Quasielastic Scattering of the Halo Nucleus ^6He at 25 MeV／u from a ^9Be Target

The differential cross sections of quasielastic scattering of a 25 MeV/u ^6He from ^9Be target have been measured.The double-folding model approach is applied to generate the real part of the optical potential. The imaginary potential parameters as well as some of the real potential parameters are studied in comparison with the experimental data. The effect of the unstable nucleus is discussed.     

用相位调制方法测量光盘盘基应力双折射的精度分析

偏振相位调制方法是测量微小双折射的一种高精度检测方法。本文系统全面地分析了以ＰＭＣＳＡ结构形式测量光盘盘基应力双折射的相位调制方法中，由各种误差源造成的对测试结果的影响。     

Development of an RPLC-based Method for Measurement of Indoprofen Stability and Validation of the Method

A method for quantitative measurement of the photochemical decomposition of the anti-inflammatory agent, indoprofen （INP） is descriped. An RPLC-based assay that could determine the extent of degradation of INP in a rapid, sensitive, and accurate manner was developed. The method was validated under photoirradiation. Quantitation was monitored with an Inertsil ODS-3V column using a mobile phase of acetonitril and 1% HOAc solution in deionized H2O. Statistics relevant to the system criteria, peak integrity and resolution among the parent drug and its degradation products were performed. From the intra- and inter-day tests, the coefficients of variation were found to range from 0.59% to 4.25% for the former and from 0.71% to 4.86% for the latter. The good selectivity and specificity of this RPLC-based procedure render it suitable for measurements of INP stability.     

人尿中异黄酮的高效液相色谱分析

建立了测定人尿中异黄酮组分(大豆苷原、黄豆黄素、雌马酚、染料木黄酮)含量的反相高效液相色谱法。在尿样中加入黄酮作为内标,异黄酮经酶解后在pH=7.0中性条件下用乙酸乙酯(1∶1)提取,然后用0.02%TFA-M eOH-ACN三元梯度洗脱的方法分离异黄酮。在该条件下,大豆苷原、黄豆黄素、雌马酚、染料木黄酮的检出限分别为12.9 nmol/L、13.9 nmol/L、71.6 nmol/L和11.8 nmol/L;回收率均在89%以上。本方法具有测试步骤简单、准确度高、重现性好等优点,适合大批量样品测定。     

钴配合物的合成晶体结构及活性研究

The complex [Co₂Cl₂(EGTB)]·(ClO₄)₂·5H₂O was synthesized in methanol-aqueous solution and its crystal structure was determined by X-ray diffraction method. The crystal belongs to monoclinic with space group of P2₁/c. The cell parameters are a=1.42231(2)nm,b=2.53181(3)nm,c=1.43392(2)nm,β=102.0518(5)°, Z=4, F(000)=2360,D_c=1.508g·cm^-3, The final R=0.0788,wR₂=0.232, The catalytic rate constant of the dismutation of superoxide radicals has been obtained by means of photo reduction of nitroblue tetrazolium(NBT),and it is 1.875×10⁶mol^-1·L·s^-1.     

分光光度计测铁矿石中钛的测量不确定度评定

紫外-可见分光光度计在化学分析中应用较为广泛。对于借助其进行化学分析测量不确定度的评定，目前较多见于溶液测定。实际应用中，测试样品多为固体，涉及到称样、溶解、稀释、定容等步骤。此文试从随机效应和系统效应的角度考虑，对紫外-可见分光光度计应用ISO4691：1985铁矿石中钛含量的测定——二安替比林甲烷分光光度法对铁矿石中钛的测量过程中的不确定度来源进行了较为全面的分析，并最终给出评定结果。     

纳滤膜处理镀铬废水的实验研究

以重金属回收和废水回用为目的，研究了纳滤膜处理镀铬废水。本文讨论了操作压力、膜通量、CrO4^2-离子浓度以及浓缩过程等影响。由实验结果可知，操作压力对CrO4^2-离子的截留率影响较大，而CrO4^2-离子浓度以及浓缩过程的影响较小。在低压和废水浓度较低的情况下，CrO4^2-的截留率可达99％以上，从而实现了镀铬废水分离处理，并达到了回用目的。     

园林绿化在城市建设中发展对策研究

随着园林工程建设规模的扩大,在城市建设中的作用越来越大,所以需要对发展中的对策需要进行研究。本文介绍了园林绿化在城市建设中的重要性及作用的体现和园林绿化的发展前景等。     

静电纺丝小口径人工血管支架材料的制备及其抗凝血性能的初步评价

首先合成催化体内一氧化氮供体(RSNO)释放一氧化氮(NO)的铜离子络合物(Cu(Ⅱ)-DTTCT),然后以Cu(Ⅱ)-DTTCT和具有良好生物相容性的高分子聚合物—聚己内酯(PCL)为原材料,利用静电纺丝技术制备小口径人工血管支架材料.结果表明,采用物理共混方式制备的支架材料尽管具有良好的催化性能,但存在突释现象和不同程度的细胞毒性.为了解决这一问题,选取较低细胞毒性的催化剂用量,以同轴电纺方式制备出以催化剂Cu(Ⅱ)-DTTCT和PCL为芯,以PCL为壳的具有芯壳结构的小口径人工血管支架材料,并对它的抗凝血性能进行了初步评价.这种芯壳结构支架材料在一定程度上能够控制NO释放速率,很好地解决了突释现象,并且不具有明显的细胞毒性.     

护专生化学思维能力的培养途径分析

本文从护专生的特点及学生对医学化学学习的畏难情绪入手,分析如何教会学生科学的思维方法,培养学生运用化学思维去发现和解决实际问题,增强学生的学习兴趣,克服怕学化学的畏难情绪,锻炼学生的思维能力。