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本文提供了提高现有活塞圆筒式高压装置流体静压强的一种实验方法。成功地制作了锰铜丝压力计,并利用铋丝相变准确地做了压力校正。各箍的应力检测分析和相对位移测量都表明:无论压腔空载或充液时,在0.000 1~3.08 GPa均不显示出同步箍紧作用;上下缸的压强差偏大带来高压暴露的危险。为把流体静压强提高到3.08 GPa以上,建议改进设计;(1)内箍中箍合二为一,外箍分为上下二层,将增加箍力;(2)调整各箍之间接触圆锥面的面积,将有助于同步箍紧;(3)增大密封套圈的无支承面,将减少上下缸压差,有利于安全运行。 相似文献
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X-ray absorption fine structure (XAFS) spectroscopy is a powerful technique for the investigation of the local environment around selected atoms in condensed matter. XAFS under pressure is an important method for the synchrotron source. We design a cell for a high pressure XAFS experiment. Sintered boron carbide is used as the anvils of this high pressure cell in order to obtain a full XAFS spectrum free from diffraction peaks. In addition, a hydraulic pump was adopted to make in-suit pressure modulation. High quality XAFS spectra of ZrH2 under high pressure (up to 13 GPa) were obtained by this cell. 相似文献
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