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1.
This paper is a report on the complexation studies of silverions with certain water soluble crown ethers viz., 15-crown-5,18-crown-6, cyclam, diaza 15-crown-5 and certain water insolublecrown ethers viz., benzo 15-crown-5, dibenzodiaza 15-crown-4,dibenzyldiaza 18-crown-6 in some nonionic surfactants viz.,polyoxyethylated alkyl phenol (TX 100), polyoxyethylene (20)sorbiton monolaurate (Tween 20), polyoxyethylene (20) sorbitonmonoleate (Tween 80) and polyoxyethylated glyco monolaurylether (Brij 35) by potentiometry. In addition, conductometry wasalso used to study the complexation of oxa crown ethers to comparethe results obtained by potentiometry, which were found to be ingood agreement with each other. The complexation studies indicate1:1 complex formation between the silver ion and macrocycle, thelogML n+ values being in the range 1 to 9.  相似文献   
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An electro-optic holographic technique (also called electronic speckle pattern interferometry or TV holography) for the measurement of displacements and strains on three-dimensional object surfaces is presented. The three components of the displacement vector, in a fixed coordinate system, are separated using four independent illumination beams. The interferometric phase for each illumination beam is extracted using the phase stepping technique. Displacements in the fixed coordinate system are projected on to the object surface using the tensor transformation law. Equations for the computation of surface strains using the projected displacements and the surface geometry are developed. The technique is applied for the measurement of strains on the surface of a cylindrical vessel subjected to internal pressure.  相似文献   
3.
Quantum wire (QWR) heterostructures suitable for optoelectronic applications should meet a number of requirements, including defect free interfaces, large subband separation, long carrier lifetime, efficient carrier capture. The structural and opticl properties of GaAs/AlGaAs and InGaAs/GaAs quantum wire (QWR) heterostructures grown by organometallic chemical vapor deposition on nonplanr substrates, which satisfy many of these criteria, are described. These crescent-shaped QWRs are formed in situ during epitaxial growth resulting in virtually defect free interfaces. Effective wire widths as small as 10nm have been achieved, corresponding to electron subband separations greater than KBT at room temperature. The enhanced density of states at the QWR subbands manifests itself in higher optical absorption and emission as visualized in photoluminescence (PL), PL excitation, amplified spontaneous emission and lasing spectra of these structures. Effective carrier capture into the wires via connected quantum well regions, which is important for enhancing the otherwise extremely small capture cross section of these wires, has also been observed. Room temperature operation of GaAs/AlGaAs and strained InGaAs/GaAs QWR lasers with threshold currents as low as 0.6mA has been demonstrated.  相似文献   
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Spin-flip (paramagnetic) scattering and neutron depolarization studies were performed on Ce2Fe17 in its paramagnetic phase on the Dhruva neutron polarization analysis spectrometer. The absence of normalQ dependence of the scattered spin flip intensity shows that Ce2Fe17 is not a normal paramagnetic and there exist superparamagnetic clusters of sufficiently large dimensions (~100Å). The observed neutron depolarization gives an indication of the dynamics of these Ce2Fe17 superparamagnetic clusters.  相似文献   
6.
We study a linearly damped preloaded two-bar linkage that exhibits hysteresis due to the presence of multiple attracting equilibria. The dynamics at the unstable equilibrium, through which a snap-through buckle occurs, are not linearizable due to a solution-dependent singularity. We stabilize the unstable equilibrium using two distinct non-linear controllers. The feedback-linearization controller requires knowledge of the linkage parameters, whereas the robust version of the intrinsic non-linear proportional-derivative controller requires only an upper bound on the stiffness.  相似文献   
7.
The switched Poisson process (SPP), also known as the doubly stochastic Poisson process, has been widely used in the modelling of point processes whose rates vary subject to some random mechanism. The class of SPP includes a wide range of both renewal and non-renewal processes with squared coefficients of variation being larger than one. In this paper, we survey various approaches to approximate a non-renewal process by a renewal process. We derive the expressions for the first two moments of the inter-renewal time of a renewal process that approximates the SPP. We illustrate the quality of these approximations with numerical results in queueing applications. We believe that our approximations have potential applications in areas such as reliability, inventory control, telecommunications and maintenance.  相似文献   
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