超分子结构水杨酸根插层水滑石的组装及结构与性能研究

以锌铝水滑石ZnAl-CO3 LDHs为前体（主体），以乙二醇为分散介质，用离子 交换法组装了水杨酸根（客体）插层水滑石ZnAl-[o-HO(C6H4)COO]LDHs，并用XRD ，FT-IR，TG-DTA等手段对样品进行了表征。结果表明，能过控制离子交换条件， 水杨酸根阴离子可取代锌铝水滑石前体层间的CO3^2-离子，组装得到晶体结构良好 的水杨酸根插层水滑石。通过研究发现，主体水滑石层板与客体以静电力和氢键相 互作用，得到的超分子结构材料紫外阻隔作用增强并具有较好的稳定性，从而成为 一种集屏蔽和吸收双重功能的新型无机-有机得合紫外阻隔材料。     

表面附聚薄壳型单分散高效阳离子柱填料的研制及其性能

 报道了一种新的表面附聚薄壳型阳离子柱填料的简易制备方法。首次合成了单分散高效阳离子柱填料。以10μm的单分散聚苯乙烯 二乙烯基苯(PSTDVB)微球为基球,对其表面季铵化,然后均匀附聚一层磺化的阳离子乳胶(0 2μm),即得到阳离子固定相。分别用碱金属及碱土金属离子对用该填料制成的柱的性能进行了测试,结果表明该柱填料对常见阳离子具有很好的分离效果、良好的重现性和低的检测限。     

重力储能放能效率探究

为了顺应未来能源“低碳”、“绿色”发展趋势，搭建实验装置探究重力储、放能及影响其效率的相关因素。实验结果表明，重力储、放能效率在一定重物质量、供电电压大小下存在最佳峰值。实验装置结构简单，易于搭建，适合对重力储能放能展开研究。     

Direct Observation of High-Temperature Superconductivity in One-Unit-Cell FeSe Films

We prepared one-unit-ceil （1-UC） thick FeSe films on insulating SrTiOa substrates with non-superconducting FeTe protection layers by molecular beam epitaxy for ex situ studies. By direct transport and magnetic measurements, we provide definitive evidence for high temperature superconductivity in the 1-UC FeSe films with an onset Tc above 40 K and an extremely large critical current density fie Jc-1.7× 106 A/cm2 at 2K, which are much higher than Tc-8K and Jc-104 A/cm^2 for bulk FeSe, respectively. Our work may pave the way to enhancing and tailoring superconductivity by interface engineering.     

Superconductivity and Fermi Surface Anisotropy in Transition Metal Dichalcogenide NbTe_2

Transition metal dichalcogenides, featuring layered structures, have aroused enormous interest as a platform for novel physical phenomena and a wide range of potential applications. Among them, special interest has been placed upon WTe_2 and MoTe_2, which exhibit non-trivial topology both in single layer and bulk as well as pressure induced or enhanced superconductivity. We study another distorted IT material NbTe_2 through systematic electrical transport measurements. Intrinsic superconductivity with onset transition temperature(T_c~(onset)) up to 0.72 K is detected where the upper critical field(H_c) shows unconventional quasi-linear behavior,indicating spin-orbit coupling induced p-wave paring. Furthermore, a general model is proposed to fit the angledependent magnetoresistance, which reveals the Fermi surface anisotropy of NbTe_2. Finally, non-saturating linear magnetoresistance up to 50 T is observed and attributed to the quantum limit transport.     

Electronic transport properties of topological insulator films and low dimensional superconductors

In this review, we present a summary of some recent experiments on topological insulators （TIs） and superconducting nanowires and fihns. Electron electron interaction （EEI）, weak anti-localization （WAL） and anisotropic magneto-resistance （AMR） effect fbund in topological insulator fihns by transport measurements are reported. Then, transport properties of superconducting films, bridges and nanowires and proximity effect in non-superconducting nanowires are described. Finally, the interplay between topological insulators and superconductors （SCs） is also discussed.     

油气太赫兹光谱仪时域谱的误差分析与标定

在针对油气产品进行太赫兹光谱测试时,仪器自身误差会为测试结果来较大影响,对实验仪器进行误差标定对油气资源的太赫兹表征与精细评价具有重要意义。对油气太赫兹光谱仪进行了误差测试与分析,并对由延迟线的移动速度导致的测试误差进行了标定。结果表明,较小的移动速度有利于减少时域波形在延迟时间与幅值上产生的偏差及浮动,其中4组实验延迟时间的浮动范围分别为0.1Ps、0.1Ps、0.2Ps和0.4Ps;信号幅值的误差率分别为2.26%,1.76%,3.28%及5.82%。此外,在测试过程中,激光器输出功率的变化也是主要的误差来源,在测试时通过实时记录输出功率并根据线性关系进行归一化处理可降低这一误差。