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通过水热合成法和溶胶凝胶法制备Fe_3O_4@NiSiO_3磁性纳米粒子,该纳米粒子微球具有均一的形貌、良好的磁性和分散性。将合成的Fe_3O_4@NiSiO_3磁性纳米粒子作为磁性固相萃取(MSPE)介质,并结合高效液相色谱(HPLC)建立了水样中痕量微囊藻毒素MC-LR的分析方法。在优化实验条件下,方法在0.25~146.5μg/L浓度范围内呈良好的线性关系,相关系数(r)为0.999 1,检出限为0.011μg/L。将该方法用于纯水中微囊藻毒素的分析,回收率为81.0%,对实际水样的回收率为66.7%~72.0%。表明Fe_3O_4@NiSiO_3磁性纳米粒子具有良好的选择性富集能力,可用于水中痕量微囊藻毒素的萃取。 相似文献
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An electro-optic tunable rectangular array illuminator in one-dimensional periodically poled LiNbO3 (PPLN) crystal is presented experimentally which result is in good agreement with results from simu- lation. The illuminator is formed based on the Talbot self-imaging effect by applying an electric field on PPLN. The intensi~.y distribution of rectangular array could be precisely modulated. Compared with other array illuminators, this tunable illuminator uses a lower voltage and could get a more concentrated intensity distribution. The influence of the incident angle to the self-imaging patterns is studied for the first time. 相似文献
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