Some Reactions of 5-(3 or 4-Pyridyl)-1,3,4-Oxadiazoles with Amines and Hydrazines

2-Amino-and 2-hydrazino-5-(3 or 4-pyridyl)-1, 3, 4-oxadiazoles [II_i-k] have been prepared by racting 2-chloro derivatives with the corresponding amines or hydrazines, the 2-hydrazino (II_i-k) compounds that obtained were heated with carbon disulphide and alcoholic potassium hydroxide where 5-(3 or 4-pyridyl)-1,3,4-oxadiazolo (2,3-C)-1,2,4-triazole 5-thione (III_a-c) were obtained, the given structures were biologically screened.     

THE REACTIONS OF N3P3CL6 AND RELATED COMPOUNDS WITH DIFUNCTIONAL REAGENTS. COMPARISONS AND CONTRASTS

Abstract

The reactions of N₃P₃Cl₆ with a variety of difunctional reagents are discussed. NMR spectroscopic and X-ray crystallographic investigations are presented.     

A Narrative Review on the Phytochemistry,Pharmacology and Therapeutic Potentials of Clinacanthus nutans (Burm. f.) Lindau Leaves as an Alternative Source of Future Medicine

The application of natural products and supplements has expanded tremendously over the past few decades. Clinacanthus nutans (C. nutans), which is affiliated to the Acanthaceae family, has recently caught the interest of researchers from the countries of subtropical Asia due to its medicinal uses in alternative treatment for skin infection conditions due to insect bites, microorganism infections and cancer, as well as for health well-being. A number of bioactive compounds from this plant’s extract, namely phenolic compounds, sulphur containing compounds, sulphur containing glycosides compounds, terpens-tripenoids, terpens-phytosterols and chlorophyll-related compounds possess high antioxidant activities. This literature search yielded about one hundred articles which were then further documented, including the valuable data and findings obtained from all accessible electronic searches and library databases. The promising pharmacological activities from C. nutans leaves extract, including antioxidant, anti-cancer, anti-viral, anti-bacterial, anti-fungal, anti-venom, analgesic and anti-nociceptive properties were meticulously dissected. Moreover, the authors also discuss a few of the pharmacological aspect of C. nutans leaves extracts against anti-hyperlipidemia, vasorelaxation and renoprotective activities, which are seldom available from the previously discussed review papers. From the aspect of toxicological studies, controversial findings have been reported in both in-vitro and in-vivo experiments. Thus, further investigations on their phytochemical compounds and their mode of action showing pharmacological activities are required to fully grasp both traditional usage and their suitability for future drugs development. Data related to therapeutic activity and the constituents of C. nutans leaves were searched by using the search engines Google scholar, PubMed, Scopus and Science Direct, and accepting literature reported between 2010 to present. On the whole, this review paper compiles all the available contemporary data from this subtropical herb on its phytochemistry and pharmacological activities with a view towards garnering further interest in exploring its use in cardiovascular and renal diseases.     

Large‐scale fading behavior for a cellular network with uniform spatial distribution

Large‐scale fading (LSF) between interacting nodes is a fundamental element in radio communications, responsible for weakening the propagation, and thus worsening the service quality. Given the importance of channel‐losses in general, and the inevitability of random spatial geometry in real‐life wireless networks, it was then natural to merge these two paradigms together in order to obtain an improved stochastical model for the LSF indicator. Therefore, in exact closed‐form notation, we generically derived the LSF distribution between a prepositioned reference base‐station and an arbitrary node for a multi‐cellular random network model. In fact, we provided an explicit and definitive formulation that considered at once: the lattice profile, the users' random geometry, the effect of the far‐field phenomenon, the path‐loss behavior, and the stochastic impact of channel scatters. The veracity and accuracy of the theoretical analysis were also confirmed through Monte Carlo simulations.     

New Schiff base complexes of tetrachlorouranium

Summary Tetrachlorouranium complexes containing a Schiff base ligand, p-XC₆H₄NH=CHC₆H₄OH(L), derived from p-XC₆H₄NH₂ and salicylaldehyde, have been prepared. Atris complex was obtained when X=NO₂ andbis complexes for the other p-substituted Schiff bases when X=Cl, Br, OH and Me.     

The synthesis and ultraviolet spectra of some N-aryl-2,3-dihydro-3-oxo-4H-1,4-oxazine derivatives

Two new derivatives of the 1,4-oxazine ring system ( 3a and 3b ) derived from p-aminobenz-amides have been synthesized. The uv absorption spectra of sixteen representative 1,4-oxazines all show two high intensity bands (? ～ 10⁵) between 220-400 ran. The positions and intensities of the absorption maxima have been correlated with the steric and electronic effects of the oxazine ring substituents.     

Some convergence results for asynchronous algorithms

Resumé Nous présentons dans cet article des résultats de convergence des algorithmes asynchrones basés essentiellement sur la notion classique de contraction.Nous généralisons, en particulier, tous les résultats de convergence de ces algorithmes qui font l'hypothèse de contraction en norme vectorielle qui récemment a été très souvant utilisée.Par ailleurs, l'hypothèse de contraction en norme vectorielle peut se trouver difficile, voire impossible à vérifier pour certains problèmes qui peuvent être cependant abordés dans le cadre de la contraction classique que nous adoptons.

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Some convergence results for asynchronous algorithms

Summary In this paper we present convergence results for the asynchronous algorithms based essentially on the notion of classical contraction.We generalize, in particular, all convergence results for those algorithms which are based on the vectorial norm hypothesis, in wide spread use recently.Certain problems, for which the vectorial norm hypothesis can be difficult or even impossible to verify, can nontheless be tackled within the scope of the classical contraction that we adopte.

     

Improved results on robust exponential stability criteria for neutral-type delayed neural networks

In this paper, we investigate the problem of robust global exponential stability analysis for a class of neutral-type neural networks. The interval time-varying delays allow for both slow and fast time-varying delays. The values of the time-varying uncertain parameters are assumed to be bounded within given compact sets. Improved global exponential stability condition is derived by employing new Lyapunov-Krasovskii functional and the integral inequality. The developed nominal and robust stability criteria is delay-dependent and characterized by linear-matrix inequalities (LMIs). The developed results are less conservative than previous published ones in the literature, which are illustrated by representative numerical examples.