基于联合变换相关器的像移测量仿真分析

对基于联合变换相关器的像移测量数学原理进行了说明,介绍了面阵CCD的安装位置以及输入图像的获取方法,分析了低信噪比输入图像、相对转动位移对测量精度的影响。应用MATLAB对输入图像进行傅里叶变换得到联合功率谱,对二值化处理的功率谱进行傅里叶变换得到相关输出,用质量中心算法计算出像移量。分析得出,输入图像信噪比大于5dB,测量均方误差小于0.05像素;输入图像相对转动位移在0.1°的范围内,转动位移对测量精度和峰噪比的影响可以忽略不计。综合分析表明像移测量均方误差小于0.05像素。     

First-principle studies on the electronic structure of Fe3O4(110) surface

The first-principle was employed to study the six possible models for the Fe₃O₄(110) surface, namely the AB-terminated surface (AB model), the AB-terminated with Fe_A vacancy (AB-Fe_A vac model), the AB-terminated with Fe_B vacancy (AB-Fe_B vac model), the B-terminated surface (B model), the B-terminated surface with Fe_B vacancy (B-Fe_B vac model) and the B-terminated surface with O vacancy (B-O vac model). The stability, the electronic structure and the magnetic properties of the six surface models were also calculated. The results predict that the B-O vac model is more stable than other types of surface models. The half-metallic property remain in the AB and B models, while the other four surface models exhibit metallic properties. At the same time, the AB, AB-Fe_A vac, AB-Fe_B vac, B and the B-Fe_B vac models have ferrimagnetic properties, while the B-O vac model has antiferromagnetic property.      

偏二甲肼纯度分析方法的改进

采用毛细管气相色谱内标法代替标准工作曲线法测定偏二甲肼纯度(UDMH),内标法的使用避免了微量进样不准确的缺陷.结果显示,该方法线性范围宽,偏二甲肼的标准曲线相关系数为0.9959,样品加标回收率98.39%,样品的测定标准偏差为0.0015,方法的准确度高、重现性好.     

三阶泛函微分方程的周期解的存在性

本文利用重合度理论研究了一类三阶泛函微分方程方程的2π-周期解的问题,获得了该方程存在2π-周期解的若干新结论,改进推广了有关文献中的已有结果．     

FRACTAL VISCOUS FINGERING AND ITS SCALING STRUCTURE IN RANDOM SIERPINSKI CARPET

Viscous fingering (VF) in random Sierpinski carpet is investigated by means of successive over-relaxation technique and under the assumption that bond radii are of Rayleigh distribution. In the random Sierpinski network, the VF pattern of porous media in the limit M→∞ (M is the viscosity ratio and equals to η₂/η₁ where η₁ and η₂ are the viscosities of the injected and displaced fluids, respectively) is found to be similar to the diffusion-limited aggregation (DLA) pattern. The interior of the cluster of the displacing fluid is compact on long length scales when M=1, and the pores in the interior of the cluster have been completely swept by the displacing fluid. For finite values of M such as M≥10, the pores in the interior of the cluster have been only partly swept by the displacing fluid on short length scales. But for values of M in 1f(α) sites have velocites scaling as L^-α; and the scaling function f(α) is measured and its variation with M is found.     

混合优化RBF-BP网络的板形缺陷识别

针对传统板形模式识别方法存在精度低、鲁棒性弱的问题,提出了一种混合优化RBF-BP组合神经网络板形模式识别方法。首先利用自组织映射网络(SOM)对样本聚类,利用聚类后的网络拓扑结构确定RBF的中心,并计算RBF的宽度,克服了传统聚类算法随机选取中心导致聚类结果不稳定的问题。然后利用遗传算法(GA)良好的全局搜索能力优化整个网络的权值。RBF-BP组合神经网络是由一个RBF子网和一BP子网串联构成的,该网络同时具备BP神经网络能较好地预测未知样本的能力以及RBF神经网络的逼近速度快的优点。并以某900HC可逆冷轧机板形识别为应用背景,在MATLAB2010a环境下进行仿真实验,结果表明混合优化RBF-BP组合神经网络的板形模式识别方法能够识别出常见的板形缺陷,提高了板形缺陷识别精度并具有较好的鲁棒性,可以满足板带轧机高精度的板形控制要求。     

超级微波消解-电感耦合等离子体发射光谱（ICP-OES）法测定土壤中18种元素

为提高土壤多元素同时检测的效率,采用超级微波消解-电感耦合等离子体发射光谱法测定土壤中钾、钠、钙、镁、铜、铁、锰、锌、磷、硫、硼、砷、镉、铬、铅、钴、镓、锂等18种元素含量。比较了超级微波消解、常规微波消解和电热板消解的处理效果,采用超级微波消解法对样品进行前处理,并优化了消解条件。在最优条件下,各元素的检出限在0.05~20 mg/kg,加标回收率在86.2%~107.5%,RSD在0.1%~3.0%,方法准确度及精密度可以满足多元素同时测定的需求,且该方法具有简单、快速、成本低、用酸量少、重现性好等特点。     

废水中偏二甲肼在Ni/Fe催化剂上的催化分解研究

研究了Ni/Fe催化剂对废水中偏二甲肼臭氧化分解的催化作用,考察了组分含量、体系的pH值和偏二甲肼初始浓度对催化反应的影响.结果表明,Ni/Fe催化剂对水中偏二甲肼的臭氧化具有良好的催化活性.催化剂组分含量、体系的pH值和初始浓度对反应的影响程度不大.对催化剂的XRD表征结果表明,催化剂主要由尖晶石结构的铁酸盐和FeNi3合金相组成,催化剂的良好催化性能与催化剂中尖晶石结构的铁酸盐和FeNi3合金相的形成有关.     

青蒿素转化成异氢化青蒿酸及有关反应

本文报道从青蒿素经六步反应转化成异氢化青蒿酸。青蒿素经酸处理得失碳倍半萜内酯3,3经硷水解再酯化生成α,β-不饱和酮酯5,然后由Wittig反应得共轭双烯酯6,用RaneyNi(W_2)催化氢化生成异氢化青蒿酸酯7,最后经硷水解得到异氢化青蒿酸8。     

THE OVERLAP OF MAGNETIZATION AND THE COUPLING OF IMPURITIES WI丁H LATTICE FOR DM SPIN GLASS

The overlap of magnetization of the giound state in a RKKY spin glass system with the Dzyaloshinsky-Moriya interaction is studied based on the theory of infinite number of order parameter. It is shown that the nonmagnetic impurities are coupled with the host lattice.The results are in good agreement with experiments.