排序方式: 共有63条查询结果,搜索用时 15 毫秒
1.
G. Z. Kaziev A. A. Dutov S. I. Quinones A. de Ita S. N. Sychkin 《Russian Journal of General Chemistry》2005,75(1):18-20
Indium dodecatungstosilicate of the composition [In(OH)⋅5H2O]2 [SiW12O40]⋅H2O is synthesized and studied by means of IR spectroscopy, thermogravimetry, and X-ray phase analysis. The crystals of this compound are triclinic, space group P1, a 13.079(3), b 13.795(3), c 13.967(3) Å, α 90.08(3)°, β 103.76(3)°, ψ107.76(3)°, Z 2, and πcalc 4.900 g cm−3.__________Translated from Zhurnal Obshchei Khimii, Vol. 75, No. 1, 2005, pp. 21–23.Original Russian Text Copyright © 2005 by Kaziev, Dutov, Quinones, Ita, Sychkin. 相似文献
2.
Tumarkin A. V. Kaziev A. V. Kolodko D. V. Pisarev A. A. Kharkov M. M. Khodachenko G. V. 《Physics of Atomic Nuclei》2015,78(14):1674-1676
Copper coatings were deposited on monocrystalline Si substrates using a magnetron discharge with a liquid cathode in the metal vapour plasma. During the deposition, the bias voltage in the range from 0 V to–400 V was applied to the substrate. The prepared films were investigated by a scanning electron microscope, and their adhesive properties were studied using a scratch tester. It was demonstrated that the adhesion of the deposited films strongly depends on the bias voltage and varies in a wide range.
相似文献3.
4.
Ammonium hexamolybdooxalatovanadate of the composition (NH4)3[V(C2O4)Mo6O18(OH)6] · 3H2O (I) has been synthesized and studied by mass spectroscopy, IR spectroscopy, thermogravimetry, and X_ray powder diffraction. Crystals of I are monoclinic with the unit cell parameters a = 11.9737 Å, b = 18.6533 Å, c = 11.2178 Å, β = 121.021°, V = 3162. 95 Å3, M = 1214.01 g/mol, ρcalcd = 1.91 g/cm3, and Z = 3. 相似文献
5.
G. Z. Kaziev A. V. Oreshkina S. Holguin Quinones A. F. Stepnova V. E. Zavodnik Antonio de Ita D. A. Alekseev 《Russian Journal of Coordination Chemistry》2010,36(12):887-890
The sodium hydrogen oxovanadate [Na2(H2O)8] 2H2[V10O28] · 4H2O was synthesized and studied by TGA, X-ray diffraction, and NMR and IR spectroscopy. The crystals are triclinic, space group
P
$
\bar 1
$
\bar 1
, a = 8.545(7) ?, b = 10.827(2) ?, c = 11.627(2) ?, α = 105.48(3)°, β = 99.38(3)°, γ = 101.29(3)°, V = 989.9(3) ?3, ρ(calcd) = 2,381 g/cm3, Z= 1. 相似文献
6.
A. V. Oreshkina G. Z. Kaziev N. N. Lobanov A. V. Steblevskii 《Russian Journal of Inorganic Chemistry》2011,56(12):1883-1885
Ammonium hexamolybdobismuthate(III) of composition (NH4)3[BiMo6O18(OH)6] · 7H2O (I) was synthesized and studied by mass spectrometry, X-ray diffraction, IR spectroscopy, and thermogravimetry. The compound is monoclinic: a = 10.438 Å, b = 7.909 Å, c = 18.127 Å, β = 96.59°, V = 1486.76 Å3, ρcalc = 3.32 g/cm3, Z = 2. 相似文献
7.
E. V. Chernikova A. V. Morozov M. B. Kaziev E. S. Garina V. B. Golubev 《Polymer Science Series A》2007,49(9):962-974
The free-radical azeotropic bulk copolymerization of styrene and n-butyl acrylate at 90°C mediated by tert-butyl dithiobenzoate and copoly(strene—n-butyl acrylate) dithiobenzoate as reversible chain-transfer agents has been studied. It has been shown that low-and high-molecular mass chain-transfer agents allow one to efficiently control the molecular-mass characteristics of the copolymers. For all studied systems, the molecular mass linearly increases with conversion, and the copolymers are characterized by low polydispersity indexes. When polystyryl dithiobenzoate and poly(butyl acrylate) dithiobenzoate are used as polymer reversible chain-transfer agents in the azeotropic copolymerization of styrene and n-butyl acrylate, the diblock copolymers with the controlled block lengths are prepared. As evidenced by ESR studies, radical intermediates are formed in the course of the azeotropic copolymerization of styrene and n-butyl acrylate mediated by tert-butyl dithiobenzoate and the copolymer reversible chain-transfer agent; the kinetics of formation of these intermediates has been investigated. It has been demonstrated that the rate of the azeotropic copolymerization mediated by low-and high-molecular-mass reversible chain-transfer agents decreases with an increase in their concentration. The possible causes of this phenomenon are discussed. 相似文献
8.
9.
M. S. Zibrov G. V. Khodachenko A. V. Tumarkin A. V. Kaziev T. V. Stepanova A. A. Pisarev M. V. Atamanov 《Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques》2013,7(6):1156-1162
Depositions of copper and titanium coatings on aluminum foils and polished aluminum plates for thier protection against corrosion in alkaline media were performed. The coatings were deposited in three different types of magnetron sputtering systems: a direct current (DC) magnetron discharge, a high current impulse magnetron discharge, and a DC magnetron discharge with melted cathode. Only aluminum foils coated with copper films obtained by combined ion-plasma technology, which included preliminarily sputtering of the aluminum surface with an ion beam, deposition of a dense interlayer in the DC magnetron discharge with ion assistance of initial stage of deposition, and deposition of additional layer in the magnetron discharge with melted cathode, were resistant against 30 wt % NaOH solution. 相似文献
10.
G. Z. Kaziev Saul Holguin Quinones A. F. Stepnova V. N. Khrustalev A. V. Oreshkina L. Moralez Sanchez 《Russian Journal of General Chemistry》2014,84(9):1651-1655
Ammonium isopolymolybdate (NH4)4[Mo8O26]·4H2O was prepared for the first time and studied by X-ray diffraction analysis. 相似文献