Image registration based on matrix perturbation analysis using spectral graph

We present a novel perspective on characterizing the spectral correspondence between nodes of the weighted graph with application to image registration. It is based on matrix perturbation analysis on the spectral graph. The contribution may be divided into three parts. Firstly, the perturbation matrix is obtained by perturbing the matrix of graph model. Secondly, an orthogonal matrix is obtained based on an optimal parameter, which can better capture correspondence features. Thirdly, the optimal matching matrix is proposed by adjusting signs of orthogonal matrix for image registration. Experiments on both synthetic images and real-world images demonstrate the effectiveness and accuracy of the proposed method.     

基于自抗扰控制器的力矩电机伺服系统控制

自抗扰控制器能将被控对象的内、外“总扰动”进行估计并用前馈补偿的方法将其抵消,适于力矩电机因直接驱动所带来干扰的补偿与控制。针对测量噪声对线性自抗扰控制器观测器带宽的限制,提出了二阶线性自抗扰的相似结构,并结合三阶积分链式微分器对其效果进行了对比仿真验证。力矩电机的控制仿真实验表明,与二阶线性自抗扰算法相比,基于相似结构的改进的力矩电机控制,能在有测量噪声情况下兼顾系统跟踪精度、突加负载时抗扰动性与抗噪性。     

非制冷铁电混合式焦平面探测器新研究

本文报道一种128×128元铁电非制冷混合式焦平面探测器，涉及该器件的混合式结构.分析了影响器件性能的关键因素，给出器件所采用的铁电材料的基本物理和电学特性参数，器件的热隔离技术和相应参数，读出电路的基本结构和性能.对实验数据所涉及的原理进行了讨论，最后给出了利用该器件得到的清晰红外热像.     

Synthesis of Monodisperse Colloidal ZnS Spheres by an Acid-Free Two-Step Approach

In this work, we demonstrate a new two-step method for preparing monodisperse ZnS colloidal spheres. The method contains a hot-injection step for making primary particles as seeds and a heating-up step for aggregation growth of secondary colloidal spheres. Instead of the most commonly used thioacetamide in previous studies, thiourea (TU) was selected as the sulfur source. The temperature-dependent thermal decomposition rate of TU makes the releasing of S²⁻ and nucleation of ZnS under proper kinetic control, meanwhile making the reaction a mild and acid-free process. By separating the two steps and using a milder sulfur precursor, monodisperse ZnS colloidal spheres have been prepared. Their diameters can be delicately tuned in the range from 54 to 172 nm through simply changing the amount of Zn and S precursor. The optical properties of the obtained ZnS spheres were studied by extinction and PL measurements, and they exhibit size-dependent optical behavior.     

Synthesis,Antitumor Activity and Preliminary Structure-activity Relationship of 2-Aminothiazole Derivatives

In this paper, we described the synthesis of 2-aminothiazole sublibrary containing methyl, bromo, phenyl or butylidene at 4- or/and 5-position of its core. All target compounds were evaluated for their antitumor activities against human lung cancer cell line H1299 and human glioma cell line SHG-44. Among the compounds screened, 4,5,6,7-tetrahydrobenzo[d]thiazole(26b) exhibited the most potent antitumor activities with IC₅₀ values of 4.89 and 4.03 μmol/L against the two tested cell lines, respectively. Preliminary structure-activity relationship(SAR) studies of these compound were subsequently investigated.     

富营养化水中三种野生蓼科植物蒸腾和营养吸收的关系

本文研究了富营养化水栽培下蓼科植物酸模叶蓼，野荞麦和羊蹄蒸腾特点及与营养吸收的关系。     

S型异质结光催化剂ZnFe2O4/WO3的构筑及光催化还原CO2性能

通过在WO₃纳米片表面负载ZnFe₂O₄纳米颗粒,构建了一系列S型异质结光催化剂ZnFe₂O₄/WO₃,并研究了其光催化CO₂还原性能。在没有助催化剂和牺牲剂的条件下,所制备的ZnFe₂O₄/WO₃复合材料可对CO₂与水蒸汽进行光催化反应。优化后的材料光照5 h后CO₂还原产物CO和CH₄的产量分别为7.87和4.88 μmol·g^-1。相对于单相组分,CO和CH₄的产量明显提高。光催化活性的提高,归因于ZnFe₂O₄和WO₃异质结的形成以及光生载流子的S型电荷传输模式。     

S型异质结光催化剂ZnFe2O4/WO3的构筑及光催化还原CO2性能

通过在WO₃纳米片表面负载ZnFe₂O₄纳米颗粒,构建了一系列S型异质结光催化剂ZnFe₂O₄/WO₃,并研究了其光催化CO₂还原性能。在没有助催化剂和牺牲剂的条件下,所制备的ZnFe₂O₄/WO₃复合材料可对CO₂与水蒸汽进行光催化反应。优化后的材料光照5 h后CO₂还原产物CO和CH₄的产量分别为7.87和4.88 μmol·g^-1。相对于单相组分,CO和CH₄的产量明显提高。光催化活性的提高,归因于ZnFe₂O₄和WO₃异质结的形成以及光生载流子的S型电荷传输模式。     

混合式非致冷焦平面器件芯片工艺研究

随着红外热成像应用技术的不断发展，国内外研究和开发低成本非致冷热像仪的兴趣越来越浓。而开发非致冷热像仪的关键技术在于开发其核心部件非致冷焦平面器件。本文对致冷型焦平面器件和非致冷型焦平面器件进行简单的比较，简要报导国内外非致冷焦平面器件的发展状况、规模、目前达到的水平及其应用，着重叙述混合式１２８×１２８非致冷焦平面器件芯片的研制工艺。     

Mono(amidinate) rare earth metal bis(alkyl) complexes: Synthesis,structure and their activity for l-lactide polymerization

Alkane elimination reaction between Ln(CH₂SiMe₃)₃(THF)₂ (Ln = Y, Lu) with one equivalent of the amidines with different steric demanding HL ([CyC(N-2,6-ⁱPr₂C₆H₃)₂]H (HL₁), [CyC(N-2,6-Me₂C₆H₃)₂]H (HL₂), [PhC(N-2,6-Me₂C₆H₃)₂]H (HL₃)) in THF afforded a series of mono(amidinate) rare earth metal bis(alkyl) complexes [CyC(N-2,6-ⁱPr₂C₆H₃)₂]Ln(CH₂SiMe₃)₂(THF) (Ln = Y (1), Lu (3)), [CyC(N-2,6-Me₂C₆H₃)₂]Ln(CH₂SiMe₃)₂(THF)₂ (Ln = Y (4), Lu (6)), and [PhC(N-2,6-Me₂C₆H₃)₂]Y(CH₂SiMe₃)₂(THF)₂ (7) in 75–89% isolated yields. For the early lanthanide metal Nd, THF slurry of NdCl₃ was stirred with three equiv of LiCH₂SiMe₃ in THF, followed by addition of one equiv of the amidines HL₁ or HL₂ gave an “ate” complex [CyC(N-2,6-ⁱPr₂C₆H₃)₂]Nd(CH₂SiMe₃)₂(μ-Cl)Li(THF)₃ (2) in 48% yield and a neutral [CyC(N-2,6-Me₂C₆H₃)₂]Nd(CH₂SiMe₃)₂(THF)₂ (5) in 52% yield, respectively. They were characterized by elemental analysis, FT-IR, NMR spectroscopy (except for 2 and 5 for their strong paramagnetic property). Complexes 2, 3, 4 and 5 were subjected to X-ray single crystal structure determination. These neutral mono(amidinate) rare earth metal bis(alkyl) complexes showed activity towards l-lactide polymerization to give high molecular weight and narrow molecular weight distribution polymers.