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A sensitive and specific method for the determination of bencyclane in human plasma is presented. Bencyclane was extracted from human plasma with two 3-ml volumes of isooctane and was shaken for 10 min. The organic phase was separated and evaporated to dryness at 40 degrees C under a nitrogen stream. The residue was dissolved and an aliquot was injected into the gas chromatograph. The separation was performed with a DB-17 column with helium as the carrier gas. Nitrogen-selective detection was performed. The quantification was performed with the signal output. The limit of detection was 1 ng/ml. 相似文献
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In this paper we describe a disposable sodium sensor in double matrix membrane technology. This sensor is prepared from filter paper with an evaporated silver conducting line on one side. For insulation the sensor is laminated with a pre-perforated heat-sealing film. A defined volume of an ion-sensitive polymer matrix membrane cocktail is filled into one hole. So an ion-sensitive coated film sensor in double matrix membrane technology is produced. The double matrix membrane is formed by the polymer matrix membrane and by the additional filter paper matrix. The response behaviour of the sodium electrode is comparable with conventional macro ion-selective electrodes. By this technology a mass production of low cost sensors is possible. 相似文献
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Analysis of cigarette mainstream smoke for 1,1-dimethylhydrazine and vinyl acetate by gas chromatography-mass spectrometry 总被引:3,自引:0,他引:3
1,1-Dimethylhydrazine, also known as unsymdimethylhydrazine (UDMH) and vinyl acetate (VA), are both classified by the International Agency for Research on Cancer as 2B carcinogens (possibly carcinogenic to humans) and listed as cigarette smoke constituents; however, there is little or no quantitative data available on them. For UDMH in cigarette smoke, neither a yield nor a method has been published. For VA, the most recent information on yields dates back to 1965. To bridge this gap, we have developed new gas chromatographic-mass spectrometric methods for both compounds to determine their yields in cigarette smoke. UDMH is determined by derivatization with 2-nitrobenzaldehyde in methanol and is not found in cigarette smoke at levels above the detection limit of 19 ng/cig. In further experiments, when UDMH is added to the smoke stream or air stream of lit or unlit cigarettes, the derivative 2-nitrobenzaldehyde-2,2-dimethylhydrazone is found only in the air stream of the unlit cigarettes. From this, we conclude that UDMH is either not formed during smoking at all or, if it is, it reacts immediately and quantitatively with other smoke constituents (e.g., aldehydes) and is therefore not detectable in cigarette smoke. VA is determined by trapping in acetone at -78 degrees C and is found at a concentration of 270 ng/cig for a standard reference cigarette with a cellulose acetate filter (the reference cigarette 1 R4F). In the literature, VA is reported at concentrations of 1.6 microg/cig for a cigarette with a cellulose acetate/charcoal filter and 4 microg/cig for a cigarette with a cellulose acetate filter and for an unfiltered cigarette. 相似文献
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J. Diekmann 《Mathematische Annalen》1871,4(3):442-475
Ohne Zusammenfassung 相似文献
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O. Diekmann 《Journal of Differential Equations》2005,215(2):268-319
The paper is aimed as a contribution to the general theory of nonlinear infinite dimensional dynamical systems describing interacting physiologically structured populations. We carry out continuation of local solutions to maximal solutions in a functional analytic setting. For maximal solutions we establish global existence via exponential boundedness and by a contraction argument, adapted to derive uniform existence time. Moreover, within the setting of dual Banach spaces, we derive results on continuous dependence with respect to time and initial state.To achieve generality the paper is organized top down, in the way that we first treat abstract nonlinear dynamical systems under very few but rather strong hypotheses and thereafter work our way down towards verifiable assumptions in terms of more basic biological modelling ingredients that guarantee that the high level hypotheses hold. 相似文献
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D. Aston M. Atkinson R. Bailey A.H. Ball B. Bouquet G.R. Brookes J. Br?ring P.J. Bussey D. Clarke A.B. Clegg B. DAlmagne G. De Rosny B. Diekmann A. Donnachie M. Draper B. Drevillon I.P. Duerdoth J.-P. Dufey T.P. Yiou 《Physics letters. [Part B]》1981,104(3):231-234
The reaction γp → K+K? p has been investigated with tagged photons in the energy range of 20 < Eγ < 70 GeV. A structure in the 1.7 GeV mass region is observed and interpreted in terms of a recurrence of the ø. 相似文献