Creep strain recovery of Fe-Ni-B amorphous metallic ribbon

Creep strain recovery and structural relaxation of the amorphous metallic glass Fe₄₀Ni₄₁B₁₉ after longtime loading at different annealing temperatures below the glass transition temperature have been studied using anisothermal differential scanning calorimetry (DSC) and dilatometry (TMA). It has been demonstrated that structural relaxation effects depend on the stress-annealing temperature of the amorphous ribbon. The structural relaxation states of the amorphous ribbon annealed at different temperatures under and without applied stress have been compared. The activation energy spectra were calculated from the anisothermal dilatometric measurements using the modern method based on the Fourier transformation technique. The influence of the annealing temperature on the shape of creep strain recovery spectra has been analyzed.      

Über tensorielle Integralgleichungen

Ohne Zusammenfassung     

Gravitation and Riemannian space

The field equations of the quadratic action principle of relativity are solved, assuming a weak perturbation of the basic structure, which is a highly agitated Riemannian lattice field of a very small lattice constant. A field emerges which can be interpreted as the weak gravitational field of an apparently Minkowskian space. This field does not coincide with Einstein's theory of weak gravitational fields. Whereas the redshift remains unchanged, the light deflection becomes reduced by11.1% of the value predicted by Einstein.     

Vector potential and Riemannian space

This paper uncovers the basic reason for the mysterious change of sign from plus to minus in the fourth coordinate of nature's Pythagorean law, usually accepted on empirical grounds, although it destroys the rational basis of a Riemannian geometry. Here we assume a genuine, positive-definite Riemannian space and an action principle which is quadratic in the curvature quantities (and thus scale invariant). The constant σ between the two basic invariants is equated to1/2. Then the matter tensor has the trace zero. In consequence of the constancy of the scalar curvature and the divergence identity of the matter tensor, the perturbation metric has to satisfy a scalar and a vector condition, with a negative sign in the fourth coordinate. These conditions lead to the Lorentz condition and the wave equation for the vector potential. Thus the entire Maxwell-Lorentz type of electrodynamics becomes logically derivable, making no concession to any irrationality.     

Simultaneous measurement of proline and related compounds in oak leaves by high-performance ligand-exchange chromatography and electrospray ionization mass spectrometry for environmental stress studies

A mass spectrometer was coupled to high-performance ligand-exchange liquid chromatography (HPLEC) for simultaneous analysis of stress associated solutes such as proline, hydroxyproline, methylproline, glycine betaine and trigonelline extracted from leaves of drought stressed oaks and an internal standard namely N-acetylproline. Methanol/chloroform/water extracts were analyzed using an Aminex HPX-87C column and specifically quantified by the positive ion mode of an electrospray ionisation-mass spectrometry (ESI-MS) in single ion monitoring (SIM) mode. The recovery of N-acetyl proline added to oak leaf extracts ranged from 85.2 to 122.1% for an intra-day study. Standard calibration curves showed good linearity in the measured range from 0.3125 to 10 μmol L⁻¹ with the lowest correlation coefficient of 0.99961 for trigonelline. The advantages of this alternative procedure, compared to previously published methods using fluorescence or amperometric detections, are the simultaneous and direct detection of osmoprotectants in a single chromatographic run, a minimal sample preparation, a good specificity and reduced limits of quantification, ranging from 0.1 to 0.6 μmol L⁻¹. Fifty-six days of water deficit exposure resulted in increased foliar free proline levels (2.4-fold, P < 0.001, 155 μmol g⁻¹ FW) and glycine betaine contents (2.5-fold, P < 0.05, 175 μmol g⁻¹ FW) of drought stressed oak compared to control.