排序方式: 共有12条查询结果,搜索用时 15 毫秒
1.
Heavy ion irradiation in the electronic stopping power region induces macroscopic dimensional change in metallic glasses and introduces magnetic anisotropy in some magnetic materials. The present work is on the irradiation study of ferromagnetic metallic glasses, where both dimensional change and modification of magnetic anisotropy are expected. Magnetic anisotropy was measured using Mössbauer spectroscopy of virgin and irradiated Fe40Ni40B20 and Fe40Ni38Mo4B18 metallic glass ribbons. 90 MeV 127I beam was used for the irradiations. Irradiation doses were 5×1013 and 7.5×1013 ions/cm2. The relative intensity ratios D 23 of the second and third lines of the Mössbauer spectra were measured to determine the magnetic anisotropy. The virgin samples of both the materials display in-plane magnetic anisotropy, i.e., the spins are oriented parallel to the ribbon plane. Irradiation is found to cause reduction in magnetic anisotropy. Near-complete randomization of magnetic moments is observed at high irradiation doses. Correlation is found between the residual stresses introduced by ion irradiation and the change in magnetic anisotropy. 相似文献
2.
Satish R. Patil Ketan K. Nerurkar Ashok M. Kalamkar Vishwas Pukale Kiran V. Mangaonkar Satish G. Pingale 《Journal of mass spectrometry : JMS》2012,47(1):23-28
An analytical method based on liquid–liquid extraction has been developed and validated for analysis of agomelatine in human plasma. Fluoxetine was used as an internal standard for agomelatine. A Betasil C18 (4.0 × 100 mm, 5 µm) column provided chromatographic separation of analytes followed by detection with mass spectrometry. The method involves simple isocratic chromatographic conditions and mass spectrometric detection in the positive ionization mode using an API‐4000 system. The proposed method has been validated with linear range of 0.050–8.000 ng/ml for agomelatine. The intra‐run and inter‐run precision values are within 12.12% and 9.01%, respectively, for agomelatine at the lower limit of quantification level. The overall recovery for agomelatine and fluoxetine was 67.10% and 72.96%, respectively. This validated method was used successfully for analysis of plasma samples from a pharmacokinetic study. Copyright © 2012 John Wiley & Sons, Ltd. 相似文献
3.
Banerjee Ananya Sane Ramesh T. Mangaonkar Kiran Shailajan Sunita Deshpande Abhijeet Gundi Gunesh 《平面色谱法杂志一现代薄层色谱法》2006,19(1):68-72
JPC – Journal of Planar Chromatography – Modern TLC - A sensitive, simple, and accurate high-performance thin-layer chro-matographic method has been established for determination of... 相似文献
4.
Amita Gupta Alexei Yu Ganin Parmanand Sharma Vikrant Agnihotri LM Belova KV Rao Mikhail E Kozlov AA Zakhidov RH Baughman 《Pramana》2002,58(5-6):1051-1059
We present studies of novel nanocomposites of BiNi impregnated into the structure of opals as well as inverse opals. Atomic force microscopy and high resolution elemental analyses show
a highly ordered structure and uniform distribution of the BiNi filler in the matrix. These BiNi-based nanocomposites are
found to exhibit distinct ferromagnetic-like ordering with transition temperature of about 675 K. As far as we know there
exists no report in literature on any BiNi compound which is magnetic. 相似文献
5.
Using the recent results for the surface current density on cylindrical surfaces of arbitrary cross-section producing uniform
interior magnetic field we propose a method for obtaining solutions of Bean’s critical state model for general cylindrical
samples. The method uses the technique of conformal mapping to express the sample surface and the flux-fronts in terms of
a set of coefficients that depend on a parameter. The flux-fronts are to be determined by solving a system of nonlinear ordinary
differential equations for the coefficients. Retaining only a certain finite number of leading coefficients we get an approximate
solution. The procedure is illustrated by considering two cyclindrical samples — one with an elliptical cross-section and
the other with a non-elliptical cross-section. The virgin curve and small and large magnetization hysteresis loops for the
two samples are obtained. 相似文献
6.
We present a novel ac susceptibility technique for the study of vortex creep in superconducting thin films. With this technique
we study the dynamics of dilute vortices in c-axis oriented Y-123, Hg-1212, and Tl-1212 thin films, as well as a axis oriented Hg-1212 thin films. Results on the Hg-1212 and Tl-1212 thin films indicate that dislocation-mediated plastic
flux creep of single vortices dominates at low temperatures and fields. As the temperature (or the field) is increased, the
increasing vortex-vortex interactions promote a collective behavior, which can be characterized by elastic creep with a non-zero
μ exponent. Also, in some of these samples effects of thermally assisted quantum creep are visible up to 45 K in some of these
samples. In Y-123 thin films, creep is found to be collective down to the lowest temperatures and fields investigated, while
the quantum creep persists only up to 10–11 K. 相似文献
7.
Satish Gangaram Pingale Ketan K. Nerurkar Ajit M. Padgaonkar Uttam D. Pawar Kiran V. Mangaonkar 《Chromatographia》2009,70(5-6):947-951
A sensitive and selective method for the determination of atovaquone in human plasma was developed and validated. The procedure employed the use of an internal standard (chlorothalidone) and a solvent extraction step. Detection was by electrospray ionization tandem mass spectrometry with multiple reaction monitoring. The method showed a linear range from 50 to 2,000 ng mL?1. The extraction recovery was determined to be 84.91 ± 6.42% (SD), the intra- and inter-day assay accuracy (relative error) was within 7.57% and precision (RSD) was below 6.06%. The method was successfully employed to analyze plasma samples and evaluate the pharmacokinetics of atovaquone in human volunteers. 相似文献
8.
Satish G. Pingale Ketan K. Nerurkar Ajit M. Padgaonkar Uttam D. Pawar Kiran V. Mangaonkar 《Chromatographia》2009,70(7-8):1095-1102
An alternative rapid and sensitive liquid chromatography–tandem mass spectrometry method has been developed and validated for simultaneous analysis of proguanil (PRO) and cycloguanil (CYC) in human plasma. The analytes were extracted from human plasma by solid phase extraction. Riluzole (RIL) was used as an internal standard for proguanil and cycloguanil. A HyPURITY Advance C18 column provided chromatographic separation of analytes followed by detection with mass spectrometry. The method involves simple isocratic chromatography conditions and mass spectrometric detection in the positive ionization mode using an API-4000 system. The proposed method has been validated with linear range of 1.5–150.0 ng mL?1 for PRO and 0.5–50.0 ng mL?1 for CYC. The inter-run and intra-run precision values are within 2.54, 9.19% for PRO and 1.99, 10.69% for CYC at LOQ levels. The overall recoveries for PRO and CYC were 102.52 and 106.72%, respectively. Total elution time was as low as 2.50 min. This validated method was used successfully for analysis of plasma samples from a bioequivalence study. 相似文献
9.
Patil SR Nerurkar KK Kalamkar AM Pukale V Mangaonkar KV Pingale SG 《Journal of mass spectrometry : JMS》2012,47(1):23-28
An analytical method based on liquid-liquid extraction has been developed and validated for analysis of agomelatine in human plasma. Fluoxetine was used as an internal standard for agomelatine. A Betasil C18 (4.0?×?100?mm, 5?μm) column provided chromatographic separation of analytes followed by detection with mass spectrometry. The method involves simple isocratic chromatographic conditions and mass spectrometric detection in the positive ionization mode using an API-4000 system. The proposed method has been validated with linear range of 0.050-8.000?ng/ml for agomelatine. The intra-run and inter-run precision values are within 12.12% and 9.01%, respectively, for agomelatine at the lower limit of quantification level. The overall recovery for agomelatine and fluoxetine was 67.10% and 72.96%, respectively. This validated method was used successfully for analysis of plasma samples from a pharmacokinetic study. 相似文献
10.
Shetty Prabha G. Mangaonkar Kiran V. Sane Ramesh T. Jaripatke Kamlakar K. Singh Shweta 《平面色谱法杂志一现代薄层色谱法》2007,20(2):117-120
JPC – Journal of Planar Chromatography – Modern TLC - A simple and rapid high-performance thin-layer chromatographic method has been established and validated for determination of... 相似文献