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Rafik Aguech Nabil Lasmar Olfa Selmi 《Annals of the Institute of Statistical Mathematics》2019,71(2):389-408
Annals of the Institute of Statistical Mathematics - In this paper, we consider an unbalanced urn model with multiple drawing. At each discrete time step n, we draw m balls at random from an urn... 相似文献
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Laila Manni Olfa Ghorbel-Bellaaj Kemel Jellouli Islem Younes Moncef Nasri 《Applied biochemistry and biotechnology》2010,162(2):345-357
Chitin is a polysaccharide found in abundance in the shell of crustaceans. In this study, the protease from Bacillus cereus SV1 was applied for chitin extraction from shrimp waste material of Metapenaeus monoceros. A high level of deproteinization 88.8% ± 0.4 was recorded with an E/S ratio of 20. The demineralization was completely achieved
within 6 h at room temperature in HCl 1.25 M, and the residual content of calcium in chitin was below 0.01%. 13C CP/MAS-NMR spectral analysis of chitin prepared by the enzymatic deproteinization of shrimp wastes was found to be similar
to that obtained by alkaline treatment and to the commercial α-chitin. The degree of N-acetylation, calculated from the spectrum,
was 89.5%. Chitin obtained by treatment with crude protease from B. cereus was converted to chitosan by N-deacetylation, and the antibacterial activity of chitosan solution against different bacteria
was investigated. Results showed that chitosan solution at 50 mg/mL markedly inhibited the growth of most Gram-negative and
Gram-positive bacteria tested. Furthermore, the antioxidant potential of the protein hydrolysates obtained during enzymatic
isolation of chitin was evaluated using various in vitro assays. All the samples exerted remarkable antioxidant activities. These results suggest that enzymatic deproteinization
of the shrimp shell wastes, using B. cereus SV1 protease, could be applicable to the chitin production process. 相似文献
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Olfa Labidi Rose-Noëlle Vannier Jean-Pierre Wignacourt 《Journal of solid state chemistry》2008,181(9):2268-2273
Reinvestigation of PbBiOXO4 (X=V, P, As) thermal behaviour revealed a phase transition for V- and P-compounds, but no transition for the As-compound. As shown by single-crystal X-ray diffraction and high-resolution neutron powder diffraction, α-PbBiOVO4 transforms to β-PbBiOVO4 at 550 °C. The two PbBiOPO4 varieties are isomorph to the vanadate forms, while PbBiOAsO4 adopts the β-type structure whatever the temperature. PbBiP1−xOAsxO4 and PbBiV1−xOMxO4 (M=As, P, Cr, Mn) solid solutions display both triclinic and monoclinic domains, and the α→β transition temperature is a function of the substitution rate. The ionic conductivity of these compounds was investigated by impedance spectroscopy. The analysis of free space in the β-PbBiOVO4 structure allows to propose a one-dimensional oxygen diffusion pathway along [010] when the temperature increases. 相似文献
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Olfa Labidi Florence Porcher Rose-Noëlle Vannier 《Journal of solid state chemistry》2008,181(9):2260-2267
Reinvestigation of PbBiOVO4 thermal behaviour revealed a phase transition. As shown by single-crystal X-ray diffraction and high-resolution neutron powder diffraction, α-PbBiOVO4 transforms to β-PbBiOVO4 at 550 °C. At 25 °C, α-PbBiOVO4 is triclinic, S.G. P-1, Z=2, with a=5.6088(3), b=7.1109(3), c=7.2978(3) Å, α=108.957(2), β=111.889(2), and γ=94.833(2)°. Above 550 °C, β-PbBiOVO4 is monoclinic, S.G. C2/m, Z=4, with a=13.61(1), b=5.64(1), c=7.18(1) Å, and β=113.75(1)°. Both structures are built upon (O2Bi2Pb2)∞ chains parallel to the [100] direction in the α polymorph and [001] in the β-polymorph. These chains are undulated in α and linear in β. In both structures, VO4 tetrahedra are organized in two sets of rows parallel to (O2Bi2Pb2)∞ chains, thus building layers of (OBiPb) sandwiched by two layers of VO4 oriented head to tail; VO4 displays different orientations in α- and β-PbBiOVO4. 相似文献
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Olfa Tabbene Dorra Gharbi Imen Ben Slimene Salem Elkahoui Mohamed Najib Alfeddy Pascal Cosette Maria Luisa Mangoni Thierry Jouenne Ferid Limam 《Applied biochemistry and biotechnology》2012,168(8):2245-2256
In the present study, we evaluated the antioxidant and the scavenging ability of C14, C15 and C16 bacillomycin D-like lipopeptides produced by B38 strain. They all displayed strong reducing power activity, hydroxyl and superoxide anion radicals scavenging activities and inhibition of lipid peroxidation. In addition, they were found to protect plasmid DNA damage from hydroxyl radical oxidation. Data suggested that their antioxidant potency can be attributed to the hydrophobic and aromatic side-chain groups of their amino acids as well as to the aliphatic chain of their beta amino fatty acids. Note that the hydrocarbon chain length did not interfere with the antioxidant power. Overall, such bacillomycin D lipopeptides which exhibit antioxidant and radical scavenging activities may be useful for cosmetic, therapeutic or pharmaceutical purposes in order to delay or prevent oxidative deterioration of manufactured products. 相似文献
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Olfa MhasniFarhat Rezgui 《Tetrahedron》2011,67(34):6322-6326
A simple and efficient Et3N-mediated transesterification between β-keto esters and Baylis-Hillman alcohols in toluene solution at reflux using a Dean-Stark apparatus, is described. Allylic esters are exclusively obtained in moderate to good yields, with no trace amounts of γ,δ-unsaturated ketones usually expected from the Carroll decarboxylative rearrangement. 相似文献
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Tabbene O Karkouch I Slimene IB Elfeddy N Cosette P Mangoni ML Jouenne T Limam F 《Applied biochemistry and biotechnology》2011,164(1):34-44
When cultured in minimal growth medium, the B38 strain of Bacillus subtilis did not exhibit any antibacterial activity against methicillin-resistant Staphylococcus aureus (MRSA) clinical isolate. Coculturing B38 strain with viable MRSA cells weakly increased antibacterial activity production
(20 AU/ml). Addition of dead MRSA cells in a B38 culture, increased by 8-fold the B. subtilis strain antibacterial activity reaching 160 AU/ml against MRSA strain. This antibacterial activity recovered from cell-free
supernatants was stimulated by an autoinducing compound which is sensitive to the action of proteinase K suggesting a proteinaceous
nature. This compound was heat-stable till 80 °C and showed a molecular mass around 20 kDa as determined by SDS-PAGE. These
results suggest that the production of antibacterial compounds by B38 strain is dependent on the amount of the autoinducing
compound. 相似文献