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Two new dicyanamide coordination polymers, {Mn(dmpz)[N(CN)2]2}2 (1) and {Cu(dmpz)[N(CN)2]2}2 (2)(dmpz=3,5-dimethylpyrazole), were synthesized and characterized by single crystal X-ray diffraction analysis and IR spectroscopy. In 1 and 2 the metal ions have two different coordination modes, where one is coordinated to four dicyanamide anions and two monodentate dmpz molecules to form a slightly distorted octahedral geometry, while the other adopts octahedral geometry, surrounded by four nitrile N atoms and two amide N atoms of the dicyanamide anions. Both complexes contain two alternating chains that are parallel to each other. 相似文献
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讨论格自仿Tile的边界结构,得到平面格自仿Tile的边界为简单闭曲线的一个充分条件;作为应用,给出Bandt-Wang的一个定理的新证明. 相似文献
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A prototype of a device with an impact structure for measuring the floor tilt has been built in our laboratory. The mechanical construction and the capacitive transducer of the device are introduced. Experimental results indicate that the floor tilt is about 16#tad in our cavity laboratory, and the uncertainty AG/G caused by such tilt is less than 0.54 parts per million (ppm), so the floor tilt can be reasonably neglected in the experimental determination of the gravitational constant G with the total uncertainty of about l0ppm. 相似文献
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A phenomenological study on the fitting method in real time has been done, and the method was applied to process and analyze the extensive data of a long period torsion pendulum used to determine Newtonian gravitational constant G. The result shows that the fitting method in real time is effective to determine the period of a torsion pendulum with a relative precision of 10-5 orders. 相似文献
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OPTIMUM DURATION OF MEASUREMENT FOR REDUCING THERMAL NOISE LIMITATIONS IN TORSION PENDULUM EXPERIMENTS
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Statistical estimates of thermal noise fluctuation of a linear harmonic oscillator used to detect weak forces are reexamined with special reference to gravitational experiments. Thermal noise limitation on the measurement of displacement of an oscillator is studied. It is found that the signal response of an oscillator reaches the maximum value while the thermal noise response reaches the minimum value at the same time during the transient state of the oscillator, and the precision of the experiments in the transient state could increase about two orders higher than that in the equilibrium state for typical experiments. It is also found that there is an optimum duration of measurement in which the uncertainty due to thermal noise in this period is the least. 相似文献
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本文通过对蓬安县三元水库大坝外坡裂缝产生的原因分析,进而运用岩、土力学的理论与方法反算推论出了裂缝的产生不是深层坝体土滑动引起的,而是局部浅层坝体土在水的诱发作用下作蠕滑-拉裂变形所产生的。在明确了大坝裂缝产生的原因后,提出了一系列相应整治工程措施,以达到彻底根治裂缝和稳固大坝的目的。 相似文献
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A torsion balance is constructed to accurately measure the magnetic properties of the real proof mass of the inertial sensor. The magnetic susceptibility and remnant moment of a titanium proof mass are measured in the first experiment, and further improvements and the potential sensitivity are also discussed. This is significant for choosing the material of the proof mass and investigating the magnetic disturbances acting on the proof mass. 相似文献