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The objective of this study was to describe the radiochemical characteristics of electric arc furnace (EAF) slag from Croatian EAF black steel slags, generated from carbon steel production process in CMC Sisak d.o.o., and steel mill in Split in order to enhance the understanding of possibilities for their use in road construction. This article presents the results of radionuclide in electric arc furnace steel slag. The presence of natural isotopes 40K, 232Th (228Ra), 226Ra and 238U was established. The measured activity in slag natural isotopes lies within the Croatian legally permitted limits.  相似文献   
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A two step sequence converts certain cyclic enones to fused methylenecyclopentanes using the annulation reagent 2-chloromethyl-3-trimethylsilylpropene.  相似文献   
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This article presents the results of 137Cs and other radionuclide monitoring in EAF steel-making process in the Croatian CMC Sisak Steel Mill. The presence of 137Cs and natural isotopes 40K, 232Th, 226Ra and 238U was established. Investigations on the occurrence of the isotope cesium, as well as natural isotopes and their distribution in waste from the process of carbon steel production by EAF have been conducted. Detection of artificial isotope cesium in EAF dust indicates that it might originate from steel scrap or from the residue of the material that was used in the technological process, thus deserving special attention.  相似文献   
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The mechanism by which dihydro-5-(3'-trifluoroacetoxypropyl)-2(3H)-furanone is formed when 3-(tetrahydro-2'-furyl)propanoic-trifluoroacetic mixed anhydride is treated with an acidic catalyst is defined, and routes to some potentially useful butanolide synthons are described.  相似文献   
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A fast, sensitive, and selective method for the determination of histamine in human urine samples by ultrahigh pressure liquid chromatography (LC) with fluorescence and mass spectrometry (MS) detection is investigated. A fluorescent reagent, 4-(1-pyrene) butyric acid N-hydroxysuccinimide ester was conjugated to the primary and secondary amino moieties of histamine. The structure of dipyrene-labeled histamine in human urine was determined by quadrupole time-of-flight MS with electospray ionization interface. The determination of the dipyrene derivative of histamine in urine samples was achieved within 3.9 min on an ultrahigh pressure LC Eclipse Zorbax XDB-C(18) column with 1.8 μm particle diameter. In this work, histamine separation was achieved significantly faster (3.9 min) with improved detection limit (signal-to-noise = 3) of 0.04 nM than 19.5 min with a detection limit of 0.183 nM as reported in a previous method.  相似文献   
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This paper describes an approach for generating lower bounds for the curriculum-based course timetabling problem, which was presented at the International Timetabling Competition (ITC-2007, Track 3). So far, several methods based on integer linear programming have been proposed for computing lower bounds of this minimization problem. We present a new partition-based approach that is based on the “divide and conquer” principle. The proposed approach uses iterative tabu search to partition the initial problem into sub-problems which are solved with an ILP solver. Computational outcomes show that this approach is able to improve on the current best lower bounds for 12 out of the 21 benchmark instances, and to prove optimality for 6 of them. These new lower bounds are useful to estimate the quality of the upper bounds obtained with various heuristic approaches.  相似文献   
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The accurate identification of Cryptosporidium (Protozoa: Apicomplexa) species and genotypes is central to the understanding of the transmission and to the diagnosis and control of cryptosporidiosis. In this study, we demonstrate the effectiveness of nonisotopic SSCP analysis of a approximately 300 bp region of the small subunit (pSSU) of ribosomal DNA for the specific identification of and delineation among 18 different Cryptosporidium species and genotypes from a wide range of hosts. This mutation scanning approach allowed the rapid and reliable differentiation between species/genotypes differing by as little as 1.3% in the pSSU sequence, with the capacity to detect point mutations. The present findings confirm the usefulness of this tool for the rapid genetic screening of Cryptosporidium samples from any host species, providing a foundation for detailed systematic, epidemiological and ecological studies. Although applied herein to pSSU, this low cost approach should be applicable to a wide range of genetic loci for population genetic investigations of Cryptosporidium.  相似文献   
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Mycobacterium neoaurum demethylates both methylarsonic acid and methylarsonous acid to mixtures of arsenate and arsenite. After 28 days of incubation, the yields of inorganic arsenic were 27% from arsenate and 43% from arsenite. A time study of the demethylation of methylarsonic acid by M. neoaurum showed that demethylation occurs rapidly during the growth and stationary phases of the bacterium, and indicates that MMA(V) is reductively demethylated to arsenite. Copyright © 2003 John Wiley & Sons, Ltd.  相似文献   
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