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Leandro F. Pedrosa William P. de Macedo Antonia C. R. Furtado Guilherme P. Guedes Luiz C. S. Pinheiro Jackson A. L. C. Resende 《合成通讯》2013,43(24):3373-3386
New thieno[2,3-b]pyridine phosphoramidates compounds were synthesized and characterized by infrared; 1H, 13C, and 31P NMR spectroscopy; and high-resolution mass spectrometry. The products were obtained in good yields (64–82%) under mild conditions by nucleophilic aromatic substitution reaction of aminoalkylphosphoramidates over 4-chlorothieno[2,3-b]pyridine-5-carbonitrile. The crystal structures of two compounds were solved by x-ray diffraction and showed a network of intermolecular interactions involving phosphoramidate groups. Druglike properties and toxicity of the new compounds were studied with the help of the software Molinspiration, Osiris, and Toxtree, and were compared with the standard drugs amphotericin B, miltefosine, benznidazole, and nifurtimox. [Supplementary materials are available for this article. Go to the publisher's online edition of Synthetic Communications® for the following free supplemental resource(s): Full experimental and spectral details.] 相似文献
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Ana Elisa Ferreira Oliveira Arnaldo César Pereira Mayra Asevedo Campos de Resende Lucas Franco Ferreira 《Electroanalysis》2022,34(5):809-819
In this work, a silver/silver chloride ink is fabricated using two steps. First the silver ink is prepare using silver, nail polish and acetone. Then the silver ink is painted in a paper substrate and a silver chloride layer is deposited using a bleach solution. The result is the silver/silver chloride conductive ink. The silver ink is cheap ($2.49/g), well-dispersive and very easy to fabricate. The materials were characterized by SEM and XRD. The Ag ink showed the formation of a continuous network throughout the silver ink film with fewer agglomeration. The effective chlorination process was also observed in the Ag/AgCl characterization. Since the Ag/AgCl substrate will be used as a quasi-reference electrode, it is important to investigate the electrical properties. The Ag ink showed an average ohmic resistance of 2.27 Ω. The addition of the AgCl layer decreases the conductivity, as expected. In summary, the Ag/Ag/Cl ink developed is simple, well-dispersed, cheap and with good conductivity. Therefore, it can be used as a conductive ink in the fabrication of quasi-reference electrodes. 相似文献
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GRASP with path-relinking is a hybrid metaheuristic, or stochastic local search (Monte Carlo) method, for combinatorial optimization.
A restart strategy in GRASP with path-relinking heuristics is a set of iterations {i
1, i
2, …} on which the heuristic is restarted from scratch using a new seed for the random number generator. Restart strategies
have been shown to speed up stochastic local search algorithms. In this paper, we propose a new restart strategy for GRASP
with path-relinking heuristics. We illustrate the speedup obtained with our restart strategy on GRASP with path-relinking
heuristics for the maximum cut problem, the maximum weighted satisfiability problem, and the private virtual circuit routing
problem. 相似文献
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José Fernando Gonçalves Mauricio G. C. Resende Jorge J. M. Mendes 《Journal of Heuristics》2011,17(5):467-486
This paper presents a biased random-key genetic algorithm for the resource constrained project scheduling problem. The chromosome
representation of the problem is based on random keys. Active schedules are constructed using a priority-rule heuristic in
which the priorities of the activities are defined by the genetic algorithm. A forward-backward improvement procedure is applied
to all solutions. The chromosomes supplied by the genetic algorithm are adjusted to reflect the solutions obtained by the
improvement procedure. The heuristic is tested on a set of standard problems taken from the literature and compared with other
approaches. The computational results validate the effectiveness of the proposed algorithm. 相似文献
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Richard S. Barr Bruce L. Golden James P. Kelly Mauricio G. C. Resende William R. Stewart Jr. 《Journal of Heuristics》1995,1(1):9-32
This article discusses the design of computational experiments to test heuristic methods and provides reporting guidelines
for such experimentation. The goal is to promote thoughtful, well-planned, and extensive testing of heuristics, full disclosure
of experimental conditions, and integrity in and reproducibility of the reported results. 相似文献