全文获取类型
收费全文 | 99篇 |
免费 | 5篇 |
国内免费 | 2篇 |
专业分类
化学 | 65篇 |
晶体学 | 1篇 |
力学 | 2篇 |
数学 | 3篇 |
物理学 | 21篇 |
无线电 | 14篇 |
出版年
2023年 | 5篇 |
2022年 | 7篇 |
2021年 | 9篇 |
2020年 | 10篇 |
2019年 | 5篇 |
2018年 | 2篇 |
2017年 | 6篇 |
2016年 | 5篇 |
2015年 | 5篇 |
2014年 | 4篇 |
2013年 | 4篇 |
2012年 | 4篇 |
2011年 | 2篇 |
2010年 | 3篇 |
2009年 | 3篇 |
2008年 | 3篇 |
2007年 | 2篇 |
2006年 | 4篇 |
2005年 | 6篇 |
2004年 | 1篇 |
2003年 | 3篇 |
2002年 | 2篇 |
1999年 | 1篇 |
1998年 | 1篇 |
1996年 | 1篇 |
1993年 | 1篇 |
1985年 | 1篇 |
1984年 | 2篇 |
1983年 | 2篇 |
1981年 | 1篇 |
1980年 | 1篇 |
排序方式: 共有106条查询结果,搜索用时 15 毫秒
1.
M. Wasim 《Journal of Radioanalytical and Nuclear Chemistry》2007,272(1):61-67
A database has been designed for storing, retrieving and analyzing information about samples, experimental conditions and
results obtained by neutron activation analysis and gamma-ray spectrometry. It has been created using Microsoft ACCESS 2002
under a Windows operating system. The database has been designed not only for saving information but also for quality assurance
and quality control purposes. The structure of the relational design has been discussed and demonstrated with a new graphical
feature of ACCESS 2002 called PIVOTCHART. 相似文献
2.
The unusual selectivity of a methylene succinic (itaconic) acid modified polymeric column was investigated for the separation of alkali, alkaline earth, transition and heavy metals employing non-chelating inorganic eluents. The retention of selected metal ions on the column was investigated with simple HNO3 eluents and eluents prepared from KNO3 and KCl salts of varying pH (adjusted using HNO3). From these studies both the effect of eluent ionic strength and pH upon retention was evaluated for the itaconic acid stationary phase. The results obtained showed that despite slow exchange kinetics causing poor efficiencies, acceptable baseline separations of selected alkaline earth and transitions could be obtained under optimum conditions (the baseline separation of Mg(II), Ca(II), Mn(II), Cd(II), Zn(II) and Co(II) was possible using a 15 mM KNO3-5 mM KCl eluent at pH 3.50 in under 25 min). The use of an simple ionic strength step gradient was shown that facilitated the addition of Pb(II) to the above group of metal ions. An investigation into the effect of temperature upon peak efficiency and retention showed increased column temperature could be used to improve the resolution of closely eluting metal ions such as Ca(II) and Sr(II) and Ca(II) and Mn(II). 相似文献
3.
G. Marin S. M. Wasim G. Sánchez Pérez P. Bocaranda A. E. Mora 《Journal of Electronic Materials》1998,27(12):1351-1357
A new method to grow single crystals with stoichiometry close to 1:1:2 of CuInTe2, an important member of the Cu-III-VI2 family of semiconductors is described. This consists of tellurization in the liquid phase of stoichiometric Cu and In and
later solidification under directional freezing. It is found from energy dispersive spectroscopy that the ingots obtained
with the evaporation temperature (Tt) of Te at 590 and 635°C were very close to the ideal stoichiometry 1:1:2. Samples of all ingots obtained with Tt between 530 and 690°C, as studied by x-ray and differential thermal analysis, were of single phase having chalcopyrite structure
and p-type conductivity. Optical and electrical characterization of different ingots were made. The acceptor ionization energy
EA and the density of states effective mass m
p
*
of the holes are estimated from the temperature dependence of the hole concentration p in samples of different ingots. m
p
*
= (0.78 ± 0.02) me agrees quite well with the reported value. From a combined analysis of the variation of EA with p1/3 and the knowledge of molecularity and valence stoichiometry of each sample, it is established that the shallow acceptor level
observed in different samples with EA (0) ⋍ 30 meV is due to VIn. 相似文献
4.
Wang Haoran Wasim Akhtar Lalit Mohan Nainwal Sumit Kumar Kaushik Mymoona Akhter Mohammad Shaquiquzzaman Mohammad Mumtaz Alam 《Journal of heterocyclic chemistry》2020,57(9):3350-3360
Thirteen new benzimidazole pendant cyanopyrimidine derivatives were synthesized. The compounds were synthesized through multistep reaction protocol. The structures of synthesized derivatives were studied by EI-MS, 1H NMR, FT-IR and elemental analysis. All the compounds were studied for their anticancer activity at National Cancer Institute. Except compound 7j , all the compounds unveiled cytotoxicity against cancer cells. The most active compound 7a had shown highest value of growth inhibition of 88.44% and 84.19% against HOP-92 and T-47D cancer cell lines. 相似文献
5.
6.
Nasir Khalid Mohammad Wasim Nadeem A. Lodhi Mohammad Arif 《Journal of Radioanalytical and Nuclear Chemistry》2013,297(1):153-159
Certified alloys of Ni–Cu based, Fe based and Cu–Sn based were analysed by semi-absolute, standardless k 0-instrumental neutron activation analysis (k 0-INAA) and flame atomic absorption spectrophotometry (FAAS) aiming at evaluating their comparative performances. In k 0-INAA measurements, the irradiations were performed at miniaturized neutron source reactor having thermal neutron flux of about 1 × 1012 cm?2 s?1. The experimentally optimized parameters for INAA suggested a maximum of three irradiations for the quantification of 21 elements within 5 days. The same experiments also produced quantitative results of 13 elements not reported in the certificates of the reference materials. AAS was, however, unable to determine any of those elements. Accuracy of the two techniques was assessed by comparing their average root mean squared errors. The data analysis concluded that k 0-INAA had better sensitivity and accuracy than FAAS. 相似文献
7.
Iron Oxide Supported on Al2O3 Catalyst for Methane Decomposition Reaction: Effect of MgO Additive and Calcination Temperature 下载免费PDF全文
Ahmed S. Al‐Fatesh Anis H. Fakeeha Ahmed A. Ibrahim Wasim U. Khan H. Atia R. Eckelt Biswajit Chowdhury 《中国化学会会志》2016,63(2):205-212
Production of hydrogen is a challenging task and have significant impact in the recent scenario. The alumina supported iron oxide nanoparticle synthesized using non‐ionic surfactant Triton‐X was found very effective for steady production of hydrogen through methane decomposition reaction. The high surface area, easily reducible catalyst calcined at 500 °C and 800 °C temperature showed steady activity towards methane decomposition reaction. At a higher reaction temperature there was catalyst deactivation. The doping of MgO facilitated particle growth rendering the poor catalytic activity. The TPR study showed that reducibility of TPR was difficult in presence of MgO additive. The formation of Fe? Mg? Al solid solution confirmed by XRD study was found mainly responsible for the lower catalytic activity. The bamboo‐shaped carbon nanotube formed from 20 % Fe/Al2O3 catalyst which is mainly because of the poor wetting property of quasi‐liquid metal and carbon nanotube. 相似文献
8.
Habib-ur- Rehman Akbar Ali Jamil Anwar Wasim Yawar 《Journal of Radioanalytical and Nuclear Chemistry》2006,267(2):421-425
Summary The synergistic mixture comprising picrolonic acid (HPA) and benzo-15-crown-5 (B15C5) in chloroform has been used for the
extraction of Ce(III), Eu(III) and Tm(III) as representatives of lanthanide(III) ions from pH 1-2 solutions having ionic strength
of 0.1 mol. dm-3(K+/H+, Cl-). The composition of the extracted species has been determined as M(PA)3. nB15C5 where M is Ce, Eu and Tm and n=1 or 2. The influence of various anions and cations on the extraction of these ions has also been studied and only oxalate,
cyanide and tartrate have some deleterious effect. The extraction equilibrium constants have been evaluated and discussed. 相似文献
9.
10.
有源滤波电路设计总结 总被引:1,自引:0,他引:1
滤波器是一种能使有用信号通过而大幅抑制无用信号的电子装置。在电子电路中常用来进行信号处理、数据传输和抑制噪声等。在运算放大器广泛应用以前滤波电路主要采用无源电子元件--电阻、电容、电感连接而成,由于电感体积大而且笨重导致整个滤波器功能模块体积大而且笨重。本文介绍由集成运算放大器、电阻和电容设计有源滤波器,着重讲解低通、高通、带通滤波电路。 相似文献