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Yu. A. Vil’pan I. L. Grinshtein A. A. Akatov S. Gucer 《Journal of Analytical Chemistry》2005,60(1):38-44
A new method was developed for the direct electrothermal atomic absorption determination of mercury in drinking water and urine using double vaporization in a two-step atomizer with a purged vaporizer. In this method, a sample is placed in the vaporizer of a two-step atomizer, dried, and vaporized. The sample vapor is transferred to an unheated atomizer cell with a flow of argon and trapped by the inner surface of cell walls. This procedure can be performed repeatedly to preconcentrate mercury in the atomizer cell. Next, a portion of the sample transferred to the inner surface of the atomizer cell is revaporized and atomized by heating the atomizer cell of the two-step atomizer with a purged vaporizer, and the atomic absorption of mercury is measured. It was found that the degree of mercury transfer and trapping is as high as 100% at sufficiently high temperatures of primary vaporization, regardless of the material of the inner surface of the atomizer cell. The detection limits for mercury were 0.24 or 0.024 µg/L for drinking water at a sample volume of 100 µL using a single sample transfer or the procedure repeated ten times, respectively, and 2.0 µg/L for urine at a sample volume of 20 µL and a single sample transfer. The accuracy of the results was confirmed by the analysis of certified mercury samples and samples with known additives.Translated from Zhurnal Analiticheskoi Khimii, Vol. 60, No. 1, 2005, pp. 45–51.Original Russian Text Copyright © 2005 by Vilpan, Grinshtein, Akatov, Gucer. 相似文献
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为提高土壤多元素同时检测的效率,采用超级微波消解-电感耦合等离子体发射光谱法测定土壤中钾、钠、钙、镁、铜、铁、锰、锌、磷、硫、硼、砷、镉、铬、铅、钴、镓、锂等18种元素含量。比较了超级微波消解、常规微波消解和电热板消解的处理效果,采用超级微波消解法对样品进行前处理,并优化了消解条件。在最优条件下,各元素的检出限在0.05~20 mg/kg,加标回收率在86.2%~107.5%,RSD在0.1%~3.0%,方法准确度及精密度可以满足多元素同时测定的需求,且该方法具有简单、快速、成本低、用酸量少、重现性好等特点。 相似文献
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In this paper we study the dispersion relation of thermal non-neutral plasma column by MHD theory. We use the dispersion relation to discuss the stability and dispersive properties in a non-neutral plasma-filled waveguide. The results are in agreement with those of cold non-neutral plasma. 相似文献
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Yuli YA. Gotlib 《Macromolecular Symposia》1999,146(1):81-87
The dynamic network model taken into account the friction relative to incompressible effective viscous medium (EVM), the hydrodynamic interactions of a network with the EVM, and the interchain friction is considered. Two collective network relaxation spectra (RS) arise. The first RS corresponds to the network motion relative to immobile EVM, the EVM does not take part in this motion. The second RS includes the combined viscous motion of the network and EVM because of long-range hydrodynamic interactions. This RS is finite and narrow for infinitely large network. The symmetry of this motion is in concordance with that of incompressible EVM. The existence of interchain friction leads to the narrowing of both types of relaxation spectra. 相似文献
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设k,n1和n2是3个正整数,G=(V1,V2;E)是一个二分图,使得|V1|=n1,|V2|=n2,其中n1≥2k+1,n2≥2k+1并且n1-n2≤1.如果对任意不相邻的x∈V1和y∈V2,都有d(x)+d(y)≥2k+2,则G包含k个相互独立的圈.以上结果部分地回答了Enomoto提出的关于二分图有独立圈的问题. 相似文献