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排序方式: 共有72条查询结果,搜索用时 14 毫秒
1.
G. Kh. Panova M. N. Khlopkin N. A. Chernoplekov A. A. Shikov 《Physics of the Solid State》2002,44(7):1218-1223
The specific heats of the Ni2B amorphous system and of its crystal analog were studied in the temperature range 3–270 K. The data obtained permitted us to isolate the contribution due to atomic vibrations from the experimentally measured specific heat, determine the electronic density of states at the Fermi level and the temperature dependence of the characteristic Debye parameter Θ, and to calculate some average frequencies (moments) of the vibrational spectrum. The electronic density of states at the Fermi level increases under amorphization. An analysis of the temperature dependence of the lattice specific heat showed that amorphization brings about a substantial growth in the density of vibrational states at low frequencies, whereas the spectrum-averaged and rms frequencies change very little, which is in good agreement with neutron diffraction measurements. 相似文献
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Olga N. Pozharitskaya Svetlana A. Ivanova Alexander N. Shikov Valery G. Makarov 《Chromatographia》2013,76(19-20):1353-1358
Chromatographic separation, analysis of in situ radical-scavenging activity, and quantitative analysis of green sea urchin shell pigments were carried out by online HPTLC-DAD and HPTLC-DPPH methods. Methanol:chloroform:acetic acid:water (11:50:5:2, v/v) was selected as the best mobile phase on silica gel plates for the separation of the pigments. Two pigment spots, S1 and S2, were observed on the TLC plates, while echinochrome A was not detected in the pigment extract of green sea urchin shells. Based on the estimated ID50 values, the antiradical activity was S2 (0.043 μg) > S1 (0.058 μg) > echinochrome A (0.134 μg). 相似文献
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G. Kh. Panova A. A. Shikov N. A. Chernoplekov A. A. Zhokhov A. N. Maljuk C. T. Lin 《Physics of the Solid State》2003,45(12):2237-2241
The anisotropy in the superconducting properties of single-crystal Nd1.85Ce0.15CuO4 was studied from measurements of the heat capacity within the temperature interval 2–40 K in zero magnetic field and in a magnetic field of 8 T. We report on the first observation of heat capacity jumps occurring at the superconducting transition for various magnetic field orientations with respect to the crystallographic axes and on a strong anisotropy of the magnetic contribution to heat capacity in magnetic fields oriented in the a-b plane and perpendicular to it. These measurements yielded the anisotropy in the electronic heat capacity coefficient γn(H) and in the superconducting transition temperature Tc(H). The angular dependence of the Sommerfeld coefficient γn in the a-b plane observed in a magnetic field of 8 T exhibits four-lobe symmetry and zero gap direction of the order parameter. A comparison of the results obtained on the Nd1.85Ce0.15CuO4 single crystal with the data available for La1.85Sr0.15CuO4 permits one to conclude that the mechanisms of superconductivity in the electron-and hole-doped superconductors are similar. 相似文献
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AA Yan LI Kai CAO ZhongHua & HU WenRui Key Laboratory of Microgravity 《中国科学:物理学 力学 天文学(英文版)》2011,(2)
The dependency of the critical Marangoni number on the geometrical aspect ratio of the floating half zone is essential to predict the onset of oscillatory thermocapillary convection.The experimental studies in the microgravity conditions on floating half zones of several centimeters in diameter have predicted that the critical Marangoni number increases with the increasing aspect ratio,and the terrestrial experimental studies have predicted the contradictory conclusion for floating half zones of several mil... 相似文献
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Non-Gravitational Effects with Density-Matching in Evaluating the Influence of Sedimentation on Colloidal Coagulation
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The method of density matching between the solid and liquid phases is often adopted to effectively eliminate the effect of sedimentation of suspensions in studies on dynamic behaviour of a colloidal system. However, the associated changes in the solvent composition may bring side effects to the properties investigated and therefore might lead to a faulty conclusion if the relevant correction is not made. To illustrate the importance of this side effect, we present an example of the sedimentation influence on the coagulation rate of suspensions of 2μm (diameter) polystyrene. The liquid mixtures, in the proper proportions of water (H2O), deuterium oxide (D2O) and methanol (MeOH) as the liquid phase, density-matched and unmatched experiments are performed. Besides the influence of viscosity, the presence of methanol in solvent media, used to enhance the sedimentation effect, causes significant changes (reduction) in rapid coagulation rates compared to that in pure water. Without the relevant corrections for those non-gravitational factors it seems that gravitational sedimentation would retard the coagulation. The magnitude of the contribution from the non-gravitational factor is quantitatively determined, making the relevant correction possible. After necessary the influence of the sedimentation on coagulation rates at corrections for all factors, our experiments show that the initial stage of the coagulation is not observable. 相似文献
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G. Kh. Panova A. A. Shikov M. N. Khlopkin N. A. Chernoplekov 《Physics of the Solid State》2002,44(1):30-33
This paper reports on the temperature and field dependences of the specific heat of high-quality La1.85Sr0.15CuO4 single crystals carried out at low temperatures in magnetic fields of up to 8 T for two magnetic field orientations, namely, along the [100] and [110] crystallographic axes. The field dependence of the electronic density of states (DOS) was found to be anisotropic for different magnetic field orientations in the a–b plane, with the electronic density being the lowest along the a axis (for H ∥ [100]) and maximum for the field inclined at 45° to the a axis (for H ∥ [110]). Electronic specific heat in a magnetic field was observed to depend linearly on temperature T and nonlinearly on the magnetic field H: C DOS=bTH 1/2. In a zero field, the electronic specific heat grows quadratically with temperature as C DOS=αT 2. Estimation of the maximum superconducting gap width from the experimentally determined values of the α coefficient of T 2 and of the electronic DOS in the normal state yields Δ 0=300 K. The observed features indicate that La1.85Sr0.15CuO4 is a superconductor with d symmetry of the order parameter. 相似文献
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