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非水毛细管电泳测定黄连饮片中5种生物碱 总被引:1,自引:0,他引:1
建立了一种非水毛细管电泳(NACE)同时测定黄连饮片生品与炮制品中小檗碱、巴马汀、药根碱、木兰碱和黄连碱含量的方法。分别考察了非水溶剂、缓冲液体系及其浓度和pH、运行电压、运行温度和检测波长等条件对实验结果的影响。在优化的实验条件下,选择非水毛细管电泳分离模式,以40 mmol/L乙酸钠-40 mmol/L乙酸铵的无水甲醇缓冲溶液(pH 5.8)为电泳介质,未涂渍标准熔融石英毛细管(64.5 cm×75 μm,有效长度56 cm)为分离通道,检测波长为254 nm,分离电压为25 kV,压力进样(5 kPa×6 s),柱温为20 ℃。结果显示,5种生物碱在20 min内可实现基线分离,加标回收率为98.37%~101.03%。该方法简单、准确,重现性较好,可用于黄连饮片内在质量的评价和控制。 相似文献
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In this paper we consider general coupled mean-field reflected forward-backward stochastic differential equations(FBSDEs),whose coefficients not only depend on the solution but also on the law of the solution.The first part of the paper is devoted to the existence and the uniqueness of solutions for such general mean-field reflected backward stochastic differential equations(BSDEs) under Lipschitz conditions,and for the one-dimensional case a comparison theorem is studied.With the help of this c... 相似文献
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