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氮化物颗粒补强石英基复合材料的制备和性能研究 总被引:7,自引:0,他引:7
热压制备了氮化物颗粒补强石英基复合材料,研究了氮化物颗粒的引入对石英基复合材料力学性能、介电性能和热学性能的影响.结果说明,氮化物颗粒的引入对石英基复合材料的力学性能有显的补强增韧作用;介电损耗在指标值以内,且随测试温度变化不大;以AlN为第二相的石英基复合材料其临界热震温差在600℃左右,复合引入AlN Si3N4时复合材料的热学性能无明显改善,而复合引入AlN BN使复合材料的临界热震温差提高到1000℃.复合引入AlN BN的石英基复合材料因为有着较好的力学性能、介电性能和热学性能等综合性能而有望用作天线窗材料。 相似文献
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合成了染料中间体2-甲基-3-磺酸丙基-取代苯并噻唑氢氧化物内盐Ⅰ_(a-f)及2-磺酸丙硫基-3-磺酸丙基苯并噻唑氢氧化物内盐Ⅱ,由Ⅰ与Ⅱ在三乙胺的催化下缩合制得-甲川噻菁染料Ⅲ_(a-f);初步研究了Ⅲ_(a-f)的结构与其在甲醇中最大吸收的关系。 相似文献
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Low-frequency internal friction (IF) of SrBi2Ta2O9(SBT) ceramics has been measured at temperatures ranging from 293 to 623 K. Two IF peaks, with their locations around 393 K (P1) and 569 K (P2) (f≈1.58 Hz), respectively, are observed. P1 is found to be associated with a relaxation process with activation energy of 0.97 eV and pre-exponential factor of 3.58×10-14 s. Peak shape analyses reveal that P1 can be well described by a broadened Debye peak with the width parameter β from 2.70 to 2.92. The mechanism responsible for P1 is proposed to be relaxation of oxygen vacancies near domain walls(DWs). P2 is considered to arise from viscous motion of DWs since it shows characteristics of static hysteresis type. Comparisons for the IF behavior between SBT and Pb(Zr, Ti)O3(PZT) suggest that in SBT oxygen vacancies are much less localized near DWs than that in PZT. This result provides a possible explanation for the weak DW pinning due to oxygen vacancies in SBT. 相似文献
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报道了7种属于半菁染料的苯乙烯噻菁染料的合成及紫外可见光谱研究。发现在甲醇溶液中,取代基对吸收光谱具有一定的影响。 相似文献
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Six Q-1 peaks in freshly-worked PbNb2O6 ceramics are observed by low-frequency internal friction measurement so far as we know for the first time. P1, P2, and P4 appear at the first heating process with remarkable shear modulus anomalies. But they are not observed during the cooling process or in the well-annealed samples. Those peaks are considered to be related with the working processes. P3 is a widened Debye relaxation peak in nature. The activation energy and pre-exponential factor are about 1.01 eV and 2.5×10-12 s, respectively. This peak is attributed to the interaction of domain walls and oxygen vacancies. P6 is corresponded with the paraelectric and ferroelectric phase transition. P5, appearing near Tc, is thought to be caused by the viscous movement of the domain walls. 相似文献
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在单晶硅表面通过多步化学反应共价键合多种菁染料,对它们的XPS分析表明,单晶硅表面存在着与各单体染料组成相同的化学元素及化学环境,并由有关元素结合能的分析证明它们是通过硅氮键键合于单晶硅表面上的。 相似文献
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报道了7种属于半菁染料的苯乙烯噻菁染料的合成及紫外可见光谱研究。发现在甲醇溶液中,取代基对吸收光谱具有一定的影响。 相似文献