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Preparation and Spectroscopical Investigations of Trivinyl- and Triallylfluorosilane Trivinyl- and Triallylfluorosilane were prepared. The i.r. and Raman spectra have been recorded. The discussion of intra- and intermolecular interactions is based on the spectroscopic data. 相似文献
3.
Spectroscopie Investigations on R? C6H4O(CH3)2SiF Compounds The i.r. and Raman spectra of a number of R? C6H4O(CH3)2SiF compounds (R = H, CH3, CH3O, Cl, Br, NO2, NH2) have been recorded. The intramolecular and intermolecular interactions were discussed by means of ν SiF, ν Si? O? (C), ν C? O? (Si) and νs SiC2 vibrations. 相似文献
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R. Furler Ingrid E. C. P. M. Licht J. K. L. Offenberg H. L. Polak 《Journal of Radioanalytical and Nuclear Chemistry》1975,25(2):255-260
Studies are reported to illustrate surface adsorption of144Ce,59Fe,234Th,233U,237Np,239Pu and241Am on a dextran gel made by crosslinkage of the polysaccharide dextran (Sephadex). Fixation of such elements was studied from
aqueous solution and was found to depend on pH, age of the tracer solution, hydrolytic behaviour of the adsorbed species,
concentration and the valency of the adsorbed element. 相似文献
6.
Felix Burkhardt Carl G. Schirmeister Christian Wesemann Massimo Nutini Stefano Pieralli Erik H. Licht Marc Metzger Frederik Wenz Rolf Mülhaupt Benedikt C. Spies 《Molecules (Basel, Switzerland)》2020,25(24)
A polyolefin with certified biocompatibility according to USP class VI was used by our group as feedstock for filament-based 3D printing to meet the highest medical standards in order to print personal protective equipment for our university hospital during the ongoing pandemic. Besides the chemical resistance and durability, as well as the ability to withstand steam sterilization, this polypropylene (PP) copolymer is characterized by its high purity, as achieved by highly efficient and selective catalytic polymerization. As the PP copolymer is suited to be printed with all common printers in fused filament fabrication (FFF), it offers an eco-friendly cost–benefit ratio, even for large-scale production. In addition, a digital workflow was established focusing on common desktop FFF printers in the medical sector. It comprises the simulation-based optimization of personalized print objects, considering the inherent material properties such as warping tendency, through to validation of the process chain by 3D scanning, sterilization, and biocompatibility analysis of the printed part. This combination of digital data processing and 3D printing with a sustainable and medically certified material showed great promise in establishing decentralized additive manufacturing in everyday hospital life to meet peaks in demand, supply bottlenecks, and enhanced personalized patient treatment. 相似文献
7.
Andrea I. Licht 《Journal of organometallic chemistry》2003,687(1):142-152
The reaction of ω-alkenyl substituted zirconocene dichloride complexes with two equivalents of n-butyllithium is strongly influenced in the presence of alkenes and alkynes. Metallacyclic zirconocene complexes of novel structures are obtained. The additives alkenes and alkynes compete with the ω-alkenyl substituents and the intermediate 1-butene for the formation of a metallacyclic structure. The reaction of ω-alkenyl substituted zirconocene dichloride complexes with two equivalents of ethyllithium and n-hexyllithium gives analogous reactions and metallacycles as with n-butyllithium. 相似文献
8.
A mathematical study via variational convergence of a periodic distribution of classical linearly elastic thin plates softly abutted together shows that it is not necessary to use a different continuum model nor to make constitutive symmetry hypothesis as starting points to deduce the Reissner–Mindlin plate model. 相似文献
9.
This study addresses a fundamental challenge posed by hexavalent iron electrochemical irreversibility, which had slowed practical development of reversible Fe(VI) cathodes; nanolayers circumvent fundamental passivation challenges, and are electrodeposited from solution phase FeO(4)(2-), forming 601 mAh g(-1) Li, and 485 mAh g(-1) Na, Fe(III/VI) alkaline cathodes, the latter exhibiting 100-200 storage cycles at 80% depth of discharge, providing pathways towards metal hydride batteries with twice the cathode capacity. 相似文献
10.
We propose a behavioral modeling that takes into account the thermomechanical couplings accompanying the phase transition in single-crystal CuZnAl samples. The goal of this model is to put forward the significant role played by the heat diffusion in the propagation mode of the phase change fronts. Numerical simulations showed the existence of such a phase change front and predicted the calorimetric and kinematic effects accompanying its propagation. In particular, an inversion of the propagation way during a creep test and caused by an increase of the room temperature was correctly simulated by the model. To cite this article: A. Chrysochoos et al., C. R. Mecanique 331 (2003). 相似文献