紫外分光光度法测定蔬菜鲜样中的硝酸盐

建立了紫外分光光度法测定蔬菜鲜样中硝酸盐含量的方法，经t检验证明，该方法的测定结果与酚二磺酸法无显著性差异，RSD小于4．5％，方法操作简便，适用于蔬菜中硝酸盐含量的测定。     

Existence in the Large for Pressure-Gradient System

In this paper, the authors use Glimm scheme to study the global existence of BV solutions to Cauchy problem of the pressure-gradient system with large initial data. To this end, some important properties of the shock curves of the pressure-gradient system in the Riemann invariant coordinate system and verify that the shock curves satisfy Diperna’s conditions (see [Diperna, R. J., Existence in the large for quasilinear hyperbolic conservation laws, Arch. Ration. Mech. Anal., 52(3), 1973, 244–257]) are studied. Then they construct the approximate solution sequence through Glimm scheme. By establishing accurate local interaction estimates, they prove the boundedness of the approximate solution sequence and its total variation.     

A global pinching theorem for compact surfaces inS 3 with constant mean curvature

LetM be a compact minimal surface inS ³. Y. J. Hsu^[5] proved that if S₂22, thenM is either the equatorial sphere or the Clifford torus, whereS is the square of the length of the second fundamental form ofM, ·₂ denotes theL ²-norm onM. In this paper, we generalize Hsu's result to any compact surfaces inS ³ with constant mean curvature.Supported by NSFH.     

Detection of individual insulating entities by electrochemical blocking

Electrochemical blocking is a type of single-entity electrochemical measurement particularly well adapted to the detection of insulating particles. The digital detection of ultralow concentrations of artificial entities such as polymer particles or biotargets such as proteins and bacteria represents an exceptional opportunity for sensing applications. In this review, we explore the latest development in the field of electrochemical blocking and propose some perspectives.     

Hydrogen Treatment for Superparamagnetic VO2 Nanowires with Large Room‐Temperature Magnetoresistance

One‐dimensional (1D) transition metal oxide (TMO) nanostructures are actively pursued in spintronic devices owing to their nontrivial d electron magnetism and confined electron transport pathways. However, for TMOs, the realization of 1D structures with long‐range magnetic order to achieve a sensitive magnetoelectric response near room temperature has been a longstanding challenge. Herein, we exploit a chemical hydric effect to regulate the spin structure of 1D V–V atomic chains in monoclinic VO₂ nanowires. Hydrogen treatment introduced V³⁺ (3d²) ions into the 1D zigzag V–V chains, triggering the formation of ferromagnetically coupled V³⁺–V⁴⁺ dimers to produce 1D superparamagnetic chains and achieve large room‐temperature negative magnetoresistance (?23.9 %, 300 K, 0.5 T). This approach offers new opportunities to regulate the spin structure of 1D nanostructures to control the intrinsic magnetoelectric properties of spintronic materials.     

Preparative isolation and purification of anti‐tumor agent ansamitocin P‐3 from fermentation broth of Actinosynnema pretiosum using high‐performance counter‐current chromatography

Ansamitocin P‐3 is a potent anti‐tumor maytansinoid found in Actinosynnema pretiosum. However, due to the complexity of the fermentation broth of Actinomycete, how to effectively separate ansamitocin P‐3 is still a challenge. In this study, both analytical and preparative high‐performance counter‐current chromatography were successfully used to separate and purify ansamitocin P‐3 from fermentation broth. A total of 28.8 mg ansamitocin P‐3 with purity of 98.4% was separated from 160 mg crude sample of fermentation broth in less than 80 min with the two‐phase solvent system of hexane–ethyl acetate–methanol–water (0.6:1:0.6:1, v/v/v/v). The purity and structural identification were determined by HPLC, ¹H NMR, ¹³C NMR and mass spectroscopy.     

A direct connection between quantum Hall plateaus and exact pair states in a 2D electron gas

It is previously found that the two-dimensional (2D) electron-pair in a homogeneous magnetic field has a set of exact solutions for a denumerably infinite set of magnetic fields. Here we demonstrate that as a function of magnetic field a band-like structure of energy associated with the exact pair states exists. A direct and simple connection between the pair states and the quantum Hall effect is revealed by the band-like structure of the hydrogen “pseudo-atom”. From such a connection one can predict the sites and widths of the integral and fractional quantum Hall plateaus for an electron gas in a GaAs-Al _x Ga_1−x As heterojunction. The results are in good agreement with the existing experimental data.     

On spacelike hypersurfaces with constant scalar curvature in the de Sitter space

We classify spacelike hypersurfaces of the de Sitter space with constant scalar curvature and with two principal curvatures. Moreover, we prove that if Mn is a complete spacelike hypersurface with constant scalar curvature n(n−1)R and with two distinct principal curvatures such that the multiplicity of one of the principal curvatures is n−1, then R<(n−2)c/n. Additionally, we prove several rigidity theorems for such hypersurfaces.