控温相变免疫分析测定雌酮

通过热引发聚合与氧化还原引发聚合，合成水凝胶，作为雌酮全抗原(E1— BSA)载体；以异硫氰基灾光素标记雌酮的单克隆抗体(McAb)作为示踪剂，建立了控温相变竞争免疫分析测定雌酮(EI)的方法并应用于分析血清样品。实验表明：以热引发聚合合成的水凝胶为载体的荧光免疫分析方法具有更高的灵敏度，它的线性范围为10-700μg/L，检出限为1μg／L(n=10，3倍空白)。经水凝胶性质的比较(包括LCST、非特异性吸附、抗原与抗体反应时间及固定化抗原活性)，证明了热引发聚合的水凝胶较氧化还原引发聚合的水凝胶更适合于作为免疫分析的载体。     

ELECTROCHROMETIC STUDIES ON POLAR MULTILAYERS OF LIQUID CRYSTALLINE POLYMERS

Electrochrometic measurements were carried on the Z-type Langmuir-Blodgett films oftwo liquid crystalline polymers: mono-{6-[4-(phenylazo) naphthyloxy] hexyl} (1a) andmono-{6-[4-(anthraquinone-1-azo) naphthyloxy] hexyl} (2a) ester of polymaleic acid. Itwas found that for both polymers, poling fields parallel and antiparalle1 to dipole momentsof the polymer side chains induce red and blue shift in absorption bands, respectively. Forpolymer la blue shift is accompanied by absorbance increase, while red shift by absorbancedecrease;but for polymer 2a only decrease in absorbance is observed. A simple model wasproposed to analyze the results.     

Global Regularity of 3D Nonhomogeneous Incompressible Micropolar Fluids

This paper is concerned with the global well-posedness of strong and classical solutions for the 3D nonhomogeneous incompressible micropolar equations with vacuum. We prove that the problem (1.1)–(1.5) has a unique global strong/classical solution \((\rho,u,w)\), provided \(\mu_{1}\) is sufficiently large, or \(\|\rho_{0}\|_{L^{\infty}}\) or \(\|\rho_{0}^{1/2}u_{0}\| ^{2}_{L^{2}}+\|\rho_{0}^{1/2}w_{0}\|^{2}_{L^{2}}\) is small enough.

     

In-situ grown metal organic framework synergistic system for the enantioseparation of three drugs in open tubular capillary electrochromatography

Metal organic frameworks have received great attention as the chiral stationary phase for racemic drug separation because of their fascinating structures and properties. However, the most homochiral metal organic frameworks were constructed by rare and precious chiral organic ligands. In this work, an achiral metal organic framework, together with a natural chiral selector carboxymethyl β-cyclodextrin built a synergistic separation system in the open tubular capillary electrochromatography. The novel coated columns were developed by inducing metal organic framework nanoparticles to grow on the imidazolyl functional capillary inner wall. The baseline separations of hydroxychloroquine, ofloxacin, and atenolol were achieved in the synergistic separation system. The effects of the concentration of chiral selector, pH, voltage, and the concentration of organic additives were studied. Compared with chiral selector auxiliary bare capillary, the resolutions of three drugs were remarkably improved. The relative standard deviations for the retention time of intraday (n = 6), interday (n = 6), and column-to-column were less than 2.1, 2.6, and 5.2%, respectively. These results demonstrate that affordable synergistic separation systems are prospective for racemic drug enantioseparation in capillary electrochromatography.     

A New Regularity Criterion for the 3D MHD Equations Involving Partial Components

In this paper, we establish a new regularity criterion for the 3D incompressible MHD equations involving partial components of the velocity gradient and magnetic fields.     

Blow-up,Global Existence and Persistence Properties for the Coupled Camassa–Holm equations

In this paper, we consider the coupled Camassa–Holm equations. First, we present some new criteria on blow-up. Then global existence and blow-up rate of the solution are also established. Finally, we discuss persistence properties of this system.     

《大音希声--应崇福传》将于近期出版

2010年春天,根据国务院领导同志批示,中国科协启动了"老科学家学术成长资料采集工程"项目（2010CJGC03）。由时任中国科协常务副主席、书记处第一书记邓楠同志担任组长,由中组部、教育部、科技部、工业和信息化部、财政部、文化部、国资委、解放军总政治部等部副部长,中国科学院、中国工程院副院长,国家自然科学基金委副主任,中国科协副主席等组成采集工程领导小组及相关领导组成领导小组办公室。下设采集工程项目办公室及以采集对象为单位的采集小组。我国著名物理学家、超声学研究奠基人、声学领域著名教育家、中国声学学会第一届理事长、中国科学院声学研究所创建人之一、中国科学院资深院士应崇福先生被列入首批采集对象。