THE POLYMERIZATION OF EPICHLOROHYDRIN WITH Nd(i-oPr)_3-Al(i-Bu)_3 SYSTEM

Epichlorohydrin (ECH) was polymerized with a rare earth catalytic system: Nd (i-OPr)_3-Al (i-Bu)_3. The effects of Al/Nd molar ratio, solvents, the polymerization time and temperature,the aging time and temperature of the catalyst preparation were studied. The results showed thatat a low Al/Nd molar ratio (4) of the Nd(i-OPr)_3-Al(i-Bu)_3 system ECH polymerized at a lowtemperature (248K) with a high conversion. The average molecular weight ofpolyepichlorohydrin (PECH) ranged from 1×10~5 to 3×10~5.     

天然商陆色素稳定性研究

从商陆科植物商陆(Phytohcca acinosa Roxb)浆果中提取一种紫红水溶性色素。在不同理化条件下对该色素进行了研究，结果表明，该色素在pH3-5范围先稳定性，热稳定性好，氧化剂有一定影响，糖无不良影响，对部分金属离子具有敏感褪色作用，毒性实验表明安全，对某些疾病具有一定的治疗作用。     

离子色谱法在中药化学成分分析中的应用进展

离子色谱作为一种新型高效液相色谱技术,最初主要应用于测定样品中的阴阳离子含量,如今发展为应用于有机酸、生物胺、糖类等化合物的组成及含量测定.离子色谱法具有操作简便、灵敏度高以及选择性好等优点,因此,目前离子色谱法已在能源、环境、地质、食品、药物等领域得到了广泛应用.总结了近年来离子色谱在中药金属离子、无机阴离子、有机酸、糖类成分的研究进展,为离子色谱法分析中药化学成分提供了参考.     

中兴煤矿3211工作面调整通风系统设计方案

概述了3211综采工作面调整设计方案,阐述了施工技术要求,介绍了3211第6联巷和第7联巷施工永久密闭的安全技术措施以及3211综采工作面调整系统后的通风布置及各用风点布置情况。     

气提式内循环好氧反应器及其产业化研究

本研究试图设计一种处理有机废水效率高、运行成本低、并可产业化的"气体式内循环好氧反应器"。其原理是利用好氧处理时供给的空气,对有机废水进行"气提,"在反应器中产生强烈的循环,使好氧微生物与废水中的有机物进行充分接触,达到提高氧的利用率、减少水力停留时间的目的。     

思想政治教育工作的经济学方法透析

经济属性是人的系统属性中的基本属性之一,在思想政治教育工作实践中要正视人的经济属性。对思想政治教育的投入将会产生两种效益,即社会效益和经济效益。思想政治教育的投入也是一种风险投入,产生良好效果的为有效投入,未产生良好效果的为无效投入,这就要求我们切实提高思想政治教育投入的针对性和有效性。在思想政治教育工作中同样存在一个市场供给与需求的关系问题:思想政治教育产品供给过度就会造成浪费或效率递减;思想政治教育对象的层次性决定了产品需求的多样性;精神产品具有物质属性和精神属性,其物质属性决定它必须受到经济规律的制约;思想政治教育产品既要满足社会需求,又不能忽略市场需求,既要重视产品的政治性特点,又要关注产品的经济性特征。     

Analysis of superconducting cavity quench events at SSRF

Quench is important and dangerous to superconducting RF cavities. This paper illustrates the mechanism of quench and how a quench detector works, and analyzes the quench events happening during beam operations and cavity conditioning. We find that the quench protection is mostly triggered by some reasons such as fluctuation of cavity voltage, multipacting or arc, rather than a real cavity thermal breakdown. The results will be beneficial to optimize the operation parameters of superconducting cavities, to discover the real reasons for beam trip by quench interlock, and to improve the operation stability of superconducting RF systems.     

Design of a higher harmonic cavity for the SSRF storage ring

Higher harmonic cavity used in the third generation synchrotron light source increases the Touschek lifetime. The higher harmonic cavity of Shanghai Synchrotron Radiation Facility (SSRF) is a 1.5GHz passive superconducting cavity. Its higher order modes (HOM) are extracted by a ferrite HOM damper out of the cryostat. Multi-cell cavity is chosen concerning the voltage. The harmonic cavity dynamics, beam dynamics with passive harmonic cavity and the design of single cell cavity are included in this paper.     

Digital prototype of LLRF system for SSRF

This paper describes a field programming gate array (FPGA) based low level radio frequency (LLRF) prototype for the SSRF storage ring RF system. This prototype includes the local oscillator (LO), analog front end, digital front end, RF out, clock distributing, digital signal processing and communication functions. All feedback algorithms are performed in FPGA. The long term of the test prototype with high power shows that the variations of the RF amplitude and the phase in the accelerating cavity are less than 1% and 1° respectively, and the variation of the cavity resonance frequency is controlled within ±10 Hz.