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在H2 + CH4 + C4H4S催化还原气氛中, 于300℃加热分解高能球磨后的前驱体(NH4)2MoS4. 用XRD, SEM, TEM, HRTEM, EDX和BET对反应产物进行了分析表征. 实验结果表明反应产物是多壁的MoS2纳米管, 它们的长度可达3~5 mm, 内径约为15 nm, 外径约为30 nm, 层间距为0.62 nm. 实验测定了MoS2纳米管N2吸/脱附等温曲线及孔径大小分布. 这种低温催化热反应对该类纳米管的规模制备有着十分重要的意义. 相似文献
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过渡金属硫族化合物纳米管的研究进展 总被引:1,自引:0,他引:1
主要介绍了过渡金属硫族化合物MX2(M=Mo,W,Nb,Ta,Ti,Zr,Hf,Re;X=S,Se)纳米材料的研究进展,综述了该类无机富勒烯纳米管的制备、生长机理及应用。由于该类纳米管包含金属与非金属组成,有别于单一成分的碳纳米管,其在原子探针、催化、储氢、储锂等方面的应用前景广阔。 相似文献
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开口WS2纳米管的制备与表征 总被引:2,自引:0,他引:2
在氢气与噻吩的催化还原气氛中,于400℃加热分解高能球磨后的前驱体(NH4)2WS4.用粉末X射线衍射(XRD),扫描电子显微镜(SEM),高分辨透射电子显微镜(HRTEM)和N2吸附比表面测定(BET)对反应产物进行了分析表征.结果表明反应产物是高纯度多壁的开口WS2纳米管,其平均长度为5μm,内径约为15nm,外径约为30nm,层间距为0.62nm.对于反应过程,提出了WS2纳米管“由内向外”的生长机理. 相似文献
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The ball-milled mixture of Ti and Se powders was carried out a solid-phase reaction at 600℃.The asprepared sample had been characterized by X-ray diffraction(XRD),scanning electron microscopy(SEM),transmission electron microscopy(TEM)and high-resolution transmission electron microscopy(HRT EM).The result shows that the products are multiwalled TiSe2 nanotubes with open-ended tips,which are about 15nm in outer diameter,several micron in lengths,and 0.6nm of interlayer spacing. 相似文献
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Since the first report on inorganic fullerene-like WS2 polyhedra and nanotubes by Tenne et al.[1] in 1992, this kind of nanostructural materials have become extensive research topics owing to their unique electronic structures. WS2 and MoS2 nanomaterials have shown potential applications in the fields of scanning probe microscopy[2], solid-state lubrication[3], heterogeneous catalysis[4], and electrochemical hydrogen storage[5]. Up to now, a great deal of progress has been achieved in the st… 相似文献
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