超高效液相色谱-四极杆-飞行时间质谱法快速检测发酵黑茶中黄曲霉毒素B_1

以直接提取稀释结合黄曲霉毒素免疫亲和柱净化的方法,利用超高效液相色谱-四极杆-飞行时间质谱(UPLC-Q-TOF-MS),建立了发酵黑茶中黄曲霉毒素B1(AFB1)的快速分析方法。样品采用甲醇-水溶液(7∶3,体积比)提取,以HSS T3色谱柱(100 mm×2.1 mm,1.8μm)进行色谱分离,通过正离子扫描,Full ms-dd-MS/MS模式进行分析。结果表明:33种发酵黑茶中的AFB1在一定范围内具有良好的线性关系,相关系数(r2)大于0.999,4种样品的加标回收率(n=4)为86.4%~98.0%,相对标准偏差(RSD)为0.3%~1.7%,检出限(LOD,S/N≥3)和定量下限(LOQ,S/N≥10)分别为0.06μg/kg和0.19μg/kg。结果显示33种样品中的AFB1含量均在合理范围内。该方法准确、快速、简单,适用于发酵黑茶中AFB1的检测。     

基于多岛遗传算法的半潜式平台主尺度优化研究

为优化某深水半潜式支持平台的主尺度，采用拉丁超立方设计对样本空间采样，在SESAM 软件中进行参数化建模，根据现有母平台资料确定主尺度约束条件，基于多岛遗传算法分别对平台的垂荡、纵摇、横摇响应进行优化分析，选出稳性最高、排水量适宜的平台主尺度方案。结果表明，该算法能得到满足约束条件下各响应最小的主尺度方案，对平台主尺度初步方案的确定有很高的参考价值。     

距离对不同强度热源红外测温影响及补偿

距离是影响热红外测温精度的主要因素。为研究不同距离下不同热源强度的热红外测温精度,设计野外实验,布设460 K和505K两个热源温度,分别在20 m的距离以间隔为1 m的测温距离采集温度数据,通过函数拟合,分析不同距离下测温值与真实值之间的变化关系。结论如下:1)随着距离的增加,红外测温值呈现先急剧下降,之后逐渐平缓至某一稳定状态的趋势,且当热源温度越高,达到这一稳定状态的距离就越长。2)通过比较多项式和指数拟合函数的相关系数,提出了基于指数函数的温度-距离拟合关系,相关系数最大为0.999。3)依据温度变化速率提出温度-距离的分段数学模型对测温数据进行误差补偿,经过补偿后红外测温值与真实值最大相对误差仅为0.59%。     

高峰值功率高光束质量光纤-固体混合放大激光系统

高峰值功率以及高光束质量的激光光源在激光加工等领域具有重要的应用价值。利用重复频率为50kHz、脉宽为3.9ps、平均功率为10.9mW的光纤种子光源,经过两级固体双通放大,最终得到平均功率为27.65W,峰值功率达到65 MW的激光输出。第一级放大器为端面抽运Nd…YVO_4放大级,第二级放大器为侧面抽运Nd…YAG放大级。通过利用球差补偿理论设计的双通放大结构以及调节放大级中的填充因子,控制最终激光输出的光束质量,得到输出激光的光束质量因子M~2=1.30。     

用于MiniLED背光模组的亮度增强薄膜设计与制备

传统的两层棱镜膜对于MiniLED背光的增亮效果不明显,因此设计了一种微结构薄膜来代替两层棱镜膜。首先,根据MiniLED背光的配光曲线及尺寸,对微结构进行分段设计。将与MiniLED芯片等宽区域设定为顶角90°的棱柱结构,对2个MiniLED芯片之间的区域,将MiniLED芯片作为扩展光源,芯片2个端点发出的光束到达微结构底面会形成一个夹角,将夹角的角平分线处光线准直到轴向方向,结合Snell定律进行计算,得到棱柱微结构倾角。然后,通过LightTools仿真软件对单个微结构及微结构阵列分别进行了建模和仿真,仿真结果表明:加微结构薄膜后的轴向视角亮度相比于加两层棱镜膜提升了31.3%。最后,通过无掩模光刻设备对设计的微结构薄膜进行加工制备,并对样片进行测试。实测结果表明:加微结构薄膜后的轴向视角亮度相较于加两层棱镜膜提升了25.7%。实现了针对MiniLED背光模组的亮度增强设计。     

利用改进的ADI方法实现单机千万节点的油水两相渗流数值模拟

针对实际油藏的非均质分布特征及其复杂的边界条件,本文通过引入迭代参数的压缩因子和放大因子,对现有的交替方向迭代法(ADI)进行改进,提出一种适用于大规模油藏数值模拟的新算法．改进的ADI 方法计算精度可靠,且与现有的算法相比计算效率有所提高．更为关键的是,ADI 算法将求解三维压力方程的七对角矩阵分解为三个方向的三对角矩阵依次迭代求解,所需的运算存储量大幅减少,最大的计算规模有了大幅的提升．使用改进的ADI 方法,在单机上成功实现了千万节点的油水两相渗流数值模拟．计算实例表明,在同等单机硬件条件下,改进ADI 算法的最大计算规模是现有算法的1.7 倍以上．     

The power spectrum and correlation of flow noise for an axisymmetric body in water

Understanding the physical features of the flow noise for an axisymmetric body is important for improving the performance of a sonar mounted on an underwater platform. Analytical calculation and numerical analysis of the physical features of the flow noise for an axisymmetric body are presented and a simulation scheme for the noise correlation on the hydrophones is given. It is shown that the numerical values of the flow noise coincide well with the analytical values. The main physical features of flow noise are obtained. The flow noises of two different models are compared and a model with a rather optimal fore-body shape is given. The flow noise in horizontal symmetry profile of the axisymmetric body is non-uniform, but it is omni-directional and has little difference in the cross section of the body. The loss of noise diffraction has a great effect on the flow noise from boundary layer transition. Meanwhile, based on the simulation, the noise power level increases with velocity to approximately the fifth power at high frequencies, which is consistent with the experiment data reported in the literature. Furthermore, the flow noise received by the acoustic array has lower correlation at a designed central frequency, which is important for sonar system design.     

The diffracted sound field from the transition region of an axisymmetric body in water

Understanding the physical features of the diffracted sound field on the surface of an axisymmetric body is important for predicting the self-noise of a sonar mounted on an underwater platform.The diffracted sound field from the transition region of an axisymmetric body was calculated by the geometrical theory of diffraction.The diffraction ray between the source point and the receiving point on the surface of an axisymmetric body was calculated by using the dynamic programming method.Based on the diffracted sound field,a simulation scheme for the noise correlation of the conformal array was presented.It was shown that the normalized pressure of the diffracted sound field from the transition region reduced with the increases of the frequency and the curvature of the ray.The flow noises of two models were compared and a rather optimum fore-body geometric shape was given.Furthermore,it was shown that the correlation of the flow noise in the low frequencies was stronger than that in the high frequencies.And the flow noise received by the acoustic array on the curved surface had a stronger correlation than that on the head plane at the designed center frequency,which is important for sonar system design.     

Array gain for a conformal acoustic vector sensor array:An experimental study

An acoustic vector sensor can measure the components of particle velocity and the acoustic pressure at the same point simultaneously, which provides a larger array gain against the ambient noise and a higher angular resolution than the omnidirectional pressure sensor. This paper presents an experimental study of array gain for a conformal acoustic vector sensor array in a practical environment. First, the manifold vector is calculated using the real measured data so that the effects of array mismatches can be minimized. Second, an optimal beamformer with a specific spatial response on the basis of the stable directivity of the ambient noise is designed, which can effectively suppress the ambient noise.Experimental results show that this beamformer for the conformal acoustic vector sensor array provides good signal-tonoise ratio enhancement and is more advantageous than the delay-and-sum and minimum variance distortionless response beamformers.     

半潜式平台波浪载荷与运动响应研究

耐波性是漂浮式结构物的重要性能之一。通过对某型半潜式平台所遭受的波浪载荷和运动响应进行分析,采用 DNV 的SESAM 软件,利用势流理论方法进行求解。其中波浪谱选择JONSWAP 谱,同时考虑了波浪的方向性。结合半潜式 平台结构形式的特点,得到了不同浪向、不同波浪周期下的波浪剪切力、波浪分离力、波浪扭转力、波浪弯矩预报结果,以 及平台甲板质心的各向加速度预报值。计算结果表明,该计算方法合理,结果可靠,半潜式平台的总体设计中应综合考虑 波浪组成各因素之间的关系。