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An improved experimental arrangement for the determination of kinetic data relating to polarographic reductions is described. The significant feature is the constant-temperature reference electrode; its construction and use in this context are described. A comparison is made of the more realistic results obtained by these means, with those obtained with a more conventional cell where the temperature of the reference electrode is varied with that of the working solution. 相似文献
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Frank W. Crow Michael L. Gross Maurice M. Bursey 《Journal of mass spectrometry : JMS》1981,16(7):309-311
Collisional activation of the molecular ions of 1-propanol, 2-propanol and methyl ethyl ether, and of the m/z 60 ion from 1,2-dimethoxyethane provides evidence for four distinct forms of [C3H8O]+˙. Collision induced decompositions may be explained either by simple cleavages, by cyclic processes involving adjacent substituents, or by bicyclic processes of adjacent substituents. Evidence for a form of [C3H8O]+˙ in which charge and radical site are separate is assembled from the spectra. 相似文献
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Stone N Hart Prieto MC Crow P Uff J Ritchie AW 《Analytical and bioanalytical chemistry》2007,387(5):1657-1668
Near-infrared Raman spectroscopy, an optical technique that is able to interrogate biological tissues, has been used to study
bladder and prostate tissues, with the objective being to provide a first approximation of gross biochemical changes associated
with the process of carcinogenesis. Prostate samples for this study were obtained by taking a chip at TURP, and bladder samples
from a biopsy taken at TURBT and TURP, following ethical approval. Spectra were taken from purchased biochemical constituents
and different pathologies within the bladder and the prostate. We were then able to determine the biochemical basis for these
pathologies by utilising an ordinary least-squares fit. We have shown for the first time that we are able to utilise Raman
spectroscopy in determining the biochemical basis for the different pathologies within the bladder and prostate gland. In
this way we can achieve a better understanding of disease processes such as carcinogenesis. This could have major implications
in the future of the diagnosis of disease within the bladder and the prostate gland. 相似文献
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