the sintering temperature of ferrite materials should be less than 950°C.These ferrite materials are research focuses and are applied in many ways in electronics.     

Enhancement of magnetic and dielectric properties of low temperature sintered NiCuZn ferrite by Bi2O3-CuO additives

With a series of 1.0 wt%Bi$_{2}$O$_{3}$-$x$ wt% CuO ($x =0.0$, 0.2, 0.4, 0.6, and 0.8) serving as sintering additives, Ni$_{0.23}$Cu$_{0.32}$Zn$_{0.45}$Fe$_{2}$O$_{4}$ ferrites are successfully synthesized at a low temperature (900 $^\circ$C) by using the solid state reaction method. The effects of the additives on the phase formation, magnetic and dielectric properties as well as the structural and gyromagnetic properties are investigated. The x-ray diffraction (XRD) results indicate that the added Bi$_{2}$O$_{3}$-CuO can lower the synthesis temperature significantly without the appearing of the second phase. The scanning electron microscope (SEM) images confirm that Bi$_{2}$O$_{3}$ is an important factor that determines the sintering behaviors, while CuO affects the grain size and densification. With CuO content $x=0.4$ or 0.6, the sample shows high saturation magnetization, low coercivity, high real part of magnetic permeability, dielectric permittivity, and small ferromagnetic resonance linewidth ($\Delta H$). The NiCuZn ferrites are a promising new generation of high-performance microwave devices, such as phase shifters and isolators.     

多层陶瓷LTCC带通滤波器设计

该文提供了一种基于低温共烧陶瓷(low temperature co_fired ceramic,LTCC)技术多层陶瓷微波带通滤波器的设计方法。首先通过ADS软件建立电路模型,使用4级UIR(uniformity impedance resonator)结构设计电路模型中的谐振结构,实现中心频率为625 MHz、带宽为50 MHz的带通滤波器。再使用Ansoft HFSS软件设计新型耦合结构,加强谐振级之间的耦合,进而降低通带内插入损耗(S21)和通带的波动,加强带外的抑制。最终实现了外形尺寸为5.0mm×5.0mm×1.5mm,插入损耗小于3.5dB,带宽为50MHz,带外70MHz处抑制大于40dB,带内波动小于1.0dB,电压驻波比(VSWR)小于1.5,且3 GHz内没有寄生的通带,中心频率为625 MHz较低频的带通滤波器。     

水利水电企业的营销战略

水利水电项目作为管理对象具有其整体性。一个水电企业就是一个整体,企业经营管理是指为达到工程项目的双赢目标,追求生产和营销的最大效益。文中以四川瓦屋山水电站为研究对象,结合本身的实践和认识,运用现代企业经营战略理论与分析方法,对水电企业的营销策略进行了系统的研究。