A facile synthesis of steroidal D-ring fused pyrazolo[1,5-a]pyrimidines

A facile method for the synthesis of steroidal D-ring fused pyrazolo[1,5-a]pyrimidines through a microwave mediated reaction between steroidal β-bromovinyl aldehydes and pyrazoloamines using palladium(II) catalyst has been described.     

A facile synthesis of benzo[b][1,4]thiazepine derivatives by palladium acetate catalyzed reaction

The preparation of steroid/nonsteroid fused benzo[b][1,4]thiazepines and 2-arylsubstituted benzo[b][1,4]thiazepines is described from Pd(OAc)₂ catalyzed reaction of steroidal/nonsteroidal β-halovinyl aldehydes and 2-aminothiophenols in DMF under heating condition.     

Constrained moving least‐squares immersed boundary method for fluid‐structure interaction analysis

A numerical method is presented for the analysis of interactions of inviscid and compressible flows with arbitrarily shaped stationary or moving rigid solids. The fluid equations are solved on a fixed rectangular Cartesian grid by using a higher‐order finite difference method based on the fifth‐order WENO scheme. A constrained moving least‐squares sharp interface method is proposed to enforce the Neumann‐type boundary conditions on the fluid‐solid interface by using a penalty term, while the Dirichlet boundary conditions are directly enforced. The solution of the fluid flow and the solid motion equations is advanced in time by staggerly using, respectively, the third‐order Runge‐Kutta and the implicit Newmark integration schemes. The stability and the robustness of the proposed method have been demonstrated by analyzing 5 challenging problems. For these problems, the numerical results have been found to agree well with their analytical and numerical solutions available in the literature. Effects of the support domain size and values assigned to the penalty parameter on the stability and the accuracy of the present method are also discussed.     

A novel microwave-mediated one-pot synthesis of indolizines via a three-component reaction

[reaction: see text] The microwave-mediated three-component reaction of acyl bromide, pyridine, and acetylene is catalyzed by basic alumina to give corresponding indolizines in excellent yields in a one-pot reaction.     

Dynamic responses of orthotropic plates under moving masses

Summary The problem considered is that of heavy masses moving on lightweight rectangular plates of orthotropic materials, slated for use in space structures. The dynamic equation of motion for orthotropic plates which contains singularities in both space and time variables is first presented. The response is expressed as a summation of double series of eigenfunctions. The equation of motion is transformed into an integro-differential equation for modal amplitudes using the Green's function. The Green's function is chosen to satisfy the initial conditions, the boundary conditions, and the transient conditions due to the moving masses. The solution series exhibits a good convergence. The effect of orthotropicity on natural frequencies and dynamic responses is demonstrated.

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Dynamische Antwort orthotroper Platten auf bewegte Massenpunkte

übersicht Behandelt wird die Bewegung von Massenpunkten auf rechteckigen Leichtbau-Platten aus orthotropem Werkstoff, die für Raumfahrtkonstruktionen vorgesehen sind. ZunÄchst wird die Bewegungsgleichung orthotroper Platten mit singulÄren Ausdrücken in den Raum- und Zeitkoordinaten angegeben. Die Antwort wird als Doppelsumme einer zweifachen Reihenentwicklung dargestellt und die Bewegungsgleichung mit Hilfe der Greenschen Funktion in eine Integro-Differentialgleichung für die Modalamplituden transformiert. Die Greensche Funktion ist so gewÄhlt, da\ sie die Anfangs- und Randbedingungen sowie die übergangsbedingungen unter der bewegten Masse erfüllt. Die Lösung durch Reihenentwicklung zeigt gute Konvergenz. Der Einflu\ der Orthotropie auf die Eigenfrequenzen und die dynamischen Antworten wird veranschaulicht.

     

Matrix multiplication operators on Banach function spaces

In this paper, we study the matrix multiplication operators on Banach function spaces and discuss their applications in semigroups for solving the abstract Cauchy problem.     

Homotopies for computation of fixed points on unbounded regions

Givenf: R ⁿ R ^n* with some conditions, our aim is to compute a fixed pointx f(x) off; hereR ⁿ isn-dimensional Euclidean space andR ^n* is the collection of nonempty subsets ofR ⁿ . A typical application of the algorithm can be motivated as follows: Beginning with the constant mapf ₀:R ⁿ {0} R ⁿ and its fixed pointx ₀ = 0, we deformf _t ast tof f and follow the pathx _t of fixed points off _t . Cluster points of thex _t 's ast are fixed points off. This research was supported in part by Army Research Office-Durham Contract DAHC-04-71-C-0041 and by National Science Foundation Grant GK-5695.     

Composition operators on Banach function spaces

We study the boundedness and the compactness of composition operators on some Banach function spaces such as absolutely continuous Banach function spaces on a -finite measure space, Lorentz function spaces on a -finite measure space and rearrangement invariant spaces on a resonant measure space. In addition, we study some properties of the spectra of a composition operator on the general Banach function spaces.

     

Supersymmetric solution of gauge hierarchy problem

Some recent developments with respect to the resolution of the gauge hierarchy problem in grand unified theories by supersymmetry are presented. A general argument is developed to show how global supersymmetry maintains the stability of the different mass-scales under perturbative effects.     

A property of matrices with positive determinants

Let $\text{P}$ be the set of all n × n real matrices which have a positive determinant. We show here that at least 2^{n ? 1} matrices are needed to “see” each matrix in $\text{P}$. Also, any finite subset of $\text{P}$ can be “seen” from a class of at most 2^{n ? 1} matrices in $\text{P}$.