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Effect of non-hydrostatic stress on X-ray diffraction in a diamond anvil cell (DAC) is studied. The pressure gradient in the sample chamber leads to the broadening of the diffraction peaks, which increase with the hkl index of the crystal. It is found that the difference between the determined d-spacing compressive ratio d/d0 and the real d-spacing compressive ratio dr/d0 is determined by the yield stress of the pressure transmitting media (if used) and the shear modulus of the sample. On the basis of the corrected experiment data of Mao et al. (MXB86), which was used to calibrate the most widely used ruby fluorescence scale, a new relationship of ruby fluorescence pressure scale is corrected, i.e., P = (1904/9.827)[(1+λ/λ0)9.827-1]. 相似文献
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在无线通信信道中,码间干扰严重影响了通信的质量和可靠性。传统的自适应均衡算法需要训练序列降低了传输效率,恒模算法(CMA)可以很好的克服了这个问题。针对CMA算法收敛速度较慢和无法纠正相位误差的缺点,提出一种新的步长迭代方法的改进型恒模算法(NSMCMA)。蒙特卡罗仿真表明,提出的算法,相比传统CMA算法,不仅可以纠正信道的相位偏转,而且具有更好的均衡效果和收敛性能。 相似文献
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在无线通信信道中,码间干扰严重影响了通信的质量和可靠性。恒模算法(CMA)可以很好的克服码间干扰。针对CMA算法收敛速度较慢和无法纠正相位误差的缺点,提出将改进型CMA算法和改进型判决引导(DD)算法结合起来的混合盲均衡算法。蒙特卡罗仿真表明,提出的算法,相比传统CMA算法,不仅可以纠正信道的相位偏转,而且具有更好的均衡效果和收敛性能。 相似文献
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The high-pressure polymorphs and structural transformation of Sn were experimentally investigated using angledispersive synchrotron x-ray diffraction up to 108.9 GPa. The results show that at least at 12.8 GPa β-Sn→bct structure transformation was completed and no two-phase coexistence was found. By using a long-wavelength x-ray, we resolved the diffraction peaks splitting and discovered the formation of a new distorted orthorhombic structure bco from the bct structure at 31.8 GPa. The variation of the lattice parameters and their ratios with pressure further validate the observation of the bco polymorph. The bcc structure appears at 40.9 GPa and coexists with the bco phase throughout a wide pressure range of40.9 GPa–73.1 GPa. Above 73.1 GPa, only the bcc polymorph is observed. The systematically experimental investigation confirms the phase transition sequence of Sn as β-Sn→bct→bco→ bco + bcc→bcc upon compression to 108.9 GPa at room temperature. 相似文献
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The static equation of state (EOS) of tantalum (Ta) is determined by in situ energy-dispersive synchrotron powder x-ray diffraction in a diamond anvil cell (DAC) up to 133GPa. The body-centered-cubic (bcc) phase of Ta is found to be stable over the entire pressure range investigated. The bulk moduli and its first pressure derivative of Ta are constrained by fitting the determined pressure-volume data to Vinet form EOS: B0 =192.65±(3.08)GPa and B'0 =3.58±(0.11). For the sake of avoiding the affect of non-hydrostatic stress, argon is used as a pressure media. A careful checking of the stress state of the sample is presented simultaneously. 相似文献
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运用金刚石对顶砧(Diamond Anvil Cell,DAC)技术,以液氩作为传压介质,在最高压力为67 GPa的压力范围内对NiO进行了原位的同步辐射X射线衍射研究。在整个实验过程中,并未发现第一类结构相变,也没有发现T.Sasaki等预测的在60 GPa左右轴比c/a随压力的变化率而突然增大的现象,且此压力范围内NiO的结构畸变程度随压力的变化趋势相比以前的研究结果要平缓一些。用三阶的Brich-Murnaghan方程对实验数据进行拟合,得到的体弹模量及其对压力的一阶导数分别为B0=195(4) GPa和B0′=5.3(2)。 相似文献
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极端条件下液体(熔体)的结构和物性是凝聚态物理、材料科学和地球科学关注的重要问题之一。由于长程周期性的缺失,液体在极端条件下的结构和物性的实验和理论研究都面临着巨大的挑战。与晶体相比,人们对极端条件下液体的结构和物性的演化规律所知甚少。本文系统介绍了近年来高温高压条件下液体的结构、密度和黏度测量的研究进展,以及取得的重要科学认识,以期对今后极端条件下液体的结构和物性研究起到一定的参考作用。 相似文献