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本文采用静电纺丝法制备出不同前驱条件下的TiO_2纳米纤维。用扫描电镜对样品的形貌进行表征,结果表明纤维直径约为100nm且表面粗糙;X-射线衍射和拉曼结果显示不同前驱条件制备的样品中锐钛矿相与金红石相的比例不同;利用紫外可见分光光度计测试TiO_2纳米纤维对亚甲基蓝的光催化活性分析所制样品的光催化活性,结果表明加热条件下样品的活性更高;原因是加热条件下金红石相的含量更多,两相混合为电子跃迁提供更多的跃迁能级,增加了光生电子和空穴的寿命,从而减少两者的复合几率,提高TiO_2纳米纤维的光催化活性。 相似文献
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Structural and Photoluminescence Properties of β-Ga2O3 Nanofibres Fabricated by Electrospinning Method 下载免费PDF全文
We have prepared the 13-Ga2 O3 nanofibres by electrospinning method followed by calcining in air at 900℃. The morphology and structure of the nanofibres are characterized by field emission scanning electron microscopy (FE-SEM), x-ray diffraction (XRD) and Raman technique. These nanofibres have diameters ranging from 60 to 130hm and lengths up to several millimetres. Photoluminescence (PL) spectrum under excitation at 325 nm shows that theseβ-Ga2 O3 nanofibres have a blue emission peaking at 466nm, which may be attributed to defects such as the oxygen vacancies, gallium vacancies and gallium-oxygen vacancy pairs. 相似文献
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Structure and photoluminescence properties of Er3+-doped TiO2-SiO2 powders prepared by sol-gel method 下载免费PDF全文
Er 3+-doped TiO 2-SiO 2 powders are prepared by the sol-gel method,and they are characterized by high resolution transmission electron microscopy (HR-TEM),X-ray diffraction (XRD) spectra,and Raman spectra of the samples.It is shown that the TiO 2 nanocrystals are surrounded by an SiO 2 glass matrix.The photoluminescence (PL) spectra are recorded at room temperature.A strong green luminescence and less intense red emission are observed in the samples when they are excited at 325 nm.The intensity of the emission,which is related to the defect states,is strongest at the annealing temperature of 800 C.The PL intensity of Er 3+ ions increases with increasing Ti/Si ratio due to energy transfer between nano-TiO 2 particles and Er 3+ ions. 相似文献
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利用低压化学气相沉积方法在以Au作催化剂的Si衬底上生长了InN纳米线. 扫描电子显微镜分析表明,这些纳米线的直径在60—100 nm的范围内, 而其长度大于1 μm.高分辨透射电子显微镜图像表明,合成的纳米线中含有六方相和立方相的InN晶体.这些InN纳米线具有良好的场发射特性和稳定的场发射电流,其开启场为10.02 V/μm(电流密度为10 μA/cm2),在24 V/μm 的电场下,其电流密度达到5.5 mA/cm2.此外,对InN纳米线的场发射机理也进行了讨论.
关键词:
InN纳米线
场电子发射
非线性Fower-Nordheim曲线 相似文献
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