排序方式: 共有53条查询结果,搜索用时 31 毫秒
1.
A simple, rapid and precise reverse-phase high performance liquid chromatographic method has been developed for the quantitative determination of eugenol from the extract of dried powder of Cinnamomum tamala leaves and its polyherbal formulation. Chromatographic analysis was carried out on Zorbax C18 column (150 mm × 4.6 mm, 5 μm) with a mobile phase of mixture of water, acetonitrile and methanol in the volume ratio of 50:40:10, at a flow rate of 1.0 mL min-1. Quantitation was performed using a UV-visible detector at 210 nm. Good linearity was obtained over the ranges of 0.20–3.0 μg mL-1 for eugenol. 相似文献
2.
Dighe Vidya V. Sane Ramesh T. Menon Shashikumar N. Tambe Harsha N. Pillai Sreedevi 《平面色谱法杂志一现代薄层色谱法》2006,19(4):319-323
JPC – Journal of Planar Chromatography – Modern TLC - A normal-phase high-performance thin-layer chromatographic (HPTLC) method has been established for quantitative estimation of... 相似文献
3.
Dighe Vidya V. Pathak Gayatri M. Tulpule Ketan M. Gokarn Vijay N. 《平面色谱法杂志一现代薄层色谱法》2007,20(3):179-182
JPC – Journal of Planar Chromatography – Modern TLC - A sensitive high-performance thin-layer chromatographic method has been established for quantification of apigenin in dried root... 相似文献
4.
Satish N. Dighe Ravindra V. Bhattad Raghunath R. Kulkarni Kishor S. Jain 《合成通讯》2013,43(23):3522-3527
The synergy of the combined use of DMSO and an ionic liquid viz. (bbim)+Br? has brought about a rapid and efficient esterification of sodium carboxylates with acyl and alkyl halides under ambient conditions in excellent isolated yields (90–95%) in short reaction times (12–40 min). 相似文献
5.
6.
Satish N. Dighe 《Tetrahedron letters》2009,50(45):6139-6142
The synergy of the combined use of DMSO and an ionic liquid viz. (bbim)+Br− has brought about a mild, convenient, efficient, and rapid protocol for the synthesis of 1-substituted-1H-1,2,3,4-tetrazoles via the condensation of amines, triethyl orthoformate, and sodium azide at ambient temperature in excellent isolated yields (85-90%). The inherent Bronsted acidity of ionic liquid and high polarity of both IL and DMSO resulted in a significant enhancement in the reaction rate. 相似文献
7.
An LC method has been developed for the simultaneous quantitative determination of eugenol, cinnamaldehyde and isoeugenol from dried leaf powder of Cinnamomum tamala Nees & Eberm and stem bark powder of Cinnamomum zeylanicum Breyn. Linear responses for eugenol, cinnamaldehyde and isoeugenol were obtained over the concentration ranges of 0.20–2.50, 5.00–100.00 and 0.10–1.00 μg mL?1, respectively. 相似文献
8.
JPC – Journal of Planar Chromatography – Modern TLC - A sensitive and accurate high-performance thin-layer chromatographic method has been developed, validated, and used for... 相似文献
9.
We show that a source-to-detector distance of 2540 km, motivated recently [S. K. Raut, R. S. Singh, and S. U. Sankar, arXiv:0908.3741] for a narrow band superbeam, offers multiple advantages for a low energy neutrino factory with a detector that can identify muon charge. At this baseline, for any neutrino hierarchy, the wrong-sign muon signal is almost independent of CP violation and θ(13) in certain energy ranges. This allows the identification of the hierarchy in a clean way. In addition, part of the muon spectrum is also sensitive to the CP violating phase and θ(13), so that the same setup can be used to probe these parameters as well. 相似文献
10.
Analysis of K-Transmit Dual-Receive Diversity with Cochannel Interferers over a Rayleigh Fading Channel 总被引:1,自引:1,他引:0
Dighe Parag A. Mallik Ranjan K. Jamuar Sudhanshu S. 《Wireless Personal Communications》2003,25(2):87-100
The need to combat the severe effects of fading and interferencein the rapidly increasing number of communication systemsproviding wireless services has motivated the study of diversityin the presence of interference.Hence the analysis of wireless systems with both transmit andreceive diversity and subject to cochannel interference is animportant tool for system design.We consider here a K-transmit dual-receive diversitycommunication systememploying K antennas for transmission and two antennasfor reception. The desired signal is corruptedby N interfering sources apart from additive whiteGaussian noise. The channel is Rayleigh fading.As a result, the channel matrix for the desired signaland the propagation vectors of the interferers havezero-mean complexGaussian entries; the entries are assumedto be independent and identically distributed.The complex receive weight vectorused for combining the received signalsis chosen so as to maximize the outputsignal-to-interference-plus-noiseratio (SINR).From the statistics of the channel matrix and thepropagation vectors of the interferers,we derive a closed-form expressionfor the probability density function (p.d.f.)of the maximum outputSINR. This p.d.f. can be used to obtainthe symbol errorprobability for different digital modulation schemes. 相似文献